1、 545482011 (IR)27 2002.184-,1.02004 .1 -,(),4,-()2 160-3-292011.632-4 34032007 .IR()(STM D 34032007 Standard test methods for rubber Evaluation of IR(isoprene rubber).,-,.-1.52004(3.5).,5 ,-.().-,2013 ,-II 5454820111 .12 .13 .14 .25 .26 .27 .68 .6 ()-,.10.11III 545482011 (IR)Isoprene rubbers(IR).Pre
2、paration and testing of rubber compounds 201307011 1.1 ,(IR).1.2,.-,-.2:5725-12002()-.1.545472011 .545492011.545522011.,-545532011 .-545542011 .,-,1 ,-.(),-().,.3 3.1 ,.-.1 545482011 3.2 .4 4.1 1.5 5.1 54549.6 6.1,-.:6.1.1 (6.2).6.1.2 B (6.3).6.1.3 C (6.4).6.1.4 D (6.5).1 SRM/IRM NIST (IR)b)TBBS)100
3、,005,002,252,0035,000,70:144,95 d)d):-3,0010,000,500,43)SRM/IRM.b)(IRB).c)N-2-.d),1,0,TBBS 0,02,-0,1.e),-0,1,0,01,-0,001.,.,V-.,.SRM/IRM.2 5454820116.2 6.2.1 54554.6.2.2 -2.2 ()-,-,.-,8,1/-0,00,0 50%,-,.0,50,5 3,03,5 .0,54,0 170 C 6,2,06,06.2.2.1 2.0,5%,.6.2.2.2 (40?5)C 6,0.6.2.2.3 124.6.2.3()3.3 ()
4、-,-,(40?5)C-.8,0/0,00,0 TBBS 50%-.0,50,5 (110?5)C 3 .2,53,0 0,8 (40?5)C2,05,0 ,6,1,06,06.2.3.1 3 .0,5%,.6.2.3.2 ,-545521-254547.6.2.3.3 ,2,2 -54554.3 5454820116.3 B 6.3.1 54554.6.3.2 ,6.2.2.6.3.3 4.6.3.3.1 4 -.0,5%,.6.3.3.2 ,-545521-254547.6.3.3.3 ,2,2 54554.4 ()-,-,(70?5)C 1,90.00 TBBS,.-.,3/4 33,.
5、3/4 36 ,0,8 28 ,6 ,196.4 6.4.1 54554.6.4.2 5.6.4.2.1 5.0,5%,.5 ()-,-,(70?5)C 0,20,11 1,40 -.3/4 23 1,70 .3/4 25,.50%-1,90.3/4 -14194 545482011 5-,-,TBBS,.-.,3/4 322,.-3/4 325 .0,8 227 ,-6,-1286.4.2.2 ,-545521-254547.6.4.2.3 ,2,2 54554.6.5 D 6.5.1 54554.(60?3)C 6,36,6/.6.5.2 ,(60?5)C ,0,5.25.6.5.3 6.
6、6.5.3.1 6 ,.-.6.5.3.2 (70?5)C0,5,3.0,8.6 (D)-,-,0,00,0 0,50,5 ,-,TBBS1,01,5 ,-1,02,5,6,59,06.5.3.3 .0,5%,.5 5454820116.5.3.4,-54552 1 -254547.6.5.3.5 -2,2 54554.7 7.1 7.1.1 2 54547.7.1.2 2:1,67,-1,160 C,30.1:1,67,-0,5,160 C,30.7.1.3:ML,MH,ts1,t?50t?90.7.2 7.2.1-.7.2.2 54554.7.2.3 20,30,40 60 -135 C.
7、-40.7.2.4 ,54553.-16 ,.8 8.1 3 4.,5725-1.8.2,-,.-,.8.3 2(),III.,.,=6,q=2,n=2.-IR .,-.:-ML4+1100 C(7);-35145 C,-:100%-,300%-,-,(8);6 545482011-160 C,-1,1,7(9);-160 C,0,5,1,7(10).7 2,III(-).ML4+1 100 C,sr(r)SR(R)50,151,350,72,41,92,26,95,46,213,710,512,22,43,32,96,99,38,213,718,016,1 :s ,;r (),s?2,83;
8、(r)(),;S ,;R (),S?2,83;(R)(),.8.4 -r,R,(r)(R).-rR,710,-.8 2,III(-).sr(r)SR(R)100%-,2,032,112,070,100,110,100,270,320,3013,4215,0414,280,310,310,310,880,870,8743,6041,0842,31 300%-,8,949,229,080,430,460,441,211,301,2613,5814,0913,850,820,840,832,312,382,3425,8325,8125,83 ,28,2228,2828,251,261,851,583
9、,585,234,4812,6818,4915,861,261,931,633,585,464,6212,6819,3316,35 ,%576,00582,75579,3815,0217,1216,1042,5048,4445,567,388,317,8623,6921,0922,4367,0359,6963,4711,6410,2410,957 545482011 8 :s ,;r (),s?2,83;(r)(),;S ,;R (),S?2,83;(R)(),.9 2,III(-).sr(r)SR(R)ML,?5,586,055,960,170,140,150,470,390,438,476
10、,467,270,490,330,421,400,941,1925,0515,5820,00MH,?36,4038,7037,550,920,690,812,591,942,297,115,026,102,192,002,106,195,675,9317,0014,6515,80ts1,3,934,234,080,130,160,150,370,460,429,3610,9710,260,350,280,320,990,780,8925,2818,5321,93t?50,6,356,586,460,230,180,210,660,510,5910,437,709,130,260,310,280
11、,730,860,8011,4513,1212,35t?90,8,498,828,660,390,250,321,090,700,9212,877,9910,610,400,380,391,131,081,1013,3312,1912,75 :s ,;r (),s?2,83;(r)(),;S ,;R (),S?2,83;(R)(),.8 545482011 10 2,III(-).sr(r)SR(R)ML,?1,681,731,700,180,180,180,510,500,5130,4129,2029,800,260,190,220,720,530,6443,0831,0137,36MH,?
12、14,7916,3915,590,260,070,190,740,200,555,031,233,500,660,670,671,881,891,8812,6911,5512,09ts1,3,153,413,280,080,130,110,240,370,317,5510,799,440,180,140,160,510,390,4516,0811,4513,79t?50,4,744,794,770,170,100,140,490,270,3910,335,618,290,200,170,180,560,470,5211,829,8110,85t?90,7,137,237,180,110,190
13、,160,320,540,444,457,476,170,390,310,351,120,881,0015,6512,1713,99 :s ,;r (),s?2,83;(r)(),;S ,;R (),S?2,83;(R)(),.8.5 ()r ,710.-,-r,710(),.8.6 ()R ,710.-,-R,710(),.8.7 (r)(R),rR.(r)(R)-.8.8,()-.-,.9 545482011(),.1 5725-12002IDT 5725-1:1994 (-).1.545472011IDT 52892007 -.-545492011MOD 38962007 .545522
14、011MOD 16462007 -.,-()545532011MOD 4122006 -.-545542011MOD 31822007 -.,-:-IDT ;-MOD .10 5454820111 62042007-(ASTM D 62042007Test method for rubber Measurement of unvulcanized rheological properties usingrotorless shear rheometers)2 20842007 .(ASTM D 20842007Standard test method for rubber property V
15、ulcanization using oscillating disk curemeter)3 44832005 -(ASTM D 44832005Standard practice for evaluating precision for test method standards in the rubber andcarbon black manufacturing industries)4 6912009 -(ASTM E 6912009Standardpracticeforconductinganinterlaboratorystudytodeterminetheprecisionofatest method)11 545482011 678.4:543.06:006.354 83.040.1069 2209:,545482011.11.02.2013.01.03.2013.60?8418.1,86.-.1,40.111.241.,123995,.,4.www.gostinfo.ruinfogostinfo.ru .,105062,.,6.
