1、 D 3906 03(2008),STANDARD TEST METHOD FOR DETERMINATION OF RELATIVE X-RAY DIFFRACTION INTENSITIES OF-TYPE-CONTAINING MATERIALS :1217-10/ASTM :31.05.2010 2010 (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This tran
2、slation is executed by FGU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these tr
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4、USA legislation and international copyright.-,.9,-49,-1,119991.:(495)236-54-49:(499)230-13-72 E-mail:interstgost.ruhttp:/www.interstandart.ru ASTM D 3906-03(2008)D 3906 03(2008),1 D 3906;,.()1.1.1 ,Y X,Y.24,2-25,0 (2,42-2,50).A1.2 ,.1.3 1 ASTM D32 D32.05 s.1 2008.2008.1980.2003 D 3906-03.1ASTM D 390
5、6-03(2008)(XRD)-,.1.4 ,NaY.(Y X,REY .),%XRD /NaY.1.5 .:1.5.1 ,.1.5.2 .1.6 ,.,.2.2.1 ASTM:2E 177 ASTM E 456 .E 691 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.2ASTM D 3906-03(2008)3.3.1 ,(NaY),.,%XRD /NaY.,(533)(23,5 Cu K),%XRD /NaY(533)4.4.1 Y X,.,.Y (FCC),X ,.4.2 Y X ,.
6、,.Y X .,.3ASTM D 3906-03(2008)H2O .,Y X .4.3.1-,4.3,.(2).1 ASTM NaY;4ASTM D 3906-03(2008)4.4 ,.,.5.5.1 ,-.5.2 ,110C.5.3 (),35%,CaCl26H2O.Y Na (2).2 NaY 5.4 5ASTM D 3906-03(2008).6.6.1 NaY RE Y .3 7.7.1 ,.7.2 ,.1 ,.8.8.1 ,8.2-8.5,NaY.8.2 3-5 110C 1.35%,16.2 ,.8.3 ,.8.4 ,14 35 2 1/3 (NIST),100 Bureau
7、Dr.,Stop 3460,Gaithersburg,MD 20899-3460.6ASTM D 3906-03(2008),.8.4.1 ,10/.()NaY,(533)23,6 50 100%.(),.,(533),10%.1 NaY ,.8.5 ,.(.2 NaY.)8.6 ,1/4/.3 ,.,0,02 2/1 NaY,10-20 .8.6.1 22,5 25 2,(533).3 NaY.,(,):14,0 17,0,(331)19.0 22,0,(440)25,5 28,0,(642)7ASTM D 3906-03(2008)4 8.6 ,.,24,2-25,0 (2,42-2,50
8、)A.X1 .(2).3 NaY ASTM 9.9.1 8ASTM D 3906-03(2008)()8.4,:9.1.1 (9.2 ),9.1.2 (9.3 ,),9.1.3 ,(9.4 ).9.2 :9.2.1 ,SFC-,SFX,SFR.,SFC=SFX/SFR.,.9.2.2 (533),8.6.,.,WF,WX,NaY,WR.,WF=WX/WR.5 .:,0,2;,.9.2.3 ,%XRD /NaY .(9ASTM D 3906-03(2008),8.4.,SFC,9.2.1,WF,9.2.2.1:6 2,1 24,2-25,0 (2,42-2,50).A 7 ,NaY.1 2 hk
9、l Peak 2 hkl 1 15,7 0,2 331 2 18,7 0,2 511,333 3 20,4 0,3 440 4 23,7 0,4 533 5 27,1 0,5 642 6 30,8 0,5 822,660 7 31,5 0,5 555,751 8 34,2 0,6 664 9.2.4 :%XRD /NaY=SFX WF (SX/SR)100(1):SX-SR-NaY.:,(533),.10ASTM D 3906-03(2008),.,.9.3 :9.3.1%XRD/NaY,(),8.4(.7).:%XRD /NaY=100RXSS(2):S-,SR-NaY.9.4 :9.4.1
10、%XRD/NaY,(),8.4(.7).:%XRD /NaY=100rxSS(2):Sx-,Sr-NaY.9.5 XRD ,.,(533).11ASTM D 3906-03(2008),.,8.6.(533)()8.6 ,NaY :9.5.1 ,8.6;9.5.2 ;9.5.3 .9.5.4 .,.3,(622),0,25 (533),.,.%/NaY(533)=100 (CX/CR)(4):CX-,CR-NaY.%XRD /NaY(533)=100 SFC (AX/AR)(5):AX-AR-,NaY.%XRD /NaY(533)=100 SFC WF (HX/HR)(6):HX-HR-NaY
11、.12ASTM D 3906-03(2008)-,(533)8.6,(331),(440),(642),(533).9.6 ,9.2,9.3 9.4:%XRD /NaY NaY,NaX 90 105 NH4Y 100 115 REY 25 50 Y 80 95 9.7 ,.9.8,9.2-9.4 ,.,9.2-9.4,1/2 2 9.5.,%XRD /NaY%XRD /NaY(533).9.9 9.2.2.,.10.10.1 :10.1.1 XRD /NaY.,REY,XRD /REY.13ASTM D 3906-03(2008)10.1.2 ,.(.9.1-9.4)(533)(.9.5).1
12、1.4 11.1 ,.E 691,.11.2 ,2,772 S,2,772 S 95%,S .E 456 E 177.()95%()95%()A 25,4 1,3%(5,2%)5,9%(23%)12,3 0,9%(7,3%)8,7%(71%)12,8 1,1%(8,6%)4,4%(34%)8 ,.11.3 .4 ASTM ,Report RR:D32-1010.14ASTM D 3906-03(2008)12.12.1;()X1.X1.1 15ASTM D 3906-03(2008)ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).16
