1、:D 3865 09 STANDARD TEST METHOD FOR PLUTONIUM IN WATER :1060-10/ASTM :02.07.2010 2010 -,.9,-49,-1,119991.:(495)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,AST
2、M International ,.This translation is executed by FGU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve an
3、d does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FGU“CIC“Interstandard”,is strictly
4、forbidden according to the USA legislation and international copyright.ASTM D 3865-09 1:D 3865 09 1 D 3865;,.()1.*1.1 -0,01/(0,3/)-(-).-239Pu 240Pu.1 ,.,.,.1.2 .1 ASTM D19 D19.04.1 2009.2009.1980.2002.D3865-02.DOI:10.1520/D3865-09.ASTM D 3865-09 21.3 ,.,.9 2.2.1 ASTM:2 C 859 1163 -1284 -D 1129 D 119
5、3 D 2777 D19 D 3084 -D 3370 D 5847 3.3.1:3.1.1 ,.D 1129 C 859.2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 3865-09 34.4.1 -,236Pu 242Pu.(III),.,8 M HNO3 .-,.4.2 -,-.1 -,.238Pu 239/240Pu ,236Pu 242Pu(.1).5.5.1 ,.,.ASTM D 3865-09 46.6.1,-228,238Pu 100 ,238Pu.228Th .-
6、60-,238Pu 228Th ;-238Pu 5,50-,228Th-5,42-.228Th-.1.A -()236Pu 2,858 5,767(69,14)5,730(30,70)238Pu 87,7 5,499(71,4)5,456(28,6)239Pu 2,4110 104 5,158(73,3)5,144(15,1)5,105(11,5)240Pu 6563 5,168(73,51)5,123(26,39)242Pu 3,733 105 4,902(79)4,858(21)241AmB 432,2 5,544(0,36)5,485(85,1)5,442(13,3)228ThB 1,9
7、131 5,423(73,4)5,340(26,6)A ,11,.,1996.,241Am,238Pu.ASTM D 3865-09 56.2 ,-.,242Pu .-236Pu ,.236Pu .,242Pu -.7.7.1 -,50-(),.15%,60000.7.2 0 12 0 2 A()().20,.1 8,.ASTM D 3865-09 6 50C.7.3 -100.7.4 13 150 100-,.8.8.1 .,.3 ,.8.2 ,D 1193,III .8.3 ,.8.4 (.15 M,28%)(NH4OH).,.,.8.5 (1,5 M)100 15 M NH4OH 3 ,
8、.,.,BDH Ltd.,Poole,ASTM D 3865-09 7 250 1.,.,.8.6 (0,15 M)10 15 M NH4OH 250 1.,.8.7 (1 M)14,5 NH4I 100.8.8 ,4%,100 200,.8%.,15,4%.8%,.8.9 (H3BO3).8.10,1 M (NH4)2SO4.132 1.,NH4OH H2SO4,pH 3.5.8.11 (C2H5OH)95%NH4OH 100 .8.12-(50 Fe/)24 FeCl36H2O 4,4 (1,19)95,6 .8.13 (.12 M,36%)(HCl).ASTM D 3865-09 88.
9、14 (9 M)750 12 M 150 1.8.15 (29 M,49%).8.16 (H2O2)30%.8.17 (16 M,69%)(HNO3).8.18 (8 M)500 16 M 250 1.8.19 (1.8 M)110 16 M 500 1.8.20 236Pu 242Pu(.0,2/),15,242Pu.236Pu ,.1 236Pu 242Pu (NIST),NIST,;.8.21 10 100 ,100 H2SO4(18 M,95%),.5 NaHSO4 100 9 M H2SO4.8.22 (NaNO2).8.23 (18 M,95%)(H2SO4).8.24 (1,8
10、M)100 18 M ASTM D 3865-09 9 750 1.:,.8.25 0,04 100 .9.9.1:.,.10.10.1 D 3370.24,pH 1 HNO3(1,8 M).11.11.1 236Pu 242Pu,NIST .,.236Pu or 242Pu,.ASTM D 3865-09 1012.12.1 :12.1.1 .1.12.1.2 ,150 HNO3 .12.1.3 236Pu 242Pu,0,2 236Pu 242Pu.,239Pu,240Pu 238Pu ,236Pu.12.1.4 60C 1.12.1.5 1 -10.12.1.6 NH4OH,.NH4OH
11、,pH 9 10,.12.1.7 30,.12.1.8 ,.,.12.1.9 100 .12.1.10 .ASTM D 3865-09 1112.1.11 ,HNO3,2 30%H2O2,2 HNO3 .,.2 HNO3 .12.1.12 ,HNO3 ,12.1.11,100-150 8 M HNO3,12.3.HNO3,12.2.12.2 :12.2.1 HNO3,HNO3 75,-75 .(.9.)12.2.2 4 .HNO3 ,150.12.2.3 -.12.2.4 .12.2.5 12.2.4,75 HCl 2 H3BO3 12.2.3.,.12.2.6 HCl-H3BO3 ,.AST
12、M D 3865-09 12 .12.2.7 -10.12.2.8 100 HNO3 HCl.12.2.9 50.12.2.10 ,.12.2.11 HNO3(8 M)150,1 H3BO3 .12.2.12 ,HNO3(8 M).12.3.1.12.3 :12.3.1 10 .12.3.2 13 80.,.12.3.3 HNO3(8 M),.12.4 :12.4.1 (12.1.12)(12.2.12),8 M HNO3,1 NaNO2,.12.4.2 5/.12.4.3 HNO3(8 M)5 ASTM D 3865-09 13/.12.4.4 HCl(9 M)2/.2.,.,9 M HCl
13、 ,1/.,.12.4.5 2/NH4I-HCl,1 1 M NH4I 30 HCl.12.4.6 HCl.12.4.7 20 5 HNO3.12.4.8 .12.4.9 20 HNO3 .12.5 .C 1284.,.12.5.1 2 5%NaHSO4H2O 9 M H2SO4.12.5.2 5 HNO3,.12.5.3 5 ,.ASTM D 3865-09 1412.5.4 ,5-10 ,.12.5.5 3 4 .-,1,5 M NH4OH -.,pH 1,8 M H2SO4.12.5.6 10 ,.12.5.7 ,1,2 A.,1,2 A.12.5.8 1,5-2,0.12.5.9 ,1
14、 NH4OH 1.12.5.10 .12.5.11 NH4OH(0,15 M).12.5.12 .12.5.13 ,.12.5.14 ,.12.6-:12.6.1 -.ASTM D 3865-09 15.D 3084.12.6.2 238Pu,239/240Pu 236Pu 242Pu,.13.13.1 239/240Pu,238Pu ,:(1):ACa-239/240Pu 238Pu ,/,Ca,n-239/240Pu 238Pu -,ACt-236Pu 242Pu,/,Vt-236Pu 242Pu,DFt-,Ct,n-236Pu 242Pu -,Va-,(.10.1).13.1.1 ,()
15、,1.13.2 -,-.ASTM D 3865-09 16:(2):Rr,n-,Ar-.13.3-:(3):t-,.13.4 (1s):(4):u(Ca,n)-,u(ACt)-236Pu 242Pu,/,u(Vt)-236Pu 242Pu,u(Ct,n)-236Pu 242Pu -,u(Va)-,.ASTM D 3865-09 17 ,Cn=Cs Cb,/:(5):Cs-,Cb-,u(Cc)-()Cc,236Pu 242Pu.13.5 :(6)13.6 ():(7):Ra,b-.14.14.1 ,.20,ASTM D 3865-09 18.14.2 12.1.3,236Pu 242Pu ()2
16、39/240Pu 238Pu .11.1,236Pu 242Pu (NIST NPL).14.2.1-236Pu 242Pu .14.2.2 -(1-)5%(.400 ).14.3 239/240Pu 238Pu ,-236Pu 242Pu.,NIST,NIST,.14.4 :14.4.1 ,.,.14.4.2 ,(),238Pu/239Pu,(1-)1%.ASTM D 3865-09 19 ,.,.,.241Am 228Th,238Pu.14.4.3 ,10%10%,.4 D 5847 ,.,.14.4.4 ().,.,.4 -ASTM International D19-1063.ASTM D 3865-09 20 241Am 228Th,238Pu.,.14.4.5 239/240Pu 238Pu .,.6A()MARLAP5.14.5 ():14.5.1 ,20.,.,.,25%.14.5.2 ,.14.6 (),20.,.,.5 NUREG 1576,EPA 402-B-04-001A-C,NTIS PB2004-105421,MARLAP,1-3,2004.www.epa.
