1、:D 368213 STANDARD TEST METHOD FOR MAJOR AND MINOR ELEMENTS IN COMBUSTION RESIDUES FROM COAL UTILIZATION PROCESSES 2014 ():2470-14/ASTM :06.10.2014 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshoho
2、cken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Co
3、nshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except
4、 for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 3682-13 1:D 368213 1 D 3682;,.()1.1.1 .1 D 5016.1.2,.1.3 ,.1 ASTM D05 D05.29 .15 2013.2013.1978.2006.D3682-01(2006).DOI:10.1520/D3682-13.ASTM D 3682-13 2 ,.2.2.
5、1 ASTM:2 D 121 D 346 D 1193 D 2013 D 3173 D 3174 D 3180 ,D 5016 D 7348 (LOI)D 7582 E 691 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 3682-13 33.3.1 ,.D 121.4.4.1 750C .(Li2B4O7)(HCl),(HNO3)./.5.5.1 .5.2 ,.6.6.1 ,500C 750C.6.2 ,1000C.6.3 ,35 85.ASTM D 3682-13 46.4
6、,200C.6.5-,(D2),.7.7.1 .,.3 ,.,.7.2 ,II,D 1193.7.3 (1000 ).7.4 (1000 ).7.5 (1000 ).7.6 (175/(LaCl3)10%).7.7 (Li2B4O7),.3 ,Washington,DC.,.,BDH Ltd.,Poole,Dorset,U.K.,Inc.(USPC),Rockville,MD.ASTM D 3682-13 57.8 (1000 ).7.9 (1000 ).7.10 (200 )(.2).7.11 (1000 ).7.12-50 (.1,19)50 (.1,42)1000.,.7.13 (100
7、0 ).2 ,.,0,1070 (SiO2)1 ,-250,9.3.1 9.3.2.200 .()9.3.1 9.3.2.(),.8.8.1 D 2013,D 346,250 (60).8.1.1 D 3173,D 3174 D7582 ,.8.2 (8.1).,6.ASTM D 3682-13 6 ,500 10C 1.,500 10C 750 10C 1.750C .,75 (200).1 750C,.8.3 107 3C.,.75 (200).,.8.4 ,2.,500 10C 1.,500 10C 750 10C 1.750C .,75 (200),750C 1.8.5 /CO2,75
8、0C.,D 7348,ASTM D 3682-13 7 ,.9.9.1 ,.,.,.9.1.1,E,:=(C B)/(A B)(N/M)F 100(1):A-;-;-;N-,;M-,;F-.3 ,:=(A B/100%):-(),%;ASTM D 3682-13 8A-,%;-(),D 3174 D 7582,%,D 3180.D 3180.9.2 ,-.,.9.3 :9.3.1 (6.3)(.4)0,1 0,0002 ,8.2 8.5,0,5 Li2B4O7.,0,5 Li2B4O7,.,1000C;15 1000C .,250-400-.,-,150 -.30 .,ASTM D 3682-
9、13 9 .4 ;.4 9.3.2 .200-,-200.500 5/Li 2B4O7.9.3.3 1 20 ,9.3.2,50-.200 2/Li2B4O7.9.3.4 2 10 ,9.3.2,100-,10 (.7.6)-.50 0,5/Li2B4O7.5 ,(,).,.10.(SiO2)10.1 ,7.10 4 .“-”,141,DC,1975,.57-65.ASTM D 3682-13 10 1 (7.3)100 (.10.2).,SiO2 .,(7.10),SiO2,%25 50 53,5 20 40 42,8 15 30 32,1 10 20 21,4 10.2 2/Li2B4O7
10、 -.10.3 200-,9.3.3.10.4 251,6.10.5 ,.,.SiO2 :SiO2,%=(C B)/(A B)N 1,07(2):A-C,-,-,N-,.ASTM D 3682-13 1111.(Al2O3)11.1 ,10 30 10.2.11.2 ,10.2.11.3 1,9.3.3.11.4 309,2.11.5 ,.Al2O3 :Al2O3,%=(C B)/(A B)N 0,94(3):A-C,-,-,N-,.12.(Fe2O3)12.1 ,2-10 10 100.(12.2).12.2 -,ASTM D 3682-13 12 0,5/Li2B4O7.12.3 2,9.
11、3.4.12.4 248,3.-.12.5 ,.Fe2O3 :Fe2O3,%=(C B)/(A B)N 2,86(4):A-C,-,-,N-,.13.(CaO)13.1 ,1 10 10 100.,12.2.13.2 ,12.2.13.3 2,9.3.4.13.4 422,7.-.ASTM D 3682-13 1313.5 ,.CaO :CaO,%=(C B)/(A B)N 2,80(5):A-C,-,-,N-,.14.(MgO)14.1 ,0,5 2 10 100.,12.2.14.2 ,12.2.14.3 2,9.3.4.14.4 285,1.-.14.5 ,.MgO :MgO,%=(C
12、B)/(A B)N 3,32(6):A-C,-,ASTM D 3682-13 14-,N-,.15.(Na2O)15.1 ,0,5 2 10 5 100.,12.2.15.2 ,12.2.15.3 2,9.3.4.15.4 589,0.-.15.5 ,.Na2O :Na2O,%=(C B)/(A B)N 2,70(7):A-C,-,-,N-,.6 ,.5 -ASTM International RR:D05-1000.ASTM D 3682-13 1516.(K2O)16.1 ,0,5 2 10 5 100.,12.2.16.2 ,12.2.16.3 2,9.3.4.16.4 766,5.-.
13、16.5 ,.K2O :Ka2O,%=(C B)/(A B)N 2,41(8):A-C,-,-,N-,.7 ,.8 ,.17.(TiO2)17.1 ,3 5/Li2B4O7,-.ASTM D 3682-13 16 (.17.2).17.2 ,5/Li2B4O7,-.17.3 ,9.3.2.17.4 364,3./.17.5 ,.TiO2 :TiO2,%=(C B)/(A B)1,00(9):A-,-,-.18.18.1 10.5,11.5,12.5,13.5,14.5,15.5,16.5 17.5.18.2 ,.18.3 ,D 3180.19.19.1 .1.,(Sr,r)ASTM D 368
14、2-13 17(SR,R).A1.1.19.1.1 (r),95%.1 ,%r R SiO2 33,14 57,73 0,33+0,04xA 1,21+0,14x Al2O3 11,32 31,83 0,80 0,24+0,09x Fe2O3 2,93 41,11 0,01+0,06x 0,36+0,06x MgO 0,45 7,12 0,04+0,03x 0,04+0,09x CaO 1,46 22,19 0,21+0,04x 0,15+0,11x TiO2 0,57 1,44 0,13 0,19 K2O 0,45 2,99 0,03+0,03x 0,05+0,05x Na2O 0,14 7
15、,15 0,06+0,03x 0,04+0,18x A x-.19.1.2 (R),95%.19.2 1633b ,.ASTM D 3682-13 18 NIST ,.2.19.3 ,E 691,1999.6 2 1633b ,%(95%)SiO2 49,57 0,96 49,25 0,17 0,65 Al2O3 28,16 0,31 28,44 0,51 0,98 Fe2O3 10,96 0,25 11,12 0,33 1,44 MgO 0,79 0,02 0,80 0,01 1,25 CaO 2,01 0,12 2,11 0,08 4,74 TiO2 1,30 0,04 1,32 0,02
16、 1,52 K2O 2,25 0,04 2,35 0,04 4,25 Na2O 0,26 0,02 0,27 0,004 3,70 20.20.1 (A12O3);-;(CaO);(Fe2O3);(MgO);(K2O);(SiO2);(Na2O);(TiO2)6 -ASTM International RR:D05-1000.ASTM D 3682-13 19()A1.A1.1 ,(Sr,r)(SR,R),.A1.1.A1.2 (Sr),.A1.3 (SR),.ASTM D 3682-13 20 A1.1 (Sr,r)(SR,R),ASTM D 3682-13 21ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,USA.()ASTM 610-832-9585,610-832-9555 serviceastm.org (www.astm.org).ASTM(www.as
