1、 D390017 ()-()-STANDARD TEST METHODS FOR RUBBER DETERMINATION OF ETHYLENE UNITS IN ETHYLENE-PROPYLENE COPOLYMERS(EPM)AND IN ETHYLENE-PROPYLENE-DIENE TERPOLYMERS(EPDM)BY INFRARED SPECTROMETRY 2018 ():23.04.2018:3411-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.in
2、terstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for
3、Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original ve
4、rsion.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D3900-17 1 D390017 ()-()-1 D3900;,.()1.1.1 ()-()35 85%.,().1 ASTM D11 D11.11 .1 2017.2017.1980
5、.2015.D3900-15.DOI:10.1520/D3900-17.ASTM D3900-17 2 ,.:1.1.1 :A ,35 70%9 14 B ,60 85%,-1,4-15 19 C ,35 85%-20 24 1.1.2 :D ,35 85%,-1,4-25 32 1.2 ,1.3,.D.1.4 ,.,.1.5 -,(TBT).ASTM D3900-17 3 2.2.1 ASTM:2 D297 D3568 (-),D4483 ,E168 -3.3.1 A 8,65/13,85 (1156/722-1),.1 ,.3.2 B 7,25/13,85 (1379/722-1),.3.
6、3 C 8,65/2,35 (1156/4255-1 2 ASTM,ASTM),.www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D3900-17 4 3.4 D 7,25/6,85 (1379/1460-1),.4.4.1 ,-D3568 .4.2 .,.5.5.1-1,4-7,25 (1379-1)A C.5.2 ,8,65 (1156-1).A C ,B D,.5.3-,-.ASTM D3900-17 5 6.6.1 ,200 (29000 .)150C.6.2-,1%,2,5 15 (4000 667-
7、1 400000 66700-1)A,B D.C ,2,0 15 (2000 667-1 200000 66700-1).,.-E168.6.3 -(-),.-,-.(33)-.7.7.1 ,.ASTM D3900-17 6 7.2 ,.8.3 8.1 ,D4483.D4483.8.2 (),.-,.8.3 1().,;.8.4 ,:,%A 40-60 6 3 A 65-76 5 2 B 60-66 4 2 D()40-70 4 4 D()72 3 1 3 ASTM International RR:D11-1021.ASTM D3900-17 7 .8.5 1 A,B D.2 ,.,.8.6
8、 ,r,R,(r)(R),.r R,1,.8.7 ,r,1.,r(),.8.8 ,R,1.,R(),.ASTM D3900-17 8 8.9 ,(r)(R),r R.(r)(R).1.1 1 (r)(R).,%A A Sr r(r)SR R(R)A 40 60 0,569 1,61 3,22 0,857 2,43 4,86 A 65 76 0,471 1,33 1,90 1,74 4,92 7,0 B 60 66 0,433 1,23 1,95 0,540 1,53 2,43 D(-)40 70 0,856 2,42 4,40 2,11 5,97 10,9 D(-)72 2,12 6,00 8
9、,3 3,55 10,0 13,9 A Sr-,;R-,;(r)-(),;SR-,;R-,;(R)-(),.8.10 :8.10.1 ,-/.,/.-C14-,ASTM D3900-17 9 ,(-).4 8.10.2 -13C,.8.10.3 (.13.2).5 1 40,1 2 52,4 3 58,6 4 66,8 5 70,8 6 78,6 7 44,8 8 52,6 9 69,5 10 77,5 4 Gardner,I.J.,Cozewith,C.,Ver Strate,G.,-(Infrared Determination of Composition of Ethylene-Pro
10、pylene Copolymers),(Rubber Chemistry and Technology),.44,1971.,.1015-1024.8.11 A -.2.-,-13C.5 ASTM International RR:D11-1065.ASTM D3900-17 10 A 8,65/13,85 9.9.1 35 70%.9.2 60 80%,B.9.3 8,65 (1156-1)8,93 (1120-1),.B D.9.4 ,.10.10.1 8,65 (1156-1)13,85 (722-1).A8.65/A13.85 .11.11.1 .,ASTM D3900-17 11 ,
11、.6 ,.11.2 ,().11.3.11.4 .11.5 ,2002001,5 (880,06).11.6 ,0,04 (0,0015).11.7 -.12.12.1/(0,2).12.2 -.6 ,.,.,.,BDH Ltd.,.,.,Inc.(USPC),.,.12.3 ,.ASTM D3900-17 12 12.4 30 60 ,(,70,10000 .150 10C).12.5 ,-.12.6 ,.12.7 ,.-.12.8 :12.8.1 -.,.12.8.2 .12.9 13,85 (722-1).,0,5 1,2 A(1,5 A;,ASTM D3900-17 13 Frank
12、Settle;14;.271).,0,5 1,2 A;.,.12.10 -.,.12.11 7 16 (1400 600-1).12.12 8,65,8,20 8,93.8,20,8,93.,8,20,().1.-;B D,.12.13 8,65;1156-1(.2).12.14 13,85-,12,7 14,8.2.1 AA ,%Sr r(r)SR R(R)-1237 52,4 0,259 0,724 1,38 0,557 1,56 2,98 -865 56,9 0,225 0,629 1,11 0,688 1,93 3,39 -2154 58,1 0,197 0,550 0,947 0,7
13、66 2,15 3,70 -306 67,9 0,400 1,12 1,65 0,814 2,28 3,36 -227 74,4 0,711 1,99 2,67 1,12 3,14 4,22 A p=9,q=5,m =2.ASTM D3900-17 14 .1.8,65 .2A:2,35,8,65 13,85 (-1).1.1156-1 1156-1 720-1 1156-1 720-1 (-1).2A.1156 720 ASTM D3900-17 15 .2:2,35,8,65 13,85 ()12.15 13,85 (.2).8,65 (),.B,C D.12.16 .13.13.1 8,
14、65 13,85.13.2 A8.65/A13.85 (-1).2.4255 1156 1156-1 A4255=A4255 A4450 A 4450-1 A 4255-1 ASTM D3900-17 16 -35 70%.,.,.7 13.3 .30.14.14.1 ,.14.2 .14.3 ,.B 7,25/13,85 15.15.1 60 85%.7 ExxonMobil Chemical,-.,ExxonMobil,5200 Bayway Drive,/5200,.,.77520.15.2 60%,.ASTM D3900-17 17 15.3 1,4-,7,25.15.4 ,.16.1
15、6.1 7,25 13,85.A7.25/A13.85 .17.17.1 .12.1 12.7.17.2 ,7,25 .12.8 ,200 MPa(29000 .),.17.3 7,25 (1379-1).,0,5 1,2 A(1,5 A8 8 Settle,F.,(Handbook of Instrumental Techniques for Analytical Chemistry),14,.271.).,0,5 1,2 A,.ASTM D3900-17 18 ,.17.4 -.12.10.17.5 6,50 17.17.6 7,25,7,1 7,6.17.7 7,25 (.3).17.8
16、 13,85,12,75 14,8.17.9 13,85 (.2).17.10 .3.7,25 13,85 (B)A 1379-1 A 721-1 1156-1()(-1).5.1379 721 ASTM D3900-17 19 18.18.1 7,25 13,85.18.2 A7.25/A13.85 -60 85%.13.2.18.3 .33.19.19.1 ,.19.2 .19.3 ,.8,65/2,35 20.20.1 35 85%,1,4-.20.2 ,5.2,9.3 12.12 8,65.,ASTM D3900-17 20 B D.20.3 .21.21.1 8,65 C-H 2,35 .22.22.1 .12.1 12.7.0,1 0,2.22.2 2,35.0,15 A 0,2 A,.,8,65.22.3 -.12.10.22.4 2,0 10,0 .22.5 2,35 2,20.A2.20 A2.35,A2.35(.2).22.6 8,65,8,20 8,93.8,20,8,93.,8,93,ASTM D3900-17 21 (.1).-;B D,.22.7 8,65