1、:D 432711 STANDARD TEST METHOD FOR ANIONS IN WATER BY SUPPRESSED ION CHROMATOGRAPHY ():1576-11/ASTM :08.12.2011 2011 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM Internat
2、ional ,ASTM International.-,ASTM International ,.This translation is executed by FGU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM In
3、ternational does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FGU“
4、CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 4327-11 1 :D 432711 1 D 4327;,.().1.*1.1 2 ,.1 ASTM D19 D19.05 .15 2011.2011.1984.2003 D 4327-03.DOI:10.1520/D4327-11.2 :Small,H.,Stevens,T.S.,Bauman,W.C.,.47,1975,.1801.Stevens,T.S.,Turkelso
5、n,V.T.,Alve,W.R.,.49,1977,.1176.Sawicki,E.,Mulik,J.D.,Witgenstein,E.,Editors,-,Ann Arbor Science Publishers,Ann Arbor,MI,1978.Mulik,J.D.,Sawicki,E.,Editors,-,.2,Ann Arbor Science Publishers,Ann Arbor,MI,1979.Weiss,J.,Dionex Corp.,Sunnyvale,CA,1986.,Waters Chromatography Division of Millipore,Method
6、A 107 and A 116,1990.Haddad,P.R.,Jackson,P.E.,:,Elsevier Scientific Publishing Co.,1990.*ASTM D 4327-11 2 1 ;.1.1.2 .(/):0,26 8,49 0,78 to 26,0-N 0,36 to 12,0 0,63 to 21,0-N 0,42 to 14,0 o-0,69 to 23,1 2,85 to 95,0 1.3 .1.4 0,01/,.50-3/,1.,.1,AS4A ;/;ASTM D 4327-11 3 1.5 ,1.1.6 ,:,.1.7 ,(),.,X2.1.8,
7、.1.9 ,.,.ASTM D 4327-11 4 2.2.1 ASTM:3 D 1066 D 1129,D 1193 D 2777 ,D19 D 3370 D 5810 D 5847 3.3.1 ,.D 1129.3.2 ,:3.2.1 ,.3.2.1.1 ,.3.2.2 ,.3.2.2.1 ,3 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 4327-11 5 .3.2.3 ,.3.2.4 ,.3.2.5 ,.3.2.6 .3.2.7 ,.1 ,A,/1 1,2 0,01 2 1,
8、7 0,02-N 3 2,0 0,004 4 2,9 0,01-N 5 3,2 0,002 o-6 5,4 0,003 7 6,9 0,02 A ,).:7.1.4.:7.1.6.:8.3.:2,0/.:50.ASTM D 4327-11 6 4.4.1 .,.,.,.5.5.1 ,F,Cl,N2,HPO42,Br,N3 S42,10-15 .,.2 ,(100 8.3)100-,(.6.3 6.4).ASTM D 4327-11 7 .,(,.),.,.,.5.2 ,Cl/Br N2/NO3,.6.6.1 ,.;,Cl/NO2,1:10 10:1,.6.2 ,.(.A1),.,.6.3 ,.
9、Cl.ASTM D 4327-11 8 .X1.6.4 ,(.2).,.,.X1.2 ASTM D 4327-11 9 7.7.1 ,.2:4 7.1.1 .7.1.2 ,1 3/2000 .7.1.3 ,.7.1.4 ,.3 .,.1.7.1.5 ,.,.,.().7.1.6 ,4 Dionex Corp.,1228 Titan Way,Sunnyvale,CA 94086.ASTM D 4327-11 10 0 1000/,.7.1.7 ,.7.1.8 ,.-100.,.,1 .1 100.7.1.8.1 ,.,23 .8.8.1 .,.5 ,.5 ,American Chemical S
10、ociety,Washington,DC.,.,BDH Ltd.,Poole,Dorset,U.K.,.ASTM D 4327-11 11 8.2 ,II D 1193;I .,II 0,22 .,.0,2/.8.3 0,2856 (1,7 M)0,3816 (1,8 M)2.,.8.3.1 NaOH ,50%NaOH()(18,2)1000 .50%NaOH ,.50%NaOH ,.5,25 50%NaOH 100 M.,ASTM D 4327-11 12 ,.,.4 -.8.4 3 H2SO4(.1,84)4 .8.5 :8.5.1 (1,00 =1,00 Br)2 (NaBr)6 150
11、C .1,2877 1.8.5.2 (1,00 =1,00 l)(NaCl)1 100C .1,648 1.8.5.3 (1,00 =1,00 F)2,210 (NaF)1.8.5.4 (1,00 =1,00 NO3)2 (NaNO3)105C 48.ASTM D 4327-11 13 1,371 1.8.5.5 (1.00 =1,00 NO2)2 (NaNO2)125-(24),H2SO4.1,500 1.5 ,.6 ,1 170C .8.5.6 (1,00 =1,00 HP42)1,433 (KH2PO4)1.8.5.7 (1,00 =1,00 S42)(Na2SO4)1 105C .1,
12、479 1.8.6 3 ,ASTM D 4327-11 14 .,.8.6.1 ,.,.,2 3,.2 ,/,/(1.00 =1,00),1000 ,/(F)10 10 1,0 0,2 (Cl)10 10 1,0 0,2 (NO2)20 20 2,0 0,4 50 50 5,0 1,0(HPO42)(Br)10 10 1,0 0,2 (NO3)30 30 3,0 0,6 (SO42)100 100 10,0 2,0 ASTM D 4327-11 15 3 (1 =1,00),/4 4 4 4 10 10 50 50 10 10 30 30 50 50 9.9.1 D 1066 D 3370.9
13、.2 .,4C.9.3 ,0,22-,.10.10.1 :10.1.1 ,.().3,8(8.5.1-8.5.7)1.ASTM D 4327-11 16 11.7 .,.10.1.2 ,3,.,1 10/.10.1.3 .1.,.10.2 ,8.6,(.11).8 ,.9 .10 .10.3 ASTM D 4327-11 17 .,.11 30/HPO42.,.30/HPO42 .11.11.1 .11.1.1 .1 30/.,.11.2 ,(15-20)10 15 .,.,.,.11.3 2-3 .(.1).12 ,ASTM D 4327-11 18 ,;,.12.12.1 ,(),10.3
14、,:,/=A F:A-,F-,.13.6 13.1 ,19,.,.(So).13.2 ,4-11.13.3 ,6 ASTM.RR:D19-1147.ASTM D 4327-11 19 ,.4 ,/,/St So ,%0,26 0,25 0,08 0,11-3,8 0,34 0,29 0,11 -14,7 2,12 2,12 0,07 0,12 0,0 2,55 2,48 0,14 -2,7 6,79 6,76 0,20 0,19-0,4 8,49 8,46 0,30 -0,4 0,26 0,24 0,08 0,05-7,7 0,34 0,34 0,11 0,0 2,12 2,09 0,18 0
15、,06-1,4 2,55 2,55 0,16 0,0 6,79 6,84 0,54 0,25+0,7 8,49 8,37 0,75 -1,4 0,26 0,25 0,15 0,06-3,8 0,34 0,32 0,08 -5,9 2,12 2,13 0,22 0,15+0,5 2,55 2,48 0,16 -2,7 6,79 6,65 0,41 0,20-2,1 8,49 8,27 0,36 -2,6 13.4 4-10 ,.13.5 D 2777-77,.,.1.4 D 2777-08,D19 .ASTM D 4327-11 20 5 ,/,/St So ,%0,78 0,79 0,17 0
16、,29+1,3 1,04 1,12 0,46 +7,7 6,50 6,31 0,27 0,14-2,9 7,80 7,76 0,39 -0,5 20,8 20,7 0,54 0,62-0,5 26,0 25,9 0,58 -0,4 0,78 0,54 0,35 0,20-30,8 1,04 0,51 0,38 -51,0 6,50 5,24 1,35 1,48-19,4 7,80 6,02 1,90 -22,8 20,8 20,0 2,26 1,14-3,8 26,0 24,0 2,65 -7,7 0,78 0,43 0,32 0,39-44,9 1,04 0,65 0,48 -37,5 6,50 4,59 1,82 0,83-29,4 7,80 5,45 2,02 -30,1 20,8 18,3 2,41 1,57-11,8 26,0 23,0 2,50 -11,5 6 ,/,/St So ,%0,36 0,37 0,04 0,04+2,8 0,48 0,48 0,06 0,0 3,00 3,18 0,12 0,06+6,0 3,60 3,83 0,12 +6,4 9,60 9,84
