1、:D 2896-15 STANDARD TEST METHOD FOR BASE NUMBER OF PETROLEUM PRODUCTS BY POTENTIOMETRIC PERCHLORIC ACID TITRATION 2016.():2887-16/ASTM :16.05.2016 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohoc
2、ken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Con
3、shohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except
4、for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 2896-15 1 :D 2896-15 1 D 2896;,.().1.1.1 .1.2 1 ASTM D02 ,D02.06 .1 2015.2016.1970.2011.D 2896-11.DOI:10.1520/D 2896-15.ASTM D 2896-15 2 .1 ,.1.3 2 ,.,.2.5.5 ,.1
5、.4,(),.2 ,16,17 19,1.1.5 300 /.19 300 /.1.6,.1.7 ,.,ASTM D 2896-15 3 .7,10 2.2.2.2.1 ASTM:2D 1193 3.3.1:3.1.1 ,.4.4.1 ,.,.,.4.2 120 .2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 2896-15 4 60 .,.,.4.3 ,.5.5.1 ,.,.;.6.6.1 ,.6.2 ,0 11,.6.3 ,/(Ag/AgCl),10.(.19.1)3 ,AST
6、M D 2896-15 5 ,/.,.;,.6.4,.,.,.6.5,10 20,0,05 0,02,.6.6 ,.6.6.1 250 300.150,60 .4 .6.7 ,.,ASTM D 2896-15 6 .5 ,().7.7.1 .,37.2 ,I,II III D 1193.,.,7.3 ,().7.4 ().7.5 ().3 Reagent Chemicals Society Specifications,American Chemical Society,Washington,DC.,.Analar Standards for Laboratory Chemicals,BDH
7、Ltd,Poole,Dorset,U.K.,and United States Pharmacopeia and National Formulary,U.S.Pharmaceutical Convention,Inc.(USPC),Rockville,MD.ASTM D 2896-15 7 7.6 ,(0,1 N)4(.,)8,5 70%-72%(HClO4,70%-72%)(10,2 60%-62%HClO4)500 30 (35 60%-62%HClO4 6 ,.).1 .24.7.7 (KHC8H4O47.8 (.,).(NaClO).4).NaClO47.9 .7.10 ,(Na2C
8、O37.11 ,0,1 N (,.16 17)5,3 Na).2CO3 4 .300 .1 ASTM D 2896-15 8 .8.8.1 (HlO48.1.1 (120)120 2 .0,1 0,2 ,0,1,40 .80 ,HlO),:48.1.2 (60)120 2 .0,05 0,1 ,0,1,20 .40 ,HlO 0,1 N,10.1 10.4 11.4 11.7.,(.14.2).40 80 (.11.8).48.1.3 ,N 0,1 N 8.1.1.20 40 (.11.8).A,HlO4N :A(1)=1000W/204,23 (V b):ASTM D 2896-15 9 W
9、-,V-HlO4b-,V ,.,7 HlO48.2 (Na ,5.5 1 (t 0,001).5 ,1+(t 0,001),t ,.2CO38.2.1 (120)120 8,00 HClO),:4 0,1 N.0,1 N,10.1 10.4 11.4 11.7.,(.14.2).,NN,:=(8,00 b)NA(2)/G:b-,V ,NA-HlO4G-,.,8.2.2 (60)60 4 HClO4 0,1 N.8.2.1.,N,:ASTM D 2896-15 10 N=(4,00 b)NA(3)/G:b-,V ,NA-HlO4G-,.,9.9.1 ,.,.8 ,.10.10.1 ,KCl,()
10、NaClO4.NaClO4 .ASTM D 2896-15 11 .,NaClO4,.,.,NaClO410.2 -,:,.10.2.1 100 0,2 844 .100 1,5 HClO410.2.2 60 0,1 0,1 N.0,3.844 .50 0,75 HClO4 9 .4 .0,1 N.0,3.10.3 ,ASTM D 2896-15 12 .:,.NaClO410.4 ,(),5 ,.10.2.NaClO,.,.,.4.,.,.11.(120)11.1 ,BN,:ASTM D 2896-15 13 ,=28/BN(4)10 (.16.2),.11.1.1 ,.20.,10 20
11、0,05 5 10 0,02 1 5 0,005 0,25 1,0 0,001 0,1 0,25 0,0005 11.2 120 .11.3 .11 ,80 ,40 .,.11.4 10.1,10.2 10.3.,.,.,700.,.1,5 .ASTM D 2896-15 14 11.5 HClO411.6:0,1 N ,.().11.6.1 ,(.12),.(),0,1 0,03 (0,5 ),0,05.(),0,1 0,03,0,03.,0,005 (0,1 )0,1.12 ,0,005/.11.6.2 1,0/.11.7 ,(.10.3).(.10.1).ASTM D 2896-15 1
12、5 11.8 ,120 .HClO4 0,1 N 0,05,.11.6.2.12.(60)12.1 ,:,=10/BN(5)13 (.17.2).12.1.1 ,.10.,5 10 0,02 1 5 0,005 0,25 1,0 0,001 0,1 0,25 0,0005 14 ,.12.2 60 .12.3 .15 ,40 ,20 .ASTM D 2896-15 16 12.4 10.1,10.2 10.3.,.,.,700.,.1,5 .12.5 HClO412.6:0,1 N ,.().12.6.1 ,(.12),.(),0,1 0,03 (0,5 ),0,05.(),0,1 0,03,
13、0,03.,0,005 (ASTM D 2896-15 17 0,1 )0,1.12.6.2 1,0/.12.7 (.10.3).(.10.1).12.8 ,60 .HClO4 0,1 N 0,05,.12.6.2.13.13.1 ,(QC).,.QC 5 5 AST M MNL,3,6,ASTM International,W.Conshohocken,PA.QC ,.QC,ASTM D 2896-15 18 .,QC ,QC.QC ,.16 QC,QC .14.14.1 .14.2 ,.,.,.,50/0,1 .14.3 ,16 17.,14.2.14.4 ,BN,:BN,KOH/=(E
14、F)NA(6)56,1/S:ASTM D 2896-15 19 E-HClO4F-,NA-HClO4S-,.,15.15.1 :(D 2896 )=(7),2.,2.4.15.2 100 0,1 /,100 1 /.16.,(120)16.1 11 .,.HClO4,HClO416.2 ,11.1.(.17).ASTM D 2896-15 20 17 5.5 ,3 .,(.19.2),5 .16.3 80 40 .16.4 8,00 HClO4 0,1 N.(HClO4 .,8,00 HClO416.5 2.(16.7).16.6 HClO416.7 16.6,11.1 11.6.2,5 (.
15、17).,HClO 0,1 N.,11.0 100.4,16.6.(8.2.1)HClO16.8 ,BN,:4.ASTM D 2896-15 21 BN,/=(G H)NB(8)56,1/S:G-,(.8.2.1 8.2.2),NBH-,-,S-,.17.,(60)17.1 12 .,.HClO4,HClO417.2 ,12.1.(.18).18 2,5.2,5 ,1,5 .17.3 40 20 .17.4 4,00 HClO4 0,1 N.(HClO4 .,ASTM D 2896-15 22 ,4,00 HClO417.5 2.(17.7).17.6 HClO417.7 17.6,12.1
16、12.6.2,2,5 (.18).,HClO 0,1 N.,12.0 100.4,17.6.(8.2.2)HClO17.8 16.8.4.18.18.1 :(D 2896 )=19.6 19.1 7 6 -ASTM International RR:D02-1011 RR:D02-1237.,7 .1 ,17.ASTM D 2896-15 23 ,/,.1.T 1 ,/0,004*0,013X*X:X ,19.2 (120):19.2.1 ,(.15 .17):19.2.1.1 ,:,3 ,24 19 1986.,1972.ASTM D 2896-15 24 .19.2.1.2 ,:,7 ,32 20 ,1.19.2.2 ,.19.3 (60):19.3.1 ,(.15 .17):19.3.1.1 ,:ASTM D 2896-15 25 ,5 19.3.1.2 ,:,7 19.2.2 ,.20.20.1 ;ASTM D 2896-15 26 ()1.1.1 ()(),.,.1.2,:1.2.1 6 70.1.2.2 5 300.1.2.3 ,5 27.2.2.1 .,.,;ASTM D
