1、 D4084-07(2017.)STANDARD TEST METHOD FOR ANALYSIS OF HYDROGEN SULFIDE IN GASEOUS FUELS(LEAD ACETATE REACTION RATE METHOD)2018 ():15.08.2018:3520-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohock
2、en,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Cons
3、hohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except f
4、or ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D4084-07(2017)1 D4084-07(2017.)1 D4084;,.().1.1.1 (H2S).H2S ,(LPG),.,.0,1 16 (.)(0,1 1 ASTM D03 ,D03.05 .1 2017.2017.1981.2012.D4084-07(2012).DOI:10.1520/D4084-07R1
5、7.ASTM D4084-07(2017)2 22/3)100%H2S .1.2 ,.,.1.3 -,(TBT).2.2.1 ASTM:2 D1193 D1914 ,D2420 (LP)()D3609 D7166 E2165 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM ASTM D4084-07(2017)3 ,(2007.)3 3.3.1 H2S .H2S ,.H2S ,H2S .,.E dE/dt ,H2S .4.4.1 /H2S.H2S .D7166 ,.3 .www.astm.org.
6、ASTM D4084-07(2017)4 5.5.1 10 (.1),.0,1 0,5 100%-H2S.,.1 5.2 ,8/(1./)1/70 (10,15 .).,(PTFE).,.-ASTM D4084-07(2017)5 .2 H2S,5.3 ,-(LPG)ASTM D4084-07(2017)6 H2S 0,1 (.2).5.4,1 10 1 M.,(DCS).6.1 :,.,.,.,.6.1 50 (CH3COOH)1 5%-.II,D1193,1/.6.2 :6.2.1 99,5%-.H2S ,.H2S,.H2S,.,ASTM D4084-07(2017)7 ().6.2.2
7、.,.,10 .,.6.2.3 H2S ,.-,.,H2S ,H2S.-,.H2S,H2S 99,5%,.6.2.3.1 ,NIST NMi.6.2.3.2 ,()ASTM D4084-07(2017)8 .6.3 D2420 ,H2S.,.,/.6.4 ,.-,.6.4.1 0,1C.6.4.2 -2.6.4.3 0,01 ,S NIST .D3609.,10%,.,/ASTM D4084-07(2017)9 .7.7.1-H2S ,.,.,.,.,.H2S .H2S .-,.-H2S .2 ,.10 (1/3.),1.ASTM D4084-07(2017)10 H2S (.X1 ).,.1
8、1.8.8.1 ,.8/(1./).:.,1/.,12.1.,-H2S.9.9.1 .D3609.,ASTM D4084-07(2017)11,C 12.1.,.,.10.10.1 .10.1.1 .24 .,.,/,24./(QA/QC)/./24.ASTM D4084-07(2017)12 ,.10.2 ,9.1,.,13.10.3 ,.10.4 .10.5 (QA),.10.5.1 /(QA/QC).H2S ,13 .ASTM D4084-07(2017)13 .10.5.2 /(QA/QC).,13.10.5.3 ().,.10.5.4 .,.ASTM D4084-07(2017)14
9、 10.6 8/,.,A,.12.1.11.2.,(12.1).,11.2,.,11.2.25%,-.11.11.1 (),.11.2 ,H2S,D,.,V,H2S(),10.H2S.H2S .H2S .ASTM D4084-07(2017)15 ,.,H2S,10,:V=0,01D:V-H2S,D-H2S ,.11.2.1 10 ,D,-0,1,V,H2S ,10.,.11.3 ,10 ,:(1)V*-,H2S,P-H2S ,.11.3.1 10 ,D,-0,1,V*,100000 H2S ,P,10.,.ASTM D4084-07(2017)16 11.4 E2165 ISO 10725.
10、11.4.1 H2S ,.11.4.2 H2S H2S,:(1)H2S,(2)H2S,(3).11.4.3 H2S H2S,H2S,:(1)H2S ,(2),(3).H2S ,.11.4.4 H2S,:(1),(2)-,(3).,.ASTM D4084-07(2017)17 11.4.5 H2S .H2S.7.1.-H2S H2S.H2S./(QA/QC).12.12.1 :X=(A B)D/(C B):A-,-,-,D-H2S ,X-H2S .12.2 W (/.)25C ASTM D4084-07(2017)18 760 .(101,3)24,450 D1914.H2S:W=1,394 X
11、:W-,/3,X-H2S ,.12.2.1 .13.13.1 :.3 13.1.1 ,H2S (),ASTM D4084-07(2017)19 ,.3.13.1.2 ,.3.14.14.1 ;()X1.X1.1 ,.X2.X2.1 ,(QC).X2.2 QC(.D6299,D6792 MNL 7).X2.3 QC (.D6299,D6792 MNL 7).ASTM D4084-07(2017)20 ().,.X2.4 ,QC ,.QC ,QC .QC ASTM.X2.5,QC ,.QC,.QC .D6299,D6792 MNL 7.X3.X3.1 NIST,NMi .SRM NIST NMi,
12、NTRM .ASTM D4084-07(2017)21 .X3.1.1 ASTM D4084.(%RSD),.X3.1.2 ,.SRM NTRM,NIST NMi.X3.2 ,48.2%,.,.X3.3 :X3.3.1 (.X3.2).X3.3.2 ,SRM/NTRM NIST NMi,.ASTM D4084-07(2017)22 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.