1、 D 277713 ,D19 STANDARD PRACTICE FOR DETERMINATION OF PRECISION AND BIAS OF APPLICABLE TEST METHODS OF COMMITTEE D19 ON WATER 2014 ():2394-14/ASTM :25.06.2014 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,We
2、st Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Dr
3、ive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any P
4、arty,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 2777-13 1 D 277713 ,D19 1 D 2777;,.().1.1.1 ,D19 .ASTM,A21.().1.2 ,1.4,1.5 1.6,1 ASTM D19 ,D19.02 ,.1 2013.2013.1969.2002.D 2777-12.DOI:10.1520/D2777
5、-13.ASTM D 2777-13 2 ,(,).1.3 (),.,.1.3.1 .,.1.3.2 ,(,),7.1-7.5,.,.1.3.3 .ASTM D 2777-13 31.4 -,.1.4.1 ,D19.24 -.,.1.4.2 -,.,(),(.7.2.5.2(3).1.4.3 ,().1.4.4 .1.5 ,.,ASTM D 2777-13 4,.1.6 ,1.4 1.5.D19,-,ASTM(1)2,.,D19 .5.,.D2777.,D19.1.7 A21.2.3 ASTM ,().,ASTM D 2777-13 5 7.6.1.8 12 :(1),(2),(3),ASTM
6、.1.9 ,1.4 1.8,-(.8),(.13).1.10 (QC),D 5847.1.11 ,.-.2.2.1 ASTM:2 D 1129,2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 2777-13 6D 1141 D 1193 D 4375 D19 D 5790 ,/-D 5847 D 5905 D 6091 99%-(IDE),.D 6512 E 177 ASTM E 178 E 456,E 691 E 1169 2.2 ASTM:DQCALC Microsoft Exc
7、el (IQE)3 3 -ASTM International ADJDQ-CALC.2007.ASTM D 2777-13 73.3.1 ,.D 1129,D 4375 456,177.3.2 ,:3.2.1 ,.3.2.2 .3.2.3 ,.3.2.4 ,/.3.2.5 ,.3.2.5.1 ,.3.2.6 ,D2777 ,.3.2.7 ,ASTM D 2777-13 8 .3.2.7.1 ,.3.2.8 ,.3.2.8.1 ,.3.2.9 ,(),.3.3 3.3.1 MDL .4.4.1 ,.-,1.4,1.5 1.6,.ASTM D 2777-13 9 .,.,-.ASTM.;,.,(
8、)-ASTM,.4.1.1 .1.1 A .4.1.2 ,.3,6.0.4.1.3 ,.ASTM D 2777-13 105.5.1 ,.,.,().5.2 ,.,.,.5.3 ,.6.6.1 (2,3).,ASTM D 2777-13 11,.,(4)(.9.3 9.4).,(.E 1169).6.2 ,.6.3 ,D 6091()D 6512(),.(,),(,MDL ).6.3.1 :6.3.1.1 I .ASTM D 2777-13 12.,;.6.3.1.2 II .,I,.7.7.1 ,.,.,.,.7.2 :7.2.1 ,.,.,ASTM D 2777-13 13,.s().,(
9、sT),(so).7.2.2,.,.,D1129.7.2.3 ,(.10.3),.,.,.ASTM D 2777-13 147.2.4 ,(.1.4.2),8,().7.2.5 ,.7.2.5.1 ,D 1193,D 5905,D 1141,.,;,(),.,.7.2.5.2 ,.,(),ASTM D 2777-13 15 .,.,(NIST).,.(1)(),.(2),.(3),1.4.2,.,.,.7.2.5.3 .7.2.5.4 ,ASTM D 2777-13 167.2.5.1 7.2.5.2 ,-,10 ;.,.7.2.6 ,(5)(.),.,.,(,)(),(IDE).,ASTM
10、D 2777-13 17 IQE.,.1 ,.7.2.6.1 ,.,.(.).1/3 ,/,.ASTM D 2777-13 18 (),.7.2.7 ,.7.2.7.1 ,.7.2.8 ,.7.2.9 (,),.7.3 :7.3.1 ,D19,.,1.6.(,),.ASTM D 2777-13 19 ,20%;.,.7.3.2 ,;(Youden)(Steiner)(6).,.(7)(8),.7.3.3,-.,11 2.7.4 :7.4.1 (.D 1129 E 177).E 177,ASTM D 2777-13 20 ,.,.().7.4.2 /.()(.).7.4.3 ,:(1),(2),
11、(3)(9).(,0,5,1,1,5,2,2,5).,.7.4.4 .,(.)().,(),ASTM D 2777-13 21 ,.,.7.5 :7.5.1,-,;,.7.5.2 /,7.5.1,.7.6 ,(.1.6)7.1 7.5,.7.6.1 .,.7.6.2 ASTM D 2777-13 22 ,.7.6.3 .7.6.4 ,.7.6.5 .,.,().,/.,(),D 2777,.(/).7.6.6 .,.7.7 ,(.1.3),.,ASTM D 2777-13 23,.7.7.1 ,7.1 7.5,.7.7.1.1 ,.7.7.1.2 ,7.2.5.7.7.1.3 (),.,.,.
12、7.7.1.4 ,(),.,.,-,.7.7.2 ,ASTM D 2777-13 24,.,.7.7.2.1 ,.7.7.2.2 ,7.2.5.7.7.2.3 (),.,.,.7.7.3 .,.8.8.1 (),:(1)(ASTM );(2),;(3)7.3.1;(4),;(5);(6)ASTM D 2777-13 25;(7)QC-,;(8);(9),.-.8.1.1 1(.1.1).8.2 -,.8.3 -().9.9.1 ,(1);(2)();(3)().9.1.1 ,ASTM D 2777-13 26.,.9.1.2 ,-,.,.9.1.3 ,3.9.2 ,.,(,.),.(1,5 .
13、).ASTM D 2777-13 27 .9.3 ,.(,),.,.9.4 ,:(1);(2);(3)();(4),;(5).9.4.1 ,.,.9.4.2 ,.ASTM D 2777-13 28 ,.9.4.3 ,.9.5 (),.().10.10.1 /,(1);(2),(.10.3);(3),(ASTM D 2777-13 29,);(4);(5),;(6).10.1.1 ,2.10.2 ,(10).(.,).,.10.2.1 ,.10.3 ,.,ASTM D 2777-13 30 ,.,.10.3.1 ,.10.3.2 ,-.E178.11.,11.1 ,:11.1.1 ,(so),(
14、Youden),:ASTM D 2777-13 31(1):m-,Di-,i-,i-,D-m-Di.2 Di (),-.11.1.2 so :(2)m 11.2 (x)(sT)11.2.1 ,xi,i 1 n.(x)(sT),:ASTM D 2777-13 32(3)(4)11.2.2 ()(),(x1i+x2i)/2 xi,x1i x2i ,i-.sT ,.:(5)so 11.1.2.11.3 11.1 ,.11.4 11.4.1 (7.4).(,ASTM D 2777-13 33),.11.4.2 ,:(%)=100(x b c)/c(6):x-,-,b-().11.4.3 ,.-.11.
15、4.4,(1.6),E691.,E691.-.11.4.5,ASTM D 2777-13 34 ,E 691.12.12.1 :12.1.1 .,D 2777,.12.1.1.1 ,.,.12.1.2 ,.12.1.3 ,ASTM D 2777-13 35 (c),():(1)(X),(2)%c,(3)(sT).,(so),.,()sT so (+).,.,(.x ).,-ASTM.,.12.1.4 ,ASTM D 2777-13 36 .,.,().,.12.1.5 ,12.1.3,.,;,./,.,p-,.12.2 ,ASTM D 2777-13 37,1.4,1.5 1.6,.D19 -
16、,.12.3 :12.3.1 ,:12.3.1.1 D XXXX (),.12.4 ,:12.4.1 ,ASTM,:12.4.1.1 ()().12.5 ,(IDE),ASTM D 2777-13 38 ,.DQCALC,ASTM,.12.6 ,IQE-(),%(,10%,20%,30%,),.DQCALC,ASTM,.13.13.1 -,/:13.1.1 ,.13.1.2 .3 DQCALC ,.13.1.3 .13.1.4 ,.13.1.5,.13.1.6 (,ASTM D 2777-13 39,.),.,.13.1.7 .13.1.8 ,(,-).13.1.9 ,-,ASTM ().13.2 ,:,-ASTM RR:D_.14.14.1 ;ASTM D 2777-13 40()X1.X1.1 D 5790,524.2 USEPA,-,.X1.1 .1.1 :.ASTM D 2777-13 41X2.X2.1 ,.X2.2 .X2.1 10.2.,-.X2.1.,/5 0,88 3 1,10 8 4,41 6 5,29 7 17,64 4 22,051 1,08 1,24 4,45
