1、 D 4309 02(2007)-STANDARD PRACTICE FOR SAMPLE DIGESTION USING CLOSED VESSEL MICROWAVE HEATING TECHNIQUE FOR THE DETERMINATION OF TOTAL METALS IN WATER 2008.:0862-08/ASTM :10.01.2008 NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM Internat
2、ional(www.astm.org)for the latest information.-,.9,-49,-1,119991.:(495)236-54-49,236-43-83:(495)230-13-72 E-mail:interstgost.ru Web:www.interstandart.ru ()(ASTM)100 Harbor Drive,West Conshohocken,PA 19428,USA.ASTM ,ASTM,.,ASTM ().This translation has been made by Federal agency on technical regulati
3、ng and metrology(Interstandard)under license from the American Society for Testing and Materials(ASTM),100 Barr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM has neither approved nor endorsed this translation,and in all cases only the English edition as published and copyrighted by ASTM shall be
4、considered as the official version.Reproduction of this translation by parties other then Federal agency on technical regulating and metrology of Russia(Interstandard)or ASTM is strictly forbidden under U.S.and international copyright laws.NOTICE:This standard has either been superseded and replaced
5、 by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4309-02(2007)1 D 4309 02(2007)-1 D 4309;,.()1 1.1 ()(-).,.1.2 .,1 ASTM D19 D19.05 .15 2007.2007.1991.2002.D 4309-02.1 NOTICE:This standard has either been superseded and replaced by a new v
6、ersion or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4309-02(2007)2.1.3 ,ASTM:D 857,D 858,D 1068,D 1192,D 1687,D 1688,D 1691,D 1886,D 3370,D 3557,D 3559,D 3919,D 4190,D 4453,D 4691.1.4 ,.,.9.2.2.1 ASTM:2 D 857 D 858 D 1068 D 1129,D 1192 3 2 ASTM,ASTM ww
7、w.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM 3 NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4309-02(2007)3D 1193 D 1687 D 1688 D 1691 D 1886 D 3370 D 3557 D 355
8、9 D 3856 ,D 3919 -D 4190 -D 4453 D 4691 -2.2 :4 CFR 1.030.10,21 2.3 ():4 ,47,18 2.4 U.S.EPA():5 U.S.EPA:1979.,4.1.3,.6 4 ,U.S.Government Printing Office,Washington,DC 20401.5 (NTIS),5285 Port Royal Rd.,Springfield,VA 22161,http:/www.ntis.gov.NOTICE:This standard has either been superseded and replac
9、ed by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4309-02(2007)4 U.S.EPA:SW 846,3015 3.3.1 ,.D 1129.4.4.1 (-).,-(),(),(),-().5.5.1 -,-,-,.-NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasec
10、ontact ASTM International(www.astm.org)for the latest information.ASTM D 4309-02(2007)5 .6.6.1 -.6.2 ,.6.3 ,.7.7.1 -,575 1000.1%1.2,8 3/(100./).,1 14 ,.,200C,/,100/.7.1.1 NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.a
11、stm.org)for the latest information.ASTM D 4309-02(2007)6 ,(CFR)1030.10,(C)(1),(C)(2),(C)(3).(),18.7.2 ,100 .100/.200C.(),.7.3,.8.8.1 .,.6 ,.8.2 ,6 ,Am.Chemical Soc.,Washington,DC.,.,BDH Ltd.,Poole,Dorset,U.K.,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.NOTICE:This standard has either been s
12、uperseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4309-02(2007)7 D 1193,I.,.II ,1.8.3 (.1,19)(HCl).8.4 (.1,42)(HNO3).8.5 (1+1)1 HNO3(.1,42)1 .9.9.1 ,.,.,.9.2 ,.10.10.1 7-12:1 ,.10.2.10.1.1 ,A1.10.1.2 ASTM (,D 3856),-N
13、OTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4309-02(2007)8.10.1.3 50,0 (.2).,3 HNO3(.1,42)2 HCl(.1,19).,5 HNO3(.1,42)(.3).,.,.2 ,.3 9%.,.,.10.1.4 .10.1.3 ,12.12,50 ,.,660,.,.
14、4 ,50 .NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4309-02(2007)910.1.5 .,360.10.1.6 ,575-635,50 100%.,635 to 700,30 100%.164 4C(.1).,700,.1.10.1.7 .,.5 :,-,.10.1.8 .().,0,5
15、,.,10%-(.6).,.NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4309-02(2007)10.1 12,50 H2O,3 HNO3(.1,42),2 HCl(.1,19)6 ,(10%);,-.10.1.9 ,.55 (.3).7 ,.10.1.10 ,.10.2 1-6:10.2.1 ,(
16、.)(C)683 100%578 100%NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)for the latest information.ASTM D 4309-02(2007)11 A2.10.2.2 ASTM ,-.10.2.3 50,0 (.2).,3 HNO3(.1,42)2 HCl(.1,19).,5 HNO3(.1,42)(.3).,.,.10.2.4 .10.2.3 ,6 .6,50 ,.,660,.,(.4).10.2.5 .,360.10.2.6 ,575-635,30 NOTICE:This standard has either been superseded and replaced by a new version or withdrawn.Pleasecontact ASTM International(www.astm.org)
