1、 D328085(2014.)STANDARD TEST METHODS FOR ANALYSIS OF WHITE ZINC PIGMENTS 2018 ():19.07.2018:3491-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM Interna
2、tional.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does no
3、t approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,
4、is strictly forbidden according to the USA legislation and international copyright.ASTM D3280-85(2014)1 D328085(2014.)1 D3280;,.()1.1.1 .1.2 :6 7 8 9 10 11 1 ASTM D01 ,D01.31 .1 2014.2014.1973.2009.D3280-85(2009).DOI:10.1520/D3280-85R14.ASTM D3280-85(2014)2 ,12 13 14 15 16 17 18 19 20 21 22 23 1.3,.
5、1.4 ,.,.2.2.1 ASTM:2 D280 (,)D1193 D1394 E11 C 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D3280-85(2014)3 3.3.1 :3.1.1 .3.1.2 BaSO4 .3.1.3 A D280.3.2 ,:3.2.1 PbSO4 PbO.3.2.2 13.2.1 ,7 8.3.2.3 BaSO4 SO3.3.2.4 .3.2.5 A D280.3.2.6 .3.3 :3.3.1 9.3.3.2 8 9 ZnO ZnS.3.3.3
6、 18.ASTM D3280-85(2014)4 3.3.4 A D280.3.3.5 H2SO4 Na2CO3,BaCO3 NCl (NH4)2SO4 BaSO4,.3.3.6 D1394.4.4.1 ,.,.5.5.1 .,.3 ,.3 ,DC.,.,BDH Ltd.,Inc.(USPC),.ASTM D3280-85(2014)5 5.2 ,II D1193.5.3 :5.3.1 ,:,HC2H3O2 99,5%,HCl.1,19 ,HF 48%,HNO3.1,42 ,H2SO4.1,84 ,NH4OH.0,90 .5.3.2 ,:HCl(1+99)1 HCl(.1,19),99 .6.
7、6.1 ,.,.ASTM D3280-85(2014)6 6.2 ,180-(80)(1),105C.1 E11.6.3 .7.7.1:7.1.1 (10/)1 100 H2SO4.7.1.2 (1 =0,008 Zn)35 K4Fe(CN)63H2O ,1 0,3 (K3Fe(CN)6).(320-340),.7.2.,1,00 .7.2 0,4 0,1 400-.20 15 HCl.NH4OH,.15 H2SO4(1+2)200.60C,2 K4Fe(CN)6 -.2 -.-ASTM D3280-85(2014)7 K4Fe(CN)6.0,5-1,0 ,.,-.7.3 ZnO,A,:(1)
8、:V2-K4Fe(CN)6,Z-,K4Fe(CN)6,/,S1-,1.245-ZnO(81,38)/Zn(65,38).8.8.1:8.1.1 (50/)5 UO2(C2H3O2)22H2O 100 .8.1.2 ,(1 =0,008 Zn),.7.1.2.,:(1):Z-,K4Fe(CN)6,/,W-,V-K4Fe(CN)6,B-K4Fe(CN)6,.ASTM D3280-85(2014)8 8.2:8.2.1 0,4 0,1 400-.20 ,10 HCl.NH4OH .HCl ,3.250 .K4Fe(CN)6 ,1.8.2.2 .8.3 ZnO,A,:(3):V-K4Fe(CN)6,S
9、-,1,245-ZnO(81,38)/Zn(65,38).9.9.1 ,A,:(4):L-PbO,%,Z1-ZnO,%,S5-SO3,%.ASTM D3280-85(2014)9 10.10.1:10.1.1 ().10.1.2 .10.1.3 (100 BaCl2)117 BaCl22H2O 1.10.2:10.2.1 10 0,1 400-.50 ,100 35 HCl.,3-5 .,.10.2.2 300 ,NH4OH 6 HCl.25 BaCl2 .2.10.2.3 .30.BaSO4.10.3 ,A,:(5):P-BaSO4,S2-,0,1374-(32,064)/BaSO4(233
10、,43).ASTM D3280-85(2014)10 11.11.1 A D280.,12.12.1:12.1.1 0,5 0,1 400-.250 20 HNO3(2).5 H2SO4 .,50 95%200 1-2.H2SO4(1+99).,40%,(13).3 ,H2S HCl,NH4OH .PbS ZnS HNO3 ,.12.1.2 -(550 50C)20,.12.2 PbO,A,:(6):P1-PbSO4,S3-,0,736-PbO(223,21)/PbSO4(303,28).ASTM D3280-85(2014)11 13.13.1 .7.1 8.1,.13.2:13.2.1 ,
11、40%,.12.1.1.,40%,1 0,1,PbSO4,.12.1.1,.13.2.2 ,7 8.14.14.1 .10.1.3.14.2:14.2.1 1 0,1 400-.10 ,3 NH4Cl,5 HCl .15.50 ,Na2CO3.10-15.,250 ,.14.2.2 HCl,.5 HCl.10 15.NH4OH 6 HCl.25 BaCl2 .2.14.2.3 .ASTM D3280-85(2014)12 30.14.3 SO3,A,:(7):P2-BaSO4,S4-,0,343-SO3(80,07)/BaSO4(233,43).15.15.1 ,A,:(8):L-PbO,%,
12、Z1-ZnO,%,S5-SO3,%.16.16.1 A D280.17.17.1:17.1.1 5 0,1 500-.250 10.,ASTM D3280-85(2014)13 .17.1.2 400 105 2C,.17.1.3 .17.2 ,W,:(9):R-,B2-,S5-,.18.18.1 .8.1.18.2:18.2.1 5 1 500-200 (3+97).20 500-.18.2.2 400 600-.20 HCl NH4OH,.HCl ASTM D3280-85(2014)14 3.K4Fe(CN)6,.8.2.18.3 ,A,:(10):V3-K4Fe(CN)6,B3-K4F
13、e(CN)6,Z-,K4Fe(CN)6,/,S6-,1,245-ZnO(81,38)/Zn(65,38).19.19.1 .7 8,.19.2 0,1 400-.,10 H2SO4(1+1).,.7.2 8.2.19.3 ,C,:(11):V4-K4Fe(CN)6,ASTM D3280-85(2014)15 B4-K4Fe(CN)6,Z-,K4Fe(CN)6,/,S7-,A-(18),1,20-ZnO ZnS 1,491-ZnS(97,44)/Zn(65,38).20.20.1 ,17.21.21.1 A D280.22.22.1:22.1.1 (30/)30 (NH4)2SO4 1.22.1
14、.2 0,1 100 .22.1.3 (2/)2 Na2CO3 1.22.2:22.2.1 1 1 400-.,100 H2SO4(1+1).,200 ASTM D3280-85(2014)16 .15.22.2.2 .,6 Na2CO3 .2 Na2CO3 40 .200 400-.Na2CO3.22.2.3 BaCO3 HCl(1+4),600-.NH4OH,.HCl 6.400,25 (NH4)2SO4 .4.22.2.4 .,30,.22.3 (BaSO4),A,:(12):P3-BaSO4,S8-,.23.23.1 9-13 D1394.TiO2 ,ASTM D3280-85(2014)17 ,D1394,.24.24.1;ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.
