1、:D1159-07(2017.):130/98 STANDARD TEST METHOD FOR BROMINE NUMBERS OF PETROLEUM DISTILLATES AND COMMERCIAL ALIPHATIC OLEFINS BY ELECTROMETRIC TITRATION 2017 ():07.09.2017:3262-17/ASTM -,.9,-49,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)10
2、0 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM Internatio
3、nal)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified t
4、ranslations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D1159-07(2017)1 :D1159-07(2017.):130/98 1 D1159;,.().1.1.1 2 :1.1.1 ,90%-(D86)327 (626 F).(,1 ASTM D02 ,D02.06 .IP .1 2017.2017.195
5、1.2012.D1159-07(2012).DOI:10.1520/D1159-07R17.2 Dubois,H.D.,and Skoog,D.A.,“Determination of Bromine Addition Numbers,”Analytical Chemistry,Vol 20,1948,pp.624627.ASTM D1159-07(2017)2),:90%-,(F),.2 205(400)175 205 327(400 626)10 1.1.2 ,95 165(.1).,.-.1 .1.2 ,;1.1.3 1,0 ,D2710.0,5,D2710 .D1492 D5776 .
6、1000 .1.4,.1.4.1 ASTM D1159-07(2017)3.1.5 ,.,.7,8 9.1.6 -,(TBT).2.2.1 ASTM:3 D86 D1193 D1492 D2710 D5776 3 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D1159-07(2017)4 3.3.1 ,:3.1.1 ,100 .4.4.1 ,(.8.1)0 5 (32 F 41 F),-.5.5.1 .,2,315 (600 F).5.2 .6.6.1 ,(.2),0,8,ASTM D1
7、159-07(2017)5 50 ,.,-.2 ,.6.2 120 45 ,0 5 (32 F 41 F).6.3 .6.4 12 1 .5 55 .65%.6.5 ,0,5 .7.7.1 .,(ACS)4,.,4“Reagent Chemicals,American Chemical Society Specifications”,Am.Chemical Soc.,Washington,DC.,.”Annual Standards for Laboratory Chemicals,”BDH Ltd.,Poole,Dorset,U.K.,and the United States Pharma
8、copeia,and National Formulary,U.S.Pharmacopeial Convention,Inc.,(USPC),Rockville,MD.ASTM D1159-07(2017)6 .7.2 ,III,D1193.7.3 (,-,.,.)7.4-,(0,2500 Br2)51,0 (KBr)13,92 (KBrO3)(105 (220 F)30)1.7.4.1 ,8,.:7.4.1.1 50 1 (-,.,1,19)500-.10 10 5 0,01 -1 2 .,5 KI .5 ASTM D1159-07(2017)7 KI ,.,100 ,(Na2S2O3).1
9、 .-:)2)(5(21AMM(1):1-,Br2,-Na2S2O3,-,2-Na2S2O3,5-,2-,-.,0,002.7.5 (.)7.6 (150/)150 (KI)1.7.7 ,(0,1)25 (Na2S2O352)0,1 (Na2CO3).1,.,0,0002.ASTM D1159-07(2017)8 ,0,0005.7.8 5 3 5 .,0,65 .500 5 10.().7.9 (1+5)1 (H2SO4,.1,84)5 .(-,.)7.10 1 :714 ,134 1,1,1-(),134 18 H2SO4(1+5).7.11 1,1,1-(.).7.12 (1,1,1-,
10、.1,1,1-,ASTM International .D02.04.)3 .ASTM D1159-07(2017)9 8.8.1 ,.(:1,1,1-.,.,().9,0,6 1 (.1)6 10 10%1,1,1-.().8.2 ,:,(.7.4.1,9.3 8.1)187 199(.9.5),10%-18 20,(.7.4.1,8.3 8.1)136 144(.9.5),10%-13 15 ,.1.194,6 142,4.1.,20,/,D 20 82,5 83,5 0,8100 1,4465 101 102,5 0,7175 0,0015 1,4112 2,4,4-1-.ASTM D1
11、159-07(2017)10 8.3 5,:8.3.1 65 ,75 150 (100 200),6,16 760,.100-,30:1.,.8.3.2 30 .,.10 10,.20.(,2 10%,.)9.9.1 10 1,1,1-50-5 13019()2125(),Eastman,Rochester,NY.,-ASTM International.1,.6 923,W.R.Grace and Company,Davison Chemical Division,Baltimore,MD 21203.,-ASTM International.1,.ASTM D1159-07(2017)11
12、 .2.(1),.(,205 (400 F),).9.1.1 .,2-,.,.2.2.,0 10 10 20 20 50 50 100 100 150 150 200 20 16 10 8 5 4 2 1,5 1,0 0,8 0,8 0,6 9.1.2 20,-10,.;.9.2 0 5 (32 F 41 F),.9.3 110 ASTM D1159-07(2017)12 5-50-.,.9.4 .,6.1.9.5 -.,(.9.4)30.9.6 .9.3 9.5 ,5 (1,1,1-).0,1 -.0,1,.10.10.1 :=WMBA)98,15)()(1(2):-,-,ASTM D115
13、9-07(2017)13 ,1-Br2,W-,15,98-100 (Br2).11.7 11.1 ,:11.1.1 ,:90%-205 r=0,11(X0,70)(3)90%-205 327 r=0,11(X0,67)(4)-:r=3(5)11.1.2 ,7 (,90%-205)-ASTM International RR:D02-1290.ASTM Customer Service serviceastm.org.ASTM D1159-07(2017)14,:90%-205 R=0,72(X0,70)(6)90%-205 327 R=0,78(X0,67)(7)-8:R=12(8)11.2
14、,.4 1,1,1-.,1,1,1-.12.12.1 ;.8 ,.ASTM D1159-07(2017)15 ()1.1.1,100 .,.,.0.,.,.1.2 ,.,.1.3 ,.1.4 ASTM D1159-07(2017)16 .,.1.1.1.1.,%99,96B 0,0 0,0 0,0 2-99,88 0,0 0,0 0,1 c 0,0 0,1+0,1 99,94 0,0 0,0 0,0 2,2,4-99,96 0,0 0,1+0,1 1-99,7 228,0 208-20-2-99,91 228,0 235+7 1-99,80 189,9 181-9-2-99,83 189,9
15、189-1-2-99,87 189,9 189-1-3-99,94 189,9 193+3-3-189,9 191,4+1,5 1-99,8 162,8 136-27-2-99,85 162,8 163 0-3-99,80 162,8 163 0 1-99,7 142,4 132-10 2-142,4 139-3-4-99,84 142,4 149+7 1-99,89 114,1 111,4-2,7 1-99,9 95,1 82,9-12,2 1-99,8 87,7 81,4-6,3 1-99,7 81,4 70,8-10,6 1-99,8 76,0 62,9-13,1 1-99,84 71,
16、2 62,8-8,4 2-1-99,90 228,0 231,8+3,8 2-2-99,94 228,0 235 7 2,3-1-99,86 189,9 194+4 3,3-1-99,91 189,9 167-23 2-1-99,90 189,9 198+8 2,3-2-99,90 189,9 191+1 2-1-99,92 189,9 182-8 30-1-99,70 189,9 152-38 4-1-99,82 189,9 176-14 2-2-99,91 189,9 190 0 2-2-99,85 189,9 193,7+3,8 3-2-99,86 189,9 191+1 4-2-99,92 189,9 190 0 4-2-99,75 189,9 190 0 2,3,3-1-99,94 162,8 161-2 ASTM D1159-07(2017)17 1.1 ,%3-2-1-99,8 162,8 165,4+2,6 2,3-1-99,80 162,8 158,5-4,3 2,4-1-99,87 162,8 152,8-10,0 2,3-2-99,6 162,8 162,3-0,
