1、 D 12898(2014.)1 STANDARD TEST METHODS FOR ANALYSIS OF LUBRICATING GREASE 2016 ():2897-16/ASTM :26.05.2016 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,AST
2、M International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM Internationa
3、l does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Inters
4、tandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 128-98(2014)1 1 D 12898(2014.)1 1 D 128;,.().1 21.1 2015.1.1.1 ,.,(.),.1 ,.1 ASTM D02 ,D02.G0.01 .1 2014.2014.1922.2008.D 128-98(2008).DOI:10.1520/D0128-98R1401.ASTM D 128-98(2014)1 2 1.2 X1.,-,-,.1.3
5、:7 11 ,12 20 21 23 24 ()25 29 1.4,.1.5 ,.,.2.2.1 ASTM:2D 95 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 128-98(2014)1 3 D 156 ()D 217 D 445 ()D 473 D 804,D1078 D 1193 D 1353 ,3.3.1:3.1.1 ,-,.3.1.1.1 ,.3.1.2 ,-,.ASTM D 128-98(2014)1 4 3.1.3 ,.3.1.3.1 3 4 (NLGI),.3.
6、1.4 (,),.3.1.5 ,(),.3.1.5.1 ,.(,%).3.1.6 ,(),.3.1.6.1 ,.(),ASTM D 128-98(2014)1 5 .3.1.7 ,.3.1.7.1 ,.3.1.8 .3.1.8.1 .,.3.1.9 ,.3.1.9.1 ,.,.,.NLGI33.1.10-,.3.1.11 ,3 ,:4635 Wyandotte St.,Kansas City,MO 64112-1596.ASTM D 128-98(2014)1 6 -.D 804 3.1.12 NLGI .3.1.13 NLGI ,D 217.NLGI 3.1.14 (,),.NLGI 3.1
7、.15 ,.3.1.15.1 ,.3.1.16 ,().3.1.16.1 ,.3.1.17 ,.3.1.17.1 .;ASTM D 128-98(2014)1 7 .NLGI 3.1.18 ,.3.1.19 ,(),.3.1.20 ,(,).3.1.21 ,.3.1.22 ,.3.1.22.1 (,),(,),.:,.D 217 3.1.23 ,ASTM D 128-98(2014)1 8 ,.3.1.24 ,-,.3.1.24.1 ,.3.1.25 ,-,(),-.3.1.25.1 ,-(,).,.3.1.26 ,.4.4.1 .,.4.2 -,.ASTM D 128-98(2014)1 9
8、 2 ,.4,5,6 5.5.1 .,.75.2 ,D 1193,III.,.5.3 .(.)5.4 (50%)95%-8,9 4 Stanton,G.M.,NLGI,38,5,1974.,.153-165.(.5 Stanton,G.M.,NLGI,26-29 1975.6 Bonomo,F.S.Schmidt,J.J.E.,WADC 54-464,IV,1957.(,No.AD-130922).7 ,DC.,.,BDH Ltd.,Inc.(USPC),Rockville,MD.8 ,Formulas 1,23-A,30 35-A,368 ,.9 ,-ASTM International.1
9、,.ASTM D 128-98(2014)1 10.)NaOH NaOH KOH,.(,.).5.5 (NH4)2CO35.6 (0,02/)(.)-.(.,.).(.)5.7-,24C 25,5C(;).5.8 (CS25.9 .(.).(.100C .)5.10-,9,10 10 -,“Phillips Petroleum Co.”,Bartlesville,.1.(.)ASTM D 128-98(2014)1 11 1.-ASTM ,C 66,1 D 1078 ,C 68,9 D 1078 ,/100 0,001 D 1353 ,+30 D 156 A A 11/2 125 -,10 0
10、,5 KOH 50 50%-.7 750.0,5 HCl,.9,8 0,5 HCI.,E.5.11 (37%)(HCl).(.)5.12 ,(0,5)0,5 HCl.5.13 (10%),10%HCl ,0,5%.5.14 (1+3)HCl(37%).5.15 .(.)5.16 (1+4)(70%)(.).5.17 1,0 (ASTM D 128-98(2014)1 12 ,)50 ,5.4,5 NaOH KOH.5.18 (KHSO45.19 (KOH),(0,5)0,5 .(.).(.)5.20 (KIO45.21 (Na).(.)2CO35.22 (240/)240 (NaOH)(.)1
11、.).(.)5.23 ,(0,05)0,05 NaOH.5.24 (1+4)(H2SO45.25 (3+20)3 (95%)20 .95%).(.)5.26.(.)ASTM D 128-98(2014)1 13 6.6.1 (I II ,)8 30,.10 20 3,.6.2 ,0,1.7.7.1 .3 -.-Na2CO3,.,.,Na2CO3 K2CO3,.,CaCO3 CaO.,.ASTM D 128-98(2014)1 14 8.8.1 2 5 0,1.,.,.,.9.9.1 8.1 ,.,H2SO4(1+4)(.),.,.,.(.),.-,(NH4)2CO3()SO3.ASTM D 1
12、28-98(2014)1 15 .4 ,(8),.10.10.1 ,().,-.,.,.10.2 HNO3 (1+4)(.)HCl(1+3)(.),-.11.11.1 ,.ASTM D 128-98(2014)1 16 .1 ASTM D 128-98(2014)1 17 ,12.12.1,.,II,.I.(.1.)I 13.13.1 (.5)(.6),50 HCl(10%),.,(60C 63C,.6)-(.)(.),.120C ,(,.).5 ,ASTM D 128-98(2014)1 18 13,.6 ,60C 63C.14.14.1 ,14.2,14.3.,14.4.,14.5.14.
13、2 250 500 (.6),.20 -,50 HCl(10%).,.,3;,HC1,-.14.3 250-(.6).,-,50 -(;),50 -,2 (.)2 HCl(37%).-50 (.).ASTM D 128-98(2014)1 19,-24C 27C .,.,HCl(37%)1 ,.,.,10 15.-,.14.4 ,-.(,(.13),),.-,B,25-,HCl,A.A 20-C,(16).15 ,B.,0,5 KOH(.),(,),200 ASTM D 128-98(2014)1 20(.1,0 200 KOH).,0,5 KOH,.7 ,.1.14.5 63C ,-(.14
14、.5.1).A,.-B 25-,HCl,A.A 20-C,(.16).15 ,B.,63,0,5 KOH,200(.1,0 200 KOH).,0,5 KOH,.14.5.1(-,ASTM D 128-98(2014)1 21 .)14.6 14.4 14.5,0,5 1,0 .D .-E 30,25 20 50%,D.D 25 -,D -E.D ,HC1 50 25 F.F 20-,.F ,.(.),5-(.).14.7 ,:,ASTM D 128-98(2014)1 22,.14.8 ,.()-HCl(1+3),.14.9 ,(.23),15.15.15.1 ,15.1.1 15.1.6:
15、15.1.1 :A=56,1 BN/X(1):A-,-KOH,N-KOH,X-.15.1.2 :Mf(2)=56,100/A:Mf-,ASTM D 128-98(2014)1 23 A-.15.1.3 :,%=MsC/Mf(3)E:Ms-,-,MfE-.-,15.1.4 ,(),(.8).,:,%=FMs/M(4)m:F-,MsM-,m ,.,15.1.3.-.8 .15.1.5 ,ASTM D 128-98(2014)1 24 ,.15.1.4.15.1.6 ,.,.,().,.16.()16.1 ,Na2CO3(.).,.(NaCl).ASTM D 128-98(2014)1 25 17.
16、17.1 -E(.14),125 300-,10 0,5 KOH 50 ,11/217.2 G ,H ,(.14),30-20-50%I.H I,-,G,H I ,D(.14.6).0,5 HCl,6.1,195(.1,0 195 KOH ).9 1,045 ,.18.18.1 -,G,F(.14.6),.18.2 ASTM D 128-98(2014)1 26 D 445.,150 200 ,13,.18.3 ,-,G,.,.II 19.19.1 76-(3-)10 KHSO4(.),10 ,5 .,;2.,-.-,0,5 KOH,ASTM D 128-98(2014)1 27 C(.14.4).14,17 18.20.20.1 CS2 (.100C .),120C 1,.21.21.1 10 30 ,75 -,250-50 95%(.5.4),.,10 0,5 HCl,10,CO2,0,5 KOH.22.22.1 -,ASTM D 128-98(2014)1 28 ,HCl.,0,5 HCl,.2,0,5 KOH,CaCO3,.23.23.1 ,0,5 KOH,.23.2 ,KOH
