1、 D 1608-98(2009)(-)STANDARD TEST METHOD FOR OXIDES OF NITROGEN IN GASEOUS COMBUSTION PRODUCTS(PHENOL-DISULFONIC ACID PROCEDURES)():1491-11/ASTM :05.08.2011 2011 (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This t
2、ranslation is executed by FGU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these
3、 translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FGU“CIC“Interstandard”,is strictly forbidden according to t
4、he USA legislation and international copyright.-,.9,-49,-1,119991.:(499)236-54-49,236-43-83:(499)230-13-72 E-mail:interstgost.ru Web:www.interstandart.ruASTM D 1608-98(2009)D 1608-98(2009)(-)1 D 1608;,.().1.1.1 -(1)2,(N2O).1.2 (NO2)5 (4 ).1 ASTM D22 ,D22.03 .1 2009.2009.1958.2003.D 1608-98(2003).DOI
5、:10.1520/D1608-98R09.1ASTM D 1608-98(2009)1.3 ,.1.4,.1.5 ,.,.(.8.5 3).2.2.1 ASTM:2 D 1193 D 1356,D 1357 D 1605 3 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM 3 2ASTM D 1608-98(2009)3.3.1 ,.D 1356.4.4.1 ,.().-,(6-1-2,4-),.,.5.5.1 (NOx),.6.(1,2)6.1 ,.3ASTM D 1608-98(2009),(
6、SO2),-,.,(),.6.2 .1.,D 1608.7.7.1 1.7.2,250 2 .7.3,120 4,.7.4 ,200.4ASTM D 1608-98(2009)(7).7.5 ,U-,1 36 1 0,1.1 .7.6,10,0,01.7.7 pH,7 14.7.8 2 24/40 ,.7.9,6,12/5 ,.,1/3 1/2 (1 2),().7.10,405.2 400 Project Threshold,(3,6,7),405,.7.11,.5ASTM D 1608-98(2009)7.12 ,.7.13 ,T-,24/40 ,12/5 .7.14 ,.7.15,1C
7、2F 5 +50C 25 125F.7.16 ,2,5 25 .7.17 ,50,100 1000.7.18 ,1,2,3,4 5.7.19 ,100C 212F(,).8.8.1 .,.4 ,4 ,D.C.,.,BDH Ltd.,Poole,Dorset,U.S.Pharmaceutical Convention,Inc.(USPC),Rockville.6ASTM D 1608-98(2009).8.2 ,D 1193(III ).,(0,002)(.5).8.3 3,0 (H2O2,3%)100 (H2SO4,3+997).8.4 (0,90)(NH4OH).8.5 (H2SO4-XSO
8、3),15 18%,.!8.6 (3%)10 H2O2(30%)100.3 H2O2(30%),:5 H2O2 500.20 20 H2SO4(1+9)0,1 N-(KMnO4).1 0,1 N KMnO4=0,001701 H2O2.8.7 (C6H5 OH),.8.8 -,25 150 H2SO4(1,84),75 7ASTM D 1608-98(2009)(15 18%SO3),100C 212F 2.,.8.9 (KNO3)105 110C 2 .8.10 ,(1 =1 NO2)2,1980 (KNO3)1.8.11 ,(1 =100 NO2)10 (1 =1 NO2)100 .8.1
9、2 (1 N)800 900 2 40 (NaOH).1 .8.13 (1,84)(H2SO4)95%.8.14 (3+997)3 (H2SO4)1,84 1.9.9.1 ,8ASTM D 1608-98(2009),.9.2 ,-,-.,.9.3 .10.10.1 25 -(.4),.1/3-1/2 (1 2),.,1,.(2,5-4,0 20-30 0,8-1,2 .,.,.,1,33 10 0,4 .1,.9ASTM D 1608-98(2009),().,.,.,.,(15)(.5).D 1357 D 1605.4 24/40 6 1/4 .5 ,2.,1%.11.11.1 .10 ,
10、.11.2 10ASTM D 1608-98(2009)0 125 NO2,2000 21 70F 101,33 760 29,92 .0,0,1,0,2,0,3,0,4,0 5,0 KNO3(1 =100 NO2)200,25,0 .12.3-12.5.NO2().6 ().12.12.1 ,.,.13.1.12.2 200 (.7).25 ,.,.7 ,11ASTM D 1608-98(2009),50,.200.25,0 50 ,200 .8 15,.,(NO2)10,.1 1%.9 ,15 ().12.3 NaOH ,.NaOH(7).2 -().1 4 H2SO4(1,84),3.,
11、10 .15 NH4OH.,12ASTM D 1608-98(2009)NH4OH.12.4 7 ()(.10)50.4 5 .50 .10 (7),.,.,.,50.12.5 405 .,.12.6 NO2().11 ,.,.13ASTM D 1608-98(2009)13.13.1 ()21 70F 101,33 760 29,92 .13.1.1 :Vc=(Vf Va)(Pf/Tf Pi/Ti)(21+273,2)/101,33:Vc-,Vf-,Va-,25,Pi-,Pf-,Ti-,(C+273,2),Tf-,K(C+273,2).13.2 NO2():NO2,=(24,1 W 103)
12、/46Vc:Vc-,W-NO2,24,1 103-21C 70F 101,33 760 29,92 .,46-(NO2).12 NO2 /3,/.)1,91 1,19 107,.14ASTM D 1608-98(2009)14.(3,4,5)14.1 ASTM ,-NOx 20 2000,(SR)(SW),.2(5).2-,-SB SW()NOx()2.-,-.15ASTM D 1608-98(2009)14.2 ,NOx 90 260 14,5.,-.,.14.3 95%-(95%CL)n-,m,SW 2.95%CL m (1,95/n)SW.14.4 95%CL-,n-,ST,2,:,NO
13、2 ,:ST=14,5 NO2,95%CL,1,96 ST.14.5 ,16ASTM D 1608-98(2009),1,96 ST NO2 20 2000.14.6 ,-,2/3 .,3,6 7,7%.,-(3,25%);,.14.7 -,7,(3)(4).,2(NOx 400).,ASTM -,.17ASTM D 1608-98(2009)15.15.1 ;7;7;-;(1)Beatty R.L.,Berger L.B.,Schrenk H.H.,-,U.S.Dept.Interior,-,1943.,.3687.(2)Boltz D.F.,Interscience,-,1958.(3)H
14、amil H.F.,Camann D.E.,(,),-05 1973.(4)Hamil H.F.,Thomas R.E.,(),-08 1974.(5)Howes J.E.,Jr.,Pesut R.N.,Foster J.F.,(-)ASTM D 1608-60,ASTM DS 55-S8,ASTM,1975.(6)Martens H.H.,Dee L.A.,Nakamura J.T.,Jaye F.C.,18ASTM D 1608-98(2009)19 NOx -,Environmental Science Technology,.7,1973,.1152.(7)Robertson D.J.,Groth R.H.Glastris E.G.,NOx -,Environmental Science Technology,.9,1975,.979.ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).
