1、:D 143903(2008.)1 STANDARD TEST METHODS FOR SODIUM CARBOXYMETHYLCELLULOSE ():1810-12/ASTM :08.11.2012 2012 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,AST
2、M International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM Internationa
3、l does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Inters
4、tandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 1439-03(2008)1 1 :D 143903(2008.)1 1 D 1439;,.().1 11,12,15.5 31.1 2008.1.1.1 .1.2 :4-9 :A 10-17 10,12,18-23 24-30 31-38 39-47 48-55 56-62 1 ASTM D01 ,D01.36 .1 2008.2008.1956.2003.D 1439-03.DOI:10.152
5、0/D1439-03R08E01.ASTM D 1439-03(2008)1 2 1.3 ,.,.1.4 ,.,.15.1 20.2.2.1 ASTM:2 D 1347 (2003.)3 E 1 ASTM 3.3.1 ().,4,.,.2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 www.astm.org.4 ,DC.,.,BDH Ltd.,Inc.(USPC),MD.ASTM D 1439-03(2008)1 3 3.2 ,.4.4.1 .4.2 ;,.5.5.1 ().6.6.1 ,10
6、5 3C.6.2,50 30,.6.3 .7.7.1 3 5 0,001 .ASTM D 1439-03(2008)1 4 7.2 105C 2 .,.7.3 30,.7.4 5 30 .8.8.1 ,M,:(1):A-,-,.9.9.1 2 10%0,2%(.)95%-.9.2 ,.10.10.1 ASTM D 1439-03(2008)1 5 .10.2 :10.2.1 A(),0,85.0,85 .10.2.2 (),.11.11.1 ,.,.A 12.12.1 ,.13.13.1,.13.2 ,75,70-,.ASTM D 1439-03(2008)1 6 60-.13.3 ,105C
7、.14.14.1 0,5 120 (H2SO4,9+2).14.2 (95.%),:2B,3 30.14.3 (80.%)840 2B,3 30 1 .14.4 ,(HC1,0,3 0,5-).14.5,.14.6 (.1,42)(HNO3).14.7 ,(0,3-0,5-)0,3 0,5-(NaOH).14.8 (9+2)9 H2SO4 2 .15.15.1 4 250-75 (95%).5 HNO3 1-2.ASTM D 1439-03(2008)1 7 5.(.)10-15.15.2 50-100 (95%).(80%),60C,.15.3 (),.,.15.4 ,.,(-),105C
8、3.15.5 0,5%,0,5 ,D 1347.0,5%,(80%).,15.115.4.ASTM D 1439-03(2008)1 8 15.6 0,01 1-1,5 (,)500-.,100 25,00 0,3-0,5-NaOH.15-30.15.7 ,NaOH 0,3-0,5-HCl .16.16.1 ,G,:(2)(3):A-,-NaOH,-NaOH,D-HC1,NaOH,E-HCl,F-,162-,58-.17.17.1 ()0,04 95%-.ASTM D 1439-03(2008)1 9 17.2 ,.-18.18.1 -.,.,.19.19.1 pH-,:19.1.1 ,.20
9、.2.19.1.2 .19.2,10.20.20.1 ,.20.2 2 (KCl)2 (AgCl)(Ag2O)100 .ASTM D 1439-03(2008)1 10 20.3 1,4-.20.4 (0,1-)9 (HClO4,70%)1 ,().,.20.4.1 :2 120C.2,5 0,0001 250-.,.10 100-50 .pH-.HClO4 ,0,05.,N,:(4):A-,-HClO4,204.22-,10-,250-,.ASTM D 1439-03(2008)1 11 20.5 ,84 (NIST).21.21.1 0,2 0,0001 250-.75 ,2.21.2 2
10、50-50 .0,1-HClO4 .20.4.22.22.1 ,H,(1):(5)(6):M-,A-lO4,N-HClO4,G-,-,4-7,162-,80-.ASTM D 1439-03(2008)1 12 1 ,18,;,0.5%,.23.23.1 :,(95%-)0,40 0,010 0,80 0,012 1,35 0,038 23.2 ,.24.24.1 10 10000 25C.24.2 .,.24.3 ,ASTM D 1439-03(2008)1 13.24.4 ;,.24.5 .,1,.1 ,/10 100 1 60 100 1 100 200 1 30 100 2 200 10
11、00 2 30 100 10 1000 4000 3 30 100 40 4000 10000 4 30 100 200 25.25.1 .26.26.1,.26.2 ,64 (21/2)152 (6),340 (12).26.3 .26.4 ,ASTM D 1439-03(2008)1 14 (.1),900 100/.1 26.5 ,25C 0,2C.26.6 ASTM 19 27C,17C,E 1.27.27.1 4 9.27.2 ,M,240 :302-304-316 .ASTM D 1439-03(2008)1 15 (7):A-,-,%.27.3 :(8):V-,S-,.27.4
12、.,.27.5 .900 100/2.1200/,.2 ,.27.6 1.,.27.7 10.,1.ASTM D 1439-03(2008)1 16 28.28.1 ,V,:V=(9)29.29.1 25C ,.30.30.1 ()10%95%-.30.2 ,.31.31.1 ,.0,85 .31.2 (98%)ASTM D 1439-03(2008)1 17 .32.32.1 3-15 150-(80.%)60-65C.,.,(.0,001).33.33.1 ,.98%,().34.34.1 ,50.34.2 ,.34.3 ,60 65C.34.4 ,400-.,ASTM D 1439-03
13、(2008)1 18 ,.,.,.35.35.1 (95.%),2B(3).3 ,3,.35.2 (80.%)840 95%-(30.1)1 .0,857 0,001 25/25C.35.3 ,.36.36.1 3 5 65,.105 1C ,.2-,30 ,30-0,10%.,.,.ASTM D 1439-03(2008)1 19 36.2 3 0,1 0,001 400-.36.3 150 (80%),60-65C,60-65C.,.10 ,.36.4 .,.36.5 150 (80%)60-65C 32.3 32.4.36.6 (80%)60-65C ,.250 (80%).,.,.,.
14、36.7 50 (95%),(4).ASTM D 1439-03(2008)1 20 ,.4 .,.36.8 105 1 1.(),.105 1C 1.,;(30).36.9 1-,1-0,003.,.37.37.1 ,S,:(10):A-,-,-,%.ASTM D 1439-03(2008)1 21 38.38.1 ()0,6%(.)95%-.38.2 ,.39.39.1 ,2,0%.40.40.1 (50%),.,(),2,7-.540.41.41.1 ().ASTM D 1439-03(2008)1 22 (98%),(,.).42.42.1 ,540.42.2 ,1-.42.3 2 (
15、51).43.43.1 ,.43.2.43.3 (0,100/)0,100 2,7-1 (H2SO4).,.,H2SO4.1 .43.4 ,(1 /).0,100 ,100-.1 /.1.43.5 (NaCl).43.6 (.1,84)H2SO4.ASTM D 1439-03(2008)1 23 44.44.1 100-1,2,3 4-,.,5.5 ,.0,1,2,3 4 .44.2 2 25-.20,.44.3 20 2,7-:5 ,15 .20.,H2SO4.44.4 540 .100 ,.45.45.1 0,5 (0,2 )0,001 100-.5 ,5 ,ASTM D 1439-03(
16、2008)1 24 ,(15).,50 ,1 NaCl.,.45.2 ,100-.30 ,.45.3 100-,5 5 .45.4 2 2 25-.44.2 44.4.45.5 ,.46.46.1 ,C,:(11):-,W-,A-,%,12.9-(-)10.ASTM D 1439-03(2008)1 25 47.47.1 (),0,50%,0,03%(.)95%-.47.2 ,.48.48.1 .49.49.1 .50.50.1 ().(98%),(,.).ASTM D 1439-03(2008)1 26 51.51.1 pH-,-/-.51.2,10.52.52.1 (30.%)(H2O2).52.2 (.1,42)(HNO3).52.3 ,(0,1-)17,0 (AgNO3)1 .:52.3.1 (NaCl)2 120C.0,65 0,0001 250-100 .,10 HNO3 pH-.AgNO3 ,0,05.,N,:(12):A-NaCl,-AgNO3,58.45-NaCl.ASTM D 1439-03(2008)1 27 52.4 (NaCl).53.53.1 5 0,000
