1、:D 1417-16 STANDARD TEST METHODS FOR RUBBER LATICES SYNTHETIC ():3047-16/ASTM :07.12.2016 2016.(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency
2、on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published
3、with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.-,.9,-49,-1,119991.
4、:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/ASTM D 1417-16 :D 1417-16 1 D 1417;,.().1.1.1 ABR,BR,CR,IIR,IR,NBR,NCR,NIR,PBR,PSBR,SBR,SCR,SIR,(COOH)(X),-,(Y).,(),pH,1 ASTM D11 D11.23 .1 2016.2016.1956.2010.D 1417-10.DOI:10.1520/D1417-16.1ASTM D 1417-16 .1 ,D 1418.1.
5、2,.1.3 ,.,.2.2.1 ASTM:2 D 1076 ,D 1331 ,-D 1416 (1996.)3 D 1418 D 1646 ,()D 3182 ,2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 .www.astm.org.2ASTM D 1417-16 D 3314 -D 4483 ,D 6204 E 70 pH E 200 ,E 1970 E 2975 3.3.1 .,.3.2 :3.2.1 ,75 75 .,3ASTM D 1417-16 1%,.3.3 :3.3.1 :
6、3.3.1.1 2%,10.15,10.2%,.10 .,.10 .3.3.1.2 ,.11 ,.900/.,.4ASTM D 1417-16 ,.,.1 -(,1 3 .),SBR 2000 45 SBR 2001 45 SBR 2002 45 SBR 2003 45 BR 2004 45 SBR 2005 45 SBR 2006 45 SBR 2076 45 SBR 2100 60 SBR 2101 X765 45 SBR 2102 60 SBR 2103 60 BR 2104 45 SBR 2105 45 SBR 2106 45 SBR 2107 45 SBR 2108 45 SBR 2
7、109 45 SBR 2110 45 SBR 2111 45 SBR 2112 45 SBR 2113 45 SBR 2114 45 3.3.2 ,.:15 ,.,.2 ,.5ASTM D 1417-16.3.3.3:3.3.3.1,10%,.4.4.1:4.1.1 ,50 60 3,38 (1,5)23 (0,9).4.2:4.2.1 A ,.2 .170C,15.p.:;-;A-B100A-C%(1)0,1%.4.2.2 ,6ASTM D 1417-16 ,.4.2.2.1 ,Denver IR-100:145C 0,05%/1 A1 Fisher 01-913-356 Fisher 01
8、-913-318 .IR-100 ()X-.START.Tare pan,TARE.3,0 .10,START.4,.(%).0,1%.4.2.3 C CEM.4.2.3.1:(1)/().(2).(3)5-.4.2.3.2 .1,0 5,0 .7ASTM D 1417-16 ,.Start .3 D1076.5.()5.1 -.5.2:5.2.1 ,250 3,.5.2.2 25 3.5.2.3 50 3.5.3:5.3.1 ,100 -.5.3.2 -(0,1 N)2,784 (KBrO3)10,0 (KBr)1000 3.(Na2S2O3)0,1 N (3)(KI)(H2S04),(18
9、%).5.3.3 (18%).5.3.4 (10%).5.3.5 (0,1 N).5.3.6 .5.4:8ASTM D 1417-16 5.4.1 25 0,1 250-3 .25 3 .25 3 ,100 -.,:1.2.3.,p-.5.4.2 .25 3 250-3 ,20 3,100 -,.5.4.3 20 3 0,1 N KBr-KBrO3.30.15 3 18%-H2SO4,.60.,10 3 -,60 .,.60 -,10 3 10%-KI ,.0,1 N -.1 3 9ASTM D 1417-16 ,.5.4.3.1 ,.5.5 ():(),%=(D E)(F G)0,0521
10、100/M H(2):D-,E-,F-,G-,H-,%,-,.6.pH 6.1 pH-E70.,.,pH 2 14.6.2 ,pH=10 ,pH pH .6.3 (.6.2).10ASTM D 1417-16 .pH,.pH 25 2C.7.7.1 -40 1%.200 (200)1 20/,.7.2 du Nouy,D 1331.7.3 25 3,25 2C,60 65 18 20 (.4).,3 4,.,.,.,.,.,.,.,11ASTM D 1417-16 ,.,.,.;0,5/(0,5/).4 ,.7.4 ,/(),:,/=N(3):-,N-,:(4):-,R-,P-,:P=0,04
11、534 (1,679S/R)(5):S-,R-,.8.8.1 12ASTM D 1417-16 .8.2 ,.8.3:8.3.1 .8.3.2 355.8.3.3 ,.8.3.4 ,:8.3.4.1 ,0,6/60/,1%.8.3.4.2 ,8.3.4.3,6 40 ,8.3.4.4,1%,8.3.4.5 ,.8.3.4.6 ,.8.3.4.7 ,.13ASTM D 1417-16 ,:,.8.3.4.8 ,240 (8).8.3.4.9,.8.3.4.10,.8.3.4.11 ,:(1),.8.3.5 ,20C 30C 0,1C.8.4 :8.4.1 ,.(),500 3 .8.4.2 3,
12、4 3,8 (1 .),.,.14ASTM D 1417-16 8.4.3 355.,.,.8.5:8.5.1 ,.(.E 2975.)8.5.2 (6 40),.8.5.2.1 10 95%.8.5.3 ,23 27C.8.5.4 200 240.8.5.5 (),.5 ,.8.5.6 ,8.5.2.8.5.7 60 (1)(1)(1).8.5.8 8.5.7 ,(2)(3)(2),(3),(2)(3).15ASTM D 1417-16 8.5.9 ()()(.E 1970).6 ,.9.9.1:9.1.1 ,25.9.1.2,.9.1.3 .9.1.4 .9.1.5 p.9.2 (25)9
13、,0 0,2 p.;2000-.500 0,5 1200-.500 1 .,.(50).70C 15.7 .15 p.(4).:0,010%.16ASTM D 1417-16 9.3:%5 (6)500:%5 (7)9.3.1 :(),:()()1 000=(8)8 ,.10.10.1 -.,(50%).10.2 ,11.5.10.3 ,D 1416.11.11.1 0,50%.17ASTM D 1417-16,BR(2004),CR,NCR,SCR ABR.11.2 ,.,.11.3:11.3.1 4 .11.3.2.11.3.3 ,30 20 2,5 1,00 1,41,.11.3.4 ,
14、125 2C.11.3.5 ,D 3182.11.3.6 ,D 1646,D 6204.11.4 :11.4.1 (250/3)250 NaCl ACS 1 3 .11.4.2 (7,5/3)7,5 5 1 3 USP.11.4.3 (1+9)100 3 H2S4 ACS(.1,84)900 3 .11.4.4 .4,FCI-15 Waring Blendor,.5,-,Ethyl 702,Santowhite Powder,Wingstay L,-p-Wingstay 200,PBNA(-).18ASTM D 1417-16 11.4.5 (KD-64 Harwick),11.4.6 2,2
15、%,378 5 .11.5:11.5.1 30%,30%.250 3 50 3 NaCl .11.5.1.1 250 3 ,.10 3 H2S4(l+9)2 3.,H2S4 ,.11.5.1.2 .,.11.5.2 125 2C.,.5 ,.11.5.3 D 1646,19ASTM D 1417-16 D 6204.11.5.4 -(PSBR):11.5.4.1 2400 (130F).25 .200 (75 80 ).2%-(,),.,.,.(1).10.,.11.5.4.2 .90C.,.11/2 21/2.(1)15 .,1/2.,.11.5.4.3 ,10.4.2,.,60.85 5F
16、 0,065 0,005.40/,2 9.,.20ASTM D 1417-16 ,.11.5.4.4 ,D 1646,9 12.12.12.1 ,.12.2 ,.,.12.3:12.3.1 4,6 ,14000 200/.6,3 (0,25).,.0,25 (0,010).12.3.2 36,12 0,03 (1,422 0,001)6 ,Custom Scientic Instruments,Inc.,13 Wing Dr.,Whipy,NJ 07981.21ASTM D 1417-16 1,58 0,05 (0,062 0,002).12.3.3 57,8 1 (2,28 0,04)12,7 (5)2,3 (0,09).12.3.4 ,.,12,7 2 (0,5 0,1).12.3.5 180 0,180 0,009 (0,0070 0,0004)0,131 0,01 (0,0052 0,0005).,5 (11/2).12.4:12.4.1 ,8 ,350 (),350 (),10%.12.4.2 180 50 0,5 .,.12.4.3 30 ()22ASTM D 1417-1