1、Manual on Flash Point Standards and Their Use:Methods and Regulations Harry A.Wray,#ASTM Manual Series:MNL 9 ASTM Publication Code Number(PCN)28-009092-31 1916 Race Street Philadelphia,PA 19103 Ubraiy of Congress Cataloging in Pubicalion Data Manual on flash point standards and their use:methods and
2、 regulations/hHarry A.Wray,editor.-Irst ed.(ASTM manual series:MNL 9)ASTM publication code number(PCN)2&O09092-31.Includes bibliographicfd references and index.ISBN O-803M41(M)1.Inflammable liquids-Flammability-Standards.I.Wray,Harry A.,1909-.II.American Society for Testing and Materials.III.Series:
3、Manual(American Society for Testing and Materials);9.TP363.M246 1992 91-45892 628.9222021873-dc20 CIP Copyright 1992 AMERICAN SOCIETY FOR TESTING AND MATERIALS,Philadelphia,PA.All rights reserved.This material may not be reproduced or copied,in whole or in part,in any printed,mechanical,electronic,f
4、ilm,or other distribution and storage media,without the written consent of the publisher.Photocopy Rights Authorization 1o photocopy Items for Internal or personal use,or the Internal or personal use of spedflc clients.Is granted by the AMERICAN SOCIETY FOR TESTING AND MATERIALS for users registered
5、 with the Copyright Clearance Center(OCX)Transactional Reporting Srvlce,provided that the liase fee of$2.50 per copy,plus$0.50 per page is paid directly to CCC,27 Congress SL,Salem,MA 01970;(508)744-3350.For those organizations that have been granted a photocopy license ly CCC,a separate system of p
6、ayment has been arranged.The fee code for users of the Transactional Reporting Service is 0-8031-1410-4 92$2 +.NOTE:This manual does not purport to address(all of)the safety problems associated with its use.It is the responsibility of the user of this manual to establish appropriate safety and healt
7、h practices and determine the applicability of regulatory limitations prior to use.Printed in Baltimore,MD Sept.1992 Foreword The ASTM Manual on Flash Point Standards and Their Use:Methods and Regula-tions(MNL 9)is sponsored by the ASTM Coordinating Committee for Flash Point.Harry A.Wray,Chairman Em
8、eritus of the Committee,is editor of the publication.iii Acknowledgments The editor acknowledges the help provided by the ASTM staff,especially Brent Backus,Dorothy Savini,and the editorial and word processing departments.The U.S.National Institute of Standards and Technology,National Center for Sta
9、ndards and Certifi-cation Information helped in providing lists of flash point standards of U.S.and other national standards organizations.Information obtained from U.S.standards,code,and tariff organizations,such as the National Fire Protection Association,the Under-writers Laboratories,United Parc
10、el Service,and the Hazardous Materials Systems of the Association of American Railroads is appreciated.The information obtained from the U.S.Regulatory Agencies and from international regulatory bodies regarding the control of flammable liquids was helpful in making this guide a source of informatio
11、n on international regulations.Finally,the editor wishes to thank the members,past and present,of the ASTM Coordinating Committee for Flash Point and Related Properties,especially the present chairman and vice chairman,Mr.E.M.(Bud)Nesvig and Mr.John E.Rogerson for making available a forum for obtain
12、ing the information that provided the background for this manual.Harry A.Wray Editor iv Contents PART I:ASTM FLASH POINT STANDARDS Chapter 1:Flash Point History 3 1.History of Flash Point Testing 3 2.History of ASTM Flash Point Standards 3 3.Flash Point Basics 4 Chapter 2:ASTM Basic Flash Point Stan
13、dards 5 I.Reprints of the Eight Basic ASTM Flash Point Standards Methods 6 D 56:Test Method for Flash Point by Tag Closed Tester 6 D 92:Test Method for Flash and Fire Points by Cleveland Open Cup 12 D 93:Test Methods for Flash Point by Pensky-Martens Closed Tester 17 D 1310:Test Method for Flash Poi
14、nt and Fire Point of Liquids by Tag Open-Cup Apparatus 30 D 3278:Test Methods for Flash Point of Liquids by Setaflash Closed-Cup Apparatus 37 D 3828:Test Methods for Flash Point by Setaflash Closed Tester 44 D 3934:Test Method for Flash/No Flash TestEquilibrium Method by a Closed-Cup Apparatus 50 D
15、3941:Test Method for Flash Point by the Equilibrium Method With a Closed-Cup Apparatus 53 Chapter 3:ASTM Flash Point Standards for Specific Products(Excerpts)56 1.D 115:Methods of Testing Varnishes Used for Electrical Insulation 56 2.D 117:Guide to Test Methods and Specifications for Electrical Insu
16、lating Oils of Petroleum Origin 57 3.D 154:Methods of Testing Varnishes 57 4.D 176:Methods of Solid Filling and Treating Compounds Used for Electrical Insulation 57 5.D 268:Methods of Sampling and Testing Volatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and Materials 57 6.D 333:Method for Clear and Pigmented Laquers 58 7.D 555:Guide for Testing Drying Oils 58 8.D801:Methods of Sampling and Testing Dipentene 58 9.D 803:Methods of Testing Tall Oil 58 10.D 901:Meth