1、 D7260-17 ,-(ICP-AES)STANDARD PRACTICE FOR OPTIMIZATION,CALIBRATION,AND VALIDATION OF INDUCTIVELY COUPLED PLASMA-ATOMIC EMISSION SPECTROMETRY(ICP-AES)FOR ELEMENTAL ANALYSIS OF PETROLEUM PRODUCTS AND LUBRICANTS 2018 ():02.04.2018:3392-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstg
2、ost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of Am
3、erican Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered
4、 as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D7260-17 1 D7260-17 ,-(ICP-AES)1 D7260;,.().1.1.1 ,-(ICP-AES).1.2 ,.,1 ASTM
5、 D02 ,D02.03 .1 2017.2017.2006.2012.D7260-12.DOI:10.1520/D7260-17.ASTM D7260-17 2 ,.1.3 -,(TBT).2.2.1 ASTM:2 D4057 D4307 D6299 D6792 ,2.2,ICP-AES:1111 -C1109 -D1976 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D7260-17 3-D4951 -D5184 ,-D5185 -(ICP-AES)D5600 -(ICP-AES
6、)D5708 ,-(ICP)D6130 -D6349 -,-D6357 ,-,-D7040 ILSAC GF 4 -ASTM D7260-17 4 D7111 -(ICP-AES)D7303 -D7691 -(ICP-AES)D7876 ()D8056 E 1479 -2.3 :IP 437 -3 ISO/TC 17/SC 1 N 883 -(1991)4 3.3.1-3 ,61 New Cavendish St.,London,W1G 7AR,U.K.,http:/www.energyinst.org.4 (ANSI),25 W.43rd St.,4th Floor,New York,NY
7、10036,http:/www.ansi.org ASTM D7260-17 5(ICP-AES),.1479.,.4.4.1 .4.2-,(,1111,D1976,D4951,D5184,D5185,D5600,D5708,D6130,D6349,D6357,D7040,D7111,D7303 D7691),.(Nadkarni)(1).5 4.2.1 -D8056.4.3 ICP-AES ,-5 ,.ASTM D7260-17 6,.,.5.5.1 -,0,05 ,.,;,.,.5.2 ICP-AES,(-),(),;,-.CCD-CID-,-ASTM D7260-17 7 .().,.5
8、.2.1 ,.,().5.2.2 -.-,-.,.-,-.-.5.3 :ASTM D7260-17 8 5.3.1 .,.,.5.3.2 ,.,ICP-AES.5.3.3 ,/,.5.4 :5.4.1 200,190.5.4.2 ,ASTM D7260-17 9 -,167.,.,.5.5 :5.5.1 ,-(Paschen-Runge),.5.5.2 ,.,100 1000.,.6.5.5.3 ,.5.6 ,.().,.ASTM D7260-17 10 .,/.,/,.5.7 (.,).().5.8 ,.,.,.,.5.9 ICP-AES ,/,.,.ASTM D7260-17 11 5.9
9、.1,-(/),.5.9.2 /(-).5.9.3 ,ICP-AES,;.MSDS ,.6.6.1 ICP-AES ,.6.2 :1 D5185.6.2.1 (1),(2),(3),(4),.-.ASTM D7260-17 12 6.2.2 ,.,.,2%.6.2.2.1 .,(2-7).,.(,50%),.,.,.6.2.2.2 .ASTM D7260-17 13 ,.6.2.2.3 ,.,.6.2.3 ,D5185.1109 (Boumans)(6).,.-,.6.2.3.1 ,.,ASTM D7260-17 14 ,.Mg I Mg II .6.2.4 ;.6.2.5,./3 5.6.2
10、.5.1 ,.,.,(.1 D7111).6.2.5.2 .,(588,995),.ASTM D7260-17 15 6.2.5.3 (),.,.,.6.3 ,.,(,ICP-AES ),.(Babington)(),.(,),.6.3.1 ,().,ASTM D7260-17 16 ,.,-,.,.6.3.2,.ICP-AES ;ICP-AES ,.6.3.3 ,().,10%.,%.,.7.2.6.3.4 ().,ASTM D7260-17 17,.,(,2%).6.3.5 ,(8).,.:Ag,Be,Cd,Co(),La,Mn,Pb,Sc Y.,.6.3.6 ,(.8.8.4).,.,.
11、,.6.4 :6.4.1 ,ASTM D7260-17 18.,.,.6.4.2 ,.,1%2%,(,H2S,).6.5,-(,).,.,.6.6 ().,.6.6.1,ASTM D7260-17 19 1%,.,.,190.6.6.2 500 1-3,.6.6.3 ,.(,).,.;.6.7 .ASTM D7260-17 20 7.7.1 ,.7.1.1 .,.7.2 ,-.,.ICP-AES,.7.3 .7.4,.7.5/10%-(,),ASTM D7260-17 21 ./,()(),.,.8.8.1 30 .8.2 ,().,.8.3 .30 ,.1,5-2,.,.8.4 ,ASTM
12、D7260-17 22 ,.8.5 ,.,.8.6 ,(-),.().8.7 :8.7.1-.8.7.2 (,),.,.(),/.ASTM D7260-17 23 8.7.3 ,.8.8 :8.8.1 ICP-AES (.2.2),()(),.,.,.,(),/,.,.8.8.2 .,(.).ASTM D7260-17 24 ,(),(),.8.8.2.1 ,(.),.8.8.2.2 ().,.8.8.2.3 ,.8.8.3 ,.,.100 (10/20/).ASTM D7260-17 25 ,-.8.8.4 ;,;,;,.,.8.8.4.1 ,.:Ag,Be,Cd,Co(),La,Mn,Pb
13、,Sc Y.9.9.1 (0,1%).ASTM D7260-17 26 ,./;,0,6%.,.,.9.1.1 ,.D4307.,0,1%.0,01%,0,5%.9.1.2 ,(.),.9.1.3 ASTM D7260-17 27 ,.9.1.4 ,.9.1.5 ,.9.1.6 .,.9.2 ,.9.3 ,.9.4 ()(,),.;,ASTM D7260-17 28 ,.10.10.1 :10.1.1 ,D4057.ICP-AES.10.1.2 ,60 ,.,(),.10.1.3 ,ICP-AES (,D5184,D5600,D5708),:10.1.3.1 ;10.1.3.2 ,ASTM D
14、7260-17 29 .,2-2-;10.1.3.3 ,.10.1.4 ,(,D7876).10.2 ICP-.(.1).,.,.10.3 ,.10.,.,ASTM D7260-17 30 60 .,(),-,.,(),.10.4 (),.,(5%),100-.,.10.5 ,.,8.8.1,ASTM D7260-17 31 (.,).1.ICP-AES ,A 308,215;237,01;237,313;309,271;396,153;256,799;394,401 233,53;455,403;493,410 B 182,59;249,68;249,773 315,887;317,933;
15、393,367;364,44;396,847;422,67 205,552;267,716;298,92;283,563 228,616 324,754;219,226 271,44;259,940;238,204;259,837 220,353;224,688;283,306 670,784 293,65;279,553;279,079;280,270;285,21 257,610;293,31;293,93;294,920 202,030;281,616;204,598;203,844 231,604;341,476;277,02;221,648;216,56;352,454 B 177,
16、51;178,289;213,62;214,914;253,40 766,491;769,896 255,237 288,159;251,611;212,412;282,851;252,411 328,068 330,29;588,995;589,3;589,592 B 180,731;182,04;182,62 189,989;242,95 337,280;334,941;350,50 292,403;309,31;310,230;311,07;292,464 371,030 202,48;206,209;202,551;213,856;334,58;481,05 A .,ICP-AES.,190 .10.6 ,-.,.ASTM D7260-17 32 (),.,(,).10.7 ,.,.11./11.1 (QC).QA/QC ICP-AES,2.2,D6299 D6792.11.2 ,QC .,QC ,.11.3 .11.4 QC-,.,ASTM D7260-17 33 -.11.5 QC .QC ,QC .QC,ASTM.D6792.11.6 ,NIST ,.12.12.1 :%
