1、 D 7011-15 STANDARD TEST METHOD FOR DETERMINATION OF TRACE THIOPHENE IN REFINED BENZENE BY GAS CHROMATOGRAPHY AND SULFUR SELECTIVE DETECTION 2016 ():2867-16/ASTM :05.04.2016 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr
2、Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)1
3、00 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified transl
4、ations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 7011-15 1 D 7011-15 1 D 7011;,.()1.*1.1 .0,02 2,18 (/)-(AED),0,03 1,87/-(PFPD)0,03 2.11/(SCD).,1 ASTM D16 D16.04 .1 2015.2015.2004.201
5、0.D 7011-10.DOI:10.1520/D7011-15.ASTM D 7011-15 2 ,.1.2 ,E 29.1.3,.1.4 ,.,.7.2.2.1 ASTM:2D 1193 D 2359 -535 D 3437 D 4734 -545 D 4735 D 5871 D 6809 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 7011-15 3 E 29 E 177 ASTM E 691 E 1510 2.2 :OSHA(),CFR()29 1910.1000 191
6、0.12003 3.3.1 1/,.3.2 ,-,-,5.4.,.-,3 ,:732 N.Capitol St.,NW,Mail Stop:SDE,20401,http:/www.access.gpo.gov.ASTM D 7011-15 4,0,5/.,.1,.,.1,.,0,5/.-D 4735.1.30,0,32,1,()40C 2;100C 10C/,100C 1 2/1:4 1:10 125C 1-2 4.4.1 -,.-,-,-.4.2 ,D 2359,D 4734 D 5871,.ASTM D 7011-15 5 4.3 ,D 4735.5.5.1 ,0,05.,.5.2 ,.1
7、,.,.1.E 1510.5.3 .5.4 ,:(1)102;(2)0,02/;(3)1055.5 ;(4),.ASTM D 7011-15 6 .:(1);(2);(3);(4).5.6:5.6.1-(99,995+%).,.-.5.6.2-(99,995+%).,(99,8+%).,.5.6.3 -.,1%.,70 (10 .),.550 (80 .).ASTM D 7011-15 7 1 ,SCD,.1.,0,2/,AED,PFPD SCD(,)AED ,.-(AED)-(PFPD)(SCD),ASTM D 7011-15 8 5.7 10,50,100 250 (1%).5.8 0,5
8、,1,0 2,0 (A).5.9 10,50,100 500 (A).5.10 1.6.6.1 .,46.2 ,IV D 1193.,.6.3,:6.3.1 700 1000-,5 ,100-,-.100-,100-(CdCl2 4 ,.,.,BDFf Ltd.,.,Inc.(USPC),.,.).100-,.ASTM D 7011-15 9 6.3.2 ,10.4.6.4 (20/)20 (CdCl26.5 .)200 1.6.6 0,5 200 .(61C)5,.250-.6.7 ,.6.8 H2SO46.9 ,99%.7.7.1 .,OSHA ,.7.2 ,.7.3 ,.ASTM D 7
9、011-15 10 7.4 ,.7.5 ,.7.6 .7.7 ,.7.8 .8.8.1 D 3437.8.2 ,.,.,.,.8.3 ,.9.9.1 .,ASTM D 7011-15 11 .(.10.4).9.2 ,.1.E 1510.9.3 .10.10.1 ,.,-,.10.2 100/,0,1000 1000 ,.4 .10.3 ,.,0,02,0,2,0,5,1 2/.10.4 1 2 .ASTM D 7011-15 12 (.10.1).0,02/.6.3.10.5 ,.,.,.10.6 1.Rf(1)=C/A:Rf-,/;-;A-(),(.10.4).11.11.1 .,().,
10、10.4.-.ASTM D 7011-15 13 11.2 .0,2/,AED,PFPD SCD,.1.12.12.1 ,.2:Ct=At R(2)f:CtA-(/),tR-,f12.2 0,01/.-.13.13.1 .13.1.1 ,.13.1.2 ,.13.1.3 /,.ASTM D 7011-15 14 13.1.4 /,D 6809 .14.5 14.1 (ILS)D 7011 ,2008.ILS ASTM RR:D16-1039.ILS ,E 691,8.ILS ()(),E 691.14.1.1 AED:6 3;36 .14.1.2 PFPD:5 3,4 3;42 .14.1.3
11、 SCD:6 3,5 3;51 .14.2 (r),r ,r ,5 -ASTM International RR:D16-1039.ASTM Customer Service serviceastm.org.ASTM D 7011-15 15 ,.14.2.1 .2 4.14.3 (R),R ,R ,.14.3.1 .2 4.2.AED(2),/,/,/,0,02 0,01 0,01 6 0,53 0,04 0,10 6 0,70 0,04 0,04 6 1,13 0,07 0,20 6 1,84 0,10 0,31 6 2,18 0,08 0,25 6 3.PFPD(3),/,/,/,0,0
12、3 0,01 0,07 9 0,51 0,03 0,21 9 0,73 0,12 0,36 9 1,21 0,08 0,55 6 1,87 0,19 0,61 9 :PFPD-.14.4 (),E 177.ASTM D 7011-15 16 4.SCD(3),/,/,/,0,03 0,01 0,05 9 0,60 0,03 0,24 9 0,81 0,05 0,29 9 1,24 0,04 0,45 9 1,83 0,04 0,48 9 2,11 0,06 0,44 6 14.5 ,.,.15.15.1-;-;.()XI.X1.1 X1.1.1 .,ASTM D 7011-15 17 ,.,.
13、,.X1.1 (/)0,02 0,08 0,2 0,8 1,92 E D B C A -1 0,020 0,075 0,173 0,787 2,04 2 0,019 0,084 0,222 0,797 1,93 3 0,021 0,076 0,209 0,787 1,98 0,0202 0,0784 0,201 0,790 1,983 0,0012 0,0047 0,025 0,006 0,054 0,007 0,029 0,154 0,036 0,327 -B 1 0,019 0,069 0,204 0,857 1,96 2 0,018 0,074 0,205 0,861 1,94 3 0,
14、021 0,068 0,228 0,857 1,84 0,0193 0,0706 0,212 0,858 1,913 0,0012 0,0033 0,013 0,002 0,067 0,007 0,02 0,082 0,013 0,405 C 1 0,022 0,076 0,225 0,799 1,86 2 0,022 0,080 0,225 0,786 1,87 3 0,023 0,077 0,221 0,787 1,83 0,023 0,078 0,224 0,791 1,85 0,0004 0,0025 0,002 0,007 0,025 0,002 0,015 0,013 0,044
15、0,155 A Agilent Technologies 0,02,0,2,0,5,1 2/.B O.I.Analytical 0,16 0,6/.C Ionics Instruments 0,16 0,6/.ASTM D 7011-15 18 X1.2 X1.2.1 .X1.1.t 0,05.,.D16 (D 7011-10a),.(1 2015.)(1)D 1685.ASTM D 7011-15 19 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.