收藏 分享(赏)

ASTM_D_7041_-_04_2010_rus_scan.pdf

上传人:益****师 文档编号:173623 上传时间:2023-03-04 格式:PDF 页数:11 大小:482.78KB
下载 相关 举报
ASTM_D_7041_-_04_2010_rus_scan.pdf_第1页
第1页 / 共11页
ASTM_D_7041_-_04_2010_rus_scan.pdf_第2页
第2页 / 共11页
ASTM_D_7041_-_04_2010_rus_scan.pdf_第3页
第3页 / 共11页
ASTM_D_7041_-_04_2010_rus_scan.pdf_第4页
第4页 / 共11页
ASTM_D_7041_-_04_2010_rus_scan.pdf_第5页
第5页 / 共11页
ASTM_D_7041_-_04_2010_rus_scan.pdf_第6页
第6页 / 共11页
亲,该文档总共11页,到这儿已超出免费预览范围,如果喜欢就下载吧!
资源描述

1、MEXKTOCYAPCTBEHHbIN COBET nO CTAHDAPTM3AUNM,METPOnOTNN W CEPTNONKAUNN(MrC)INTERSTATE COUNCIL FOR STANDARDIZATION,METROLOGY AND CERTIFICATION(ISc)OcTMEKOCyAAPCTBEHHbINCTAHAAPT332532015HETENPOyKTbIOnpeneneHne o6wero conepxaHna cepblMeTonOM ra3oBon xpoMatorpadnnc nnaMeHHo-doTOMeTpnyecKnM neTeKTnpoBaHne

2、MM3 naHwe o中nunanbHoeMocKBaCTaHAapTNHopM2016T0CT33253-2015npeancnoBneLenn,OCHOBHble npnHuNnbl n nopanok npoBeneHnA paboT no MexkrocynapcTBeHHon CTaHnapTn3aunnyCTaHoBneHbI B TOCT 1.0-92&MexkrocynapcTBeHHa CncTeMa CTaHnapTn3aywn.OCHOBHble nonoxkeHNTOCT 1.2-2009 MexkrocynapcTBeHHa cncTeMa cTaHnapTn3aun

3、n.CTaHAapTbl MexkrocyAapcTBeHHble,npaBnna n peKoMeHnaunn no MexkrocynapcTBeHHon cTaHnapTn3aunn.npaBnna pa3pa6oTkn,npnHaTna,npNMeHeHNA,OOHOBneHNA N OTMeHbICBeneHNA o cTaHnapte1 nOTOTOBNEH MexrocynapcTBeHHbIM TexHnyeCKnM KOMNTeTOM no CTaHnapTn3aywn MTK 31HedTAHble TonnnBa n CMa304Hble Matepnanbl,OTKpb

4、ITbIM akuMoHepHblM o6weCTBOM BcepoccnMCKNMHayuHo-nccnenoBaTenbcknn MHCTMTyT no nepepa6oTke HedTn(OAO BHVM Hn)2 BHECEH enepanbHbIM areHTCTBOM no TexHnueCKoMy perynnpoBaHnlo MeTponorn(PoCCTaHAapT)3 nPMHAT MexrocynapcTBeHHbIM coBeTOM no cTaHgapTn3aynn,MeTponornn n cepTnonkaynn(npo-T0K0n0T18MoH92015r.N9

5、47)3a npnHaTne nporonocoBann:KpaTkoe HanMeHoBaHne CTpa-KoA CTpaHblCokpaweHHoe HaNMeHoBaHNeHblnoMK(MC03166)00497HauMoHanbHoro opraHan0MK(MC03166)004-97no cTaHgapTn3aylnApMeHNAAMMNH3KOHOMNKN Pecny6nNKn ApMeHNAKnprN3N9KGKblprbl3cTaHnapTMonAoBaMDMonAoBa-CTaHAapTPoccnaRUPoccTaHnapTy36eKncTaHUZy3cTaHnapT4

6、 npnka3oM enepanbHoro areHTCTBa no TexHnyeCKoMy perynupoBaHnlo n MeTponornn OT 31 aBrycTa2015 r.Ne 1261-CT MexkrocynapcTBeHHbin CTaHaapT TOCT 33253-2015 BBeaeH B eNCTBMe B KayecTBeHayMoHanbHoro CTaHAapTa Poccnnckon enepaynn c 1 AHBapa 2017 r.5 HacToaunn cTaHnapT MAeHTw4eH cTaHAapTy ASTM D7041-04(201

7、0)Standard test method fordetermination of total sulfur in light hydrocarbons,motor fuels,and oils by online gas chromatography withflame photometric detection(CTaHnapTHbIn MeTon onpeneneHna oowen cepbl B nerknx yrneBonoponax,MOTOPHbIX TonnNBax N Macnax noTOYHON ra30BoN xpoMatorpaonen c nnaMeHHO-OOT

8、OMeTpNyeCKNM neTeK-TNpoBaHNeM).CTaHAapT pa3pa6oTaH noAKOMMTeTOM D02.03 3neMeHTHbIi aHann3TexHnueckoro KOMNTeTa ASTMDO2He中TenpoayKTbl M CMa3 OuHble Matepnanbly.nepeBon c aHrnwnckoro 93bika(en).HaNMeHOBaHne HacTogwero CTaHnapta N3MeHeHO OTHOCNTenbHO HanMeHOBaHNA yKa3aHHoro CTaH-AapTa ana npuBeneHMa B

9、CooTBeTCTBMe c rOCT 1.5-2001(nyHKT 3.6).OoMuNanbHble 3K3eMnnapbl CTaHnapta ASTM,Ha OCHOBe KOToporo nonroToBneH HacToAwNn MexKro-cynapcTBeHHbIn CTaHnapT,CTaHnapToB,Ha KoTopble naHbl cCbinkn,WMelOTCA B enepanbHOM NHopMaun-OHHOM OHne TexHNyecKnx pernameHTOB N CTaHnapToB.CBeneHNA O COOTBeTCTBNN Mexkrocy

10、napcTBeHHbIX CTaHnapToB cCblnoyHbIM CTaHnaptaM npnBeneHbl BononHNTenbHOM npwnoxkeHnN A.CTeneHb COoTBeTCTBNA-MaeHTNYHaA(IDT)6 BBENEH BNEPBbIE4FOCT 33253-2015M E K T O C YA A P C T B E H H bIMC T A HA A PTHETENPOAYKTbIOnpegeneHne o6wero cogepxaHA cepbi MeTogoM ra3oBonXpoMaTorpa中nn c nnaMeHHO-中oToMeTpn

11、yecKnM AeTeKTuPOBaHeMPetroleum products.Determination of total sulfur content by gas chromatography method with flame photometricdetectionAaTa BBeAeH-2017-01-011 06nacTb npMeHeHA1.1 HacTown cTaHAapT ycTaHaBnnBaet onpegeneHne o6wero cogepxaHn cepbi B nAKnx yrneBo-gopogax c Temnepatypom KoHua KnneHnA

12、go 450 C MeTogom ra3oBon xpoMatorpann c ncnonL3oBaHneMnnaMeHHo-oToMeTpeckoro AeTekTopa.1.2 HacTouu meTog moxho npnmeHAtb npn 06wem cogepxaHnn cepbi oT 0,5 go 100 mr/kr.p n M e 4 a H e 1-Ha ocHoBaHnn pe3ynbTaToB nporpaMMLI Mexna6opaTopHbIX o6beAHeHHbIX C-nbtahn 2002 r.6biN yctaHoBneH o6begnHeHhbi npe

13、gen konnuectBeHHoro onpegeneHnA(PLOQ),paBHbi 1 Mr/kr.p n M e 4 a H n e 2-MokHo npoBoAnTb aHann3 o6pa3yoB c pyrnMn ypoBHAMn oowero cogepxaHngcepbi,Ho Ana taknx o6pa3uoB He cneAyet npMeHATb npe3nOHHOcTb,ycTaHoBneHHyio B HacTOeM cTaHAapTe.1.3 3HaeHng,ycTaHoBneHHble B eAnHnyax C,cunTaoT cTaHAapTHbIM.1.4

14、 B HacToueM cTaHAapTe He npeAycmoTpeHO paccMoTpeHMe Bcex BonpocoB 06ecne4eHA Ge30-nacHOCTM,cBA3aHHbIX c ero cnonb3oBaHeM.onb3oBaTenb cTaHgapTa HeceT OTBeTCTBeHHOCTb 3a o6eC-ne4eHMe cOOTBeTCTByOLX Mep 6e3onacHOCT OxpaHbI 3AOpoBbA n onpegengeT yenecoopa3HOCTbnpMeHeHA 3aKoHogaTenbHbix orpaH4eH nepeg er

15、o mcnonb3oBaHeM.CneyanbHbie yKa3aHnA noTexHKe 6e3onacHocT npBeAeHbI B pa3gene 7.2 HopMaTBHble cCbInKnAng npMeHeHnA HacToero cTaHAapTa Heo6xoAnMbi cneAyioue ccbino4hble AokyMeHTbi.An HeAa-TPoBaHHbIX cCbInoK npnMeHioT nocneAHee n3aHne ccbino4Horo goKyMeHTa(Bkno4a Bce ero n3MeHeH).2.1 CTaHAapTbI ASTM1:

16、ASTM D 1298 Test method for density,relative density,or API gravity of crude petroleum and liquidpetroleum products by hydrometer method(MeTog onpegeneHA nnoTHOCT,OTHOCTeNLHO nnOTHOCTunu nnoTHoctn B rpagycax API cbipo HeTn n xnAKnx HeTenpoAyKTax apeoMeTpoM)ASTM D 4052 Test method for density,relativ

17、e density,and API gravity of liquids by digital densitymeter(Merog onpegeneHn nnoTHoctn,oTHocutenLHou nnoTHoct u nnoTHocTn xnAKocTen B rpaycaxAPI POBbIM nnoTHOMePoM)ASTM D 4057 Practice for manual sampling of petroleum and petroleum products(门lpakrnka pyqHoroOTopa npo6 HedT n HeTenpoyKTOB)ASTM D 417

18、7 Practice for automatic sampling of petroleum and petroleum products(lpaKruka aBTo-MaTneckoro oToopa npo6 HeT n HeTenpoAyKTOB)ASTM E 840 Practice for using flame photometric detectors in gas chromatography(lpakruka ncnonL-30BaHn nnameHHo-oTomeTpecknx geTekTopoB B ra3oBon xpoMaTorpaonn)3 CyuHOCTb Me

19、TogaO6pa3ey aHann3npyoT MeToAoM ra3oBo xpomaTorpann c nnaMeHHo-oToMeTpn4ecKnM geTeKTo-poM.中nKcpoBaHHoe KonMecTBo o6pa3ya BBoAAt B ra3oBb xpomaTorpa,B KoTopom 06pa3ey ncnap-eTcA.loToK Bo3Ayxa nepeHocuT napbi o6pa3ya B BbicoKoTemnepaTypHyo 30Hy(900 C),B KoTopo npn-cyTCTByoune B oopa3ye coegnHeHn oKncn

20、oTcA.Cepa,cogepxaac B coeHeHx,oKncneTcA OAnoKcnga cepbi(SO2).loTok nepeHocut oKncneHHble KOMNOHeHTbi B XpoMaTorpapnueckyio KonOHKy,B Ko-)YTo4HNTb ccbInKn Ha cTaHAapTbi ACTM MoxHo Ha cavite ACTM www.astm.org unu B cnyx6e nogepxkn knn-eHToB ACTM:serviceastm.org.B nHpopMauMOHHOM ToMe exerogHoro c6opHnK

21、a cTaHAapToB(Annual Book of ASTMStandards)cnegyeT o6pauaTbcA k cBoAke cTaHAaptoB exerogHoro c6opHnKa cTaHAapToB Ha cTpaHnye caviTa.M3aHne opnunanbHoer0CT33253-2015TopoN OHn pa3nenaloTca.n SO2 konnyeCTBeHHo onpenenaeTca nnaMeHHo-doToMeTpnyeCKNM eTekTopoM.Kann6poBky neTekTopa BbinonHAIOT c wcnonb3oBaH

22、neM COOTBeTCTByowero BHewHero CTaHnapta.4 Ha3HayeHne n npNMeHeHne4.1 HacToawnn MeTon MOXKHo ncnonb3oBaTb na onpeneneHNA o6wero conepkaHnA cepbl B TexHO-nornyeCKoM Cblpbe N TOBapHbIX nponykTax B COOTBeTCTBMN c o6nacTblo npnMeHeHNA HacToAwero MeTonaMcnbITaHnn.4.2 naxke He3HaynTenbHoe conepxkaHne cepbl

23、 B TexHonornyeCKoM Cblpbe MoXKeT npnBeCTn K OTpaB-neHWIO AoporocToAwx KaTann3aTopoB,wcnonb3yeMbIX B npoueccax nepepa6oTkn HedTn.HacToawnn Me-TO NcnbITaHnN MOXKHO Ncnonb3oBaTbn KOHTpona conepxkaHna cepbl B TaKoM Cblpbe.5 Annaparypa5.1a3 OBbIN xpoMatorpaTa3oBbln xpoMatorpad,o6opyaoBaHHbin CnCTeMon aBT

24、oMaTnyeckoro ynpaBneHna knanaHaMn,o6ec-neynBalownn aBToMaTnyeckyio KannopoBky c Ncnonb3oBaHneM BHewHero cTaHnapta n OCHaweHHbin nna-MeHHO-doToMeTpnyecKNM neTekTopoM c npenenoM neTekTnpoBaHna He 6onee 0,5 Mr/kr SO2.XpoMaTo-rpad nonkeH obecneynBaTb aBToMaTnyeckoe ynpaBneHne BpeMeHeM nepeknioyeHna knan

25、aHoB.HecMOTpaHa To YTO HacToAwNN MeTon NcnblTaHnn nepBoHayanbHo pa3paooTaH c wcnonb3oBaHneM noTOYHoro aHa-nMTNyeckoro N3MepnTenbHoro o6opynoBaHna,paboTalowero B aBTOHOMHOM pexKnMe,n HacToawero Me-Tona Takke MOXKHO Ncnonb3oBaTb COOTBeTCTBylowMe noToYHble wnn nabopaTopHble ra3oBble xpoMatorpa-dbl.Twno

26、Bble napameTpbl npnoopa npnBeneHbl B Taonnue 1.Ta 6 n u a 1-TmnoBble napameTpbl npn6opanapameTpXapakTepncTnKaa3-HOCMTenbOy山eHHbIn BO3AyXCkopoCTb noToka ra3a-HOCNTenA,CM/MWH30CkopoCTb noToka Bonopona,CM/MMH60eTekTop门naMeHHO-中OTOMeTPM4 eCKNNTeMnepaTypa neTekropa,C120TeMnepaTypa MHxKekTopa,C285TeMnepaT

27、ypa neun,C1000KonoHkaTpy6ka n3 HepxkaBerowen cTann anMHon 12,2 M(40yToB),AMametpom 3,2 MM(1/8 AOMMa)c 12 no-nnopeHnnoBoro 3cpupa/1,5 H3PO4 Ha xpoMocop6eT40/60TeMnepatypa konoHkn,C1155.1.1 KoHTponb ra3a-HocnTena n ra3oB AeTeKTopaXpoMaTorpad nonxkeH 6bITb o6opynoBaH perynaTopaMn noToka nnn perynaTopam

28、n naBneHna,o6ec-neynBalowlMN noCTOAHHyo nonayy ra3a-HOCHTena n ra30B neTekTopa.CneayeT ncnonb3oBaTb 3nekTpoH-HyHO CNCTeMy perynnpoBaHna noToka wnn naBneHNA.5.1.2 CncTeMa BBona npo6blCneayeT cnonb3oBaTb aBToMaTnueckoe yCTpoNcTBO BBoAa npo6bl.VHKeKTop AonkeH o6ecneynBaTbBBO B ra3oBbin xpoMatorpad He6o

29、nbwnx o6beMoB npo6bl OT 0,1 o 1,0 MKn c TpeoyeMon TOYHOCTbIO WBocnpoN3BOANMOCTbIO.PekoMeHayeTca Mcnonb3oBaTb kpaHbl-a03aTopbl n BBona xKMaKnx npo6 noBopoT-Horo NnM nopwHeBoro Thna wnn aBToMaTnyeckne NHKeKTopbl.KpaH wnn NHKeKTop AOKHbI 6bITb o6opyo-BaHbl cekunen HarpeBaemoro wcnapntena,o6ecneynBalowe

30、ro HarpeB He HnxKe 285 C5.2 nuponn3Haa neybneub,o6ecneynBalowaa nonnepxkaHme TeMnepaTypbl(900 C),AoCTaTouHoM n nuponn3a Bcennpo6bl n oKncneHna cepbl B cepoconepxawnx coeAnHeHnax ao SO2.5.3 KBapueBaa Tpy6ka na cxnraHnKBapueBa Tpy6ka,BblnepxnBalowa HarpeBaHne o TeMnepaTypbl 1200 C.OKncnMTenbHas cekunaOMKHa 6bITb AOCTaTOYHo 6onbwon ana o6ecneyeHna nonHoro okncneHna npo6bl.2

展开阅读全文
相关资源
猜你喜欢
相关搜索

当前位置:首页 > 专业资料 > 国外标准

copyright@ 2008-2023 wnwk.com网站版权所有

经营许可证编号:浙ICP备2024059924号-2