1、 D6300-17a STANDARD PRACTICE FOR DETERMINATION OF BIAS DATA FOR USE IN TEST METHODS FOR PETROLEUM PRODUCTS LUBRICANTS 2017 ():16.11.2017:3316-17/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,
2、PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating Metrology under the license of American Society for Testing Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA
3、 19428,USA.ASTM International does not approve does not confirm these translations in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM Internation
4、al or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation international copyright.ASTM D6300-17a 1 D6300-17a 1 D6300;,.().,RR:D02-1007,2 ASTM ,2 ISO 4259,50-ASTM (IP).ISO 4259.ISO 4259 ,.1 ASTM D02 ,D02.94 .1 2017.2017.1998.2017.D 6300-17.DOI:10.1520/D6300-17.2 -ASTM Intern
5、ational RR:D02-1007.ASTM D6300-17a 2 RR:D02-10072 D3244 .,RR:D02-1007,2 ISO.1.1.1 (,)().1.2 ,().1.3 ,1.2,.1.4 -,(TBT).*ASTM D6300-17a 3 2.2.1 ASTM:3 D3244 D3606 D6708 D 7915 (GESD)E29 E177 ASTM E456,E691 2.2 ISO:ISO 4259 4 3 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.4 (A
6、NSI),25 W.43rd St.,4th Floor,-,NY 10036,http:/www.ansi.org.ASTM D6300-17a 4 3.3.1:3.1.1 (ANOVA),.ISO 4259 3.1.2 .3.1.2.1 ,.E 177 3.1.3 (),.D 6708 3.1.4 ,.3.1.4.1 .ISO 4259 3.1.5 ,;,5%(,20).3.1.5.1 ,ASTM D6300-17a 5 ,.,(1).5 3.1.6 ,.ISO 4259 3.1.7 ,x,x -,f(x)=(1/)(2)-1/2 exp-(x-)2/22(1)1 ,(0).ISO 425
7、9 3.1.8 ,.RR:D02-10072 3.1.9 .3.1.9.1 ,.,.5 .ASTM D6300-17a 6 .RR:D02-10072 3.1.10 ,.RR:D02-10072 3.1.11 (),5%(,20).3.1.11.1 ,95%.ISO 4259 3.1.11.2 ,.RR:D02-10072 3.1.12 ,.177 3.1.13 (),5%(,20).3.1.13.1 ,ASTM D6300-17a 7 ,95%.ISO 4259 3.1.13.2 ,.RR:D02-10072 3.1.13.3 ,-,-,(,).,.3.1.14 ,.2 ,.177 3.1.
8、15 ,ASTM D6300-17a 8 .ISO 4259 3.1.16 ,.ISO 4259 3.1.17 ,.RR:D02-10072 3.1.18 ,-,.ISO 4259 3.1.18.1 ,.,.3.1.16.2 ,.3.2 ,:3.2.1 ,.3.2.2 ,.3.2.3 ,ASTM D6300-17a 9 ,-;.3.2.4 ,.3.2.4.1 .,E29.4.4.1 ,.4.1.1 ,6.2.1.4.2 ,.4.3 .,.ASTM D6300-17a 10 5.5.1 ASTM ,.ASTM .().-.5.2 D02.3.(.1).1.()()()5.2.1 ,.ASTM D
9、6300-17a 11 ,.5.3 .,.5.4 D02 D02.ISO 4259 D02,:.RR:D02-1007.2 5.5 .E691,E11 .E691 ,.2.6.()6.1 :(.6.2),(,)(.6.3),(.6.4)(.6.5).ASTM D6300-17a 12 2.D6300 E691 E691 :k h ,.,.,.,.t2,t 95%-.2,8=1,962 12.6.2 .,.6.2.1 ,.ASTM D6300-17a 13 ASTM (A21.5.1).,6.3.6.2.1.1 :(1)(3),.(2)(12),.6.2.1.2 :(1)GESD D7915.(
10、2)(v)(s),.(3),:Fmax=vmax/vmin,vmax vmin .(4)Fmax 4,85,:=(v1+v2+v3)/30,5,v1,v2,v3 ;,ASTM D6300-17a 14,.(5)Fmax 4,85,.(6)Fmax 4,85,vmax ,:10smax/averagesample,smax (vmax)0,5,averagesample .1,.1,.(7)6.4.2,X2 .3 ,6.2.1.2(7),X2.6.2.1.3 ,().(X2),:ASTM D6300-17a 15 A 2 B 2,4,A B(B ,A ),.,.6.3 :6.3.1 :(1);(
11、2),;(3);(4).6.3.2 ,;12 -.-,.,().-,.ASTM D6300-17a 16 6.4 :6.4.1 (6),(8),(6),.6.4.2 .-,(h)(.2)0,5.30 ,.30 .,.1(.6.4.3),42.:(2)hii-i,n-,pi-i,xi-ln(pi),x-xi.ASTM D6300-17a 17 L=P=/Q=/.1 (.6.4.3)6.4.3 .1 ,L,P Q,L ,P Q ASTM D6300-17a 18 (.8.3.1),.P ,Q .4 X1 .Q P,30 ;.1 (20).,.,.6.5 :6.5.1 ,.,.6.5.2 .-,.6
12、.5.3 ,.,.:6.5.3.1 .,ASTM D6300-17a 19 ,.,.,.6.5.3.2 ;6.5.3.3 (MSDS),;6.5.3.4 ();6.5.3.5 ,.,-.,().,.6.5.3.6 ,;6.5.3.7 .ASTM D6300-17a 20 ,.,.6.5.3.8 ,.6.5.3.9 ,;.6.5.4 .,.,.6.5.5 ,.,.ASTM D6300-17a 21 7.7.1:7.1.1 ,(.6):7.1.1.1 ;7.1.1.2 ,.5 ,A1 (),A2.(8),A2.6 ,(.7.2).(),.(2).7.2 :7.2.1 ,.,.7.2.1.1 ,.,
13、ASTM D6300-17a 22 ,.,.,(GESD)(.D7915)99%-.,.7 ,GESD ,.,(3 2 ).,.7.2.2 Dj dj(.A1)mj.,m,.D=f1(m)d=f2(m),.7.2.3 D=f1(m)d=f2(m).ASTM D6300-17a 23 ,uj=jjDd mj,f1 f2,.,.,uj ,D=f(m)(D d)T.,(.A4.1).7.2.4 ,uj (mj),uj mj,log(uj)log(mj),A5.,7.2.5.7.2.5 D=f(m).,.A4.2,A4.3.D=f(m)A3.1.,(2),B B0.7.2.6 ,B,A3.2.(D=f
14、(m)m),5%-.,ASTM D6300-17a 24 A5.7.2.7 5%-,D=f(m),y=F(x),x ,(3)K=.,.A3.1.7.2.8 .,(.7.7).7.2.9 :7.2.9.1.3 m,D d ,A2,.3,D d m,m.(log D log d log m),(.A4.1 A4).A4.4 ,0,638.2/3.ASTM D6300-17a 25 (4)3.7.2.9.2 ,.,.,.A1.3,.7.3 :7.3.1 ,.,-.,.7.3.1.1 ,100(/,),.ASTM D6300-17a 26 7.3.2 .(3)eij2 /.1%-(.A1.5).A2.
15、2,n ,n 1,.,.,.7.3.3 ,A2,(),.A1.3,.4.0,078 G 3.0,0422+0,0212+.+0,0262+02=0,0439.,(5)0,138 ,.72 ,.A2.2 80 0,1709,.ASTM D6300-17a 27 4.:7.3.4 :7.3.4.1 ,.(4).7.3.4.2 ,(.7.6),()(A1.6).7.3.4.3,1%-.A1.5,n /(),v ,./v ,.7.3.4.4 ,ASTM D6300-17a 28.-,.7.3.4.5 ,.7.3.5 :7.3.5.1 .7.3.5.2 .5 .5 .5.:7.3.5.3 .D 1.:A
16、STM D6300-17a 29 (6)7.3.5.4 ,n=9 1 v=56 ,.A1.5 0,3729.,D 1.7.3.5.5 ,1 ,.,F 2.:(7)7.3.5.6 ,n=9 2 v=55 ,.A1.5 0,3756.,.7.4 :7.4.1 .,.7.4.2 -,.7.4.3 1%-,.ASTM D6300-17a 30 (,)(.A1.5).,.A2.2,n v,.,-(.7.1).7.4.4 ,.,F-v1 v2 (.A1.7).v1 ,v2 .,A2.6,0,01/S,S ,.7.4.5 :7.4.5.1 D 1 .6 .6.:7.4.5.2 ,.ASTM D6300-17a 31 ,.7.4.5.3 .7,100,.7.,7.4.5.4 ,93 15,76 .,.7.4.5.5 ,.,93,(8)7.4.5.6 (9)11,66 ,.7.4.5.7 .A1.8 ,0,01/8=0,00125,8 63 ,4.,93 .7.4.5.8 ,ASTM D6300-17a 32 ,.(93),2,972/(1,132+0,992+1,362)=0,510(10)0,352
