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ASTM_D_6299_-_22e1.pdf

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1、Designation:D6299221An American National StandardStandard Practice forApplying Statistical Quality Assurance and Control ChartingTechniques to Evaluate Analytical Measurement SystemPerformance1This standard is issued under the fixed designation D6299;the number immediately following the designation

2、indicates the year oforiginal adoption or,in the case of revision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.1NOTEEditorially corrected 3.3.8 in November 2022.1.Scop

3、e*1.1 This practice covers information for the design andoperation of a program to monitor and control ongoing stabilityand precision and bias performance of selected analyticalmeasurement systems using a collection of generally acceptedstatistical quality control(SQC)procedures and tools.NOTE1A com

4、plete list of criteria for selecting measurement systemsto which this practice should be applied and for determining the frequencyat which it should be applied is beyond the scope of this practice.However,some factors to be considered include(1)frequency of use ofthe analytical measurement system,(2

5、)criticality of the parameter beingmeasured,(3)system stability and precision performance based onhistorical data,(4)business economics,and(5)regulatory,contractual,ortest method requirements.1.2 This practice is applicable to stable analytical measure-ment systems that produce results on a continuo

6、us numericalscale.1.3 This practice is applicable to laboratory test methods.1.4 This practice is applicable to validated process streamanalyzers.1.5 This practice is applicable to monitoring the differencesbetween two analytical measurement systems that purport tomeasure the same property provided

7、that both systems havebeen assessed in accordance with the statistical methodology inPractice D6708 and the appropriate bias applied.NOTE2For validation of univariate process stream analyzers,see alsoPractice D3764.NOTE3One or both of the analytical systems in 1.5 may be laboratorytest methods or va

8、lidated process stream analyzers.1.6 This practice assumes that the normal(Gaussian)modelis adequate for the description and prediction of measurementsystem behavior when it is in a state of statistical control.NOTE4For non-Gaussian processes,transformations of test resultsmay permit proper applicat

9、ion of these tools.Consult a statistician forfurther guidance and information.1.7 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the Decision on Principles for theDevelopment of International Standards,Guides and

10、 Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade(TBT)Committee.2.Referenced Documents2.1 ASTM Standards:2D3764 Practice for Validation of the Performance of ProcessStream Analyzer SystemsD4175 Terminology Relating to Petroleum Products,LiquidFuels,and LubricantsD51

11、91 Test Method for Vapor Pressure of Petroleum Prod-ucts and Liquid Fuels(Mini Method)D6300 Practice for Determination of Precision and BiasData for Use in Test Methods for Petroleum Products,Liquid Fuels,and LubricantsD6617 Practice for Laboratory Bias Detection Using SingleTest Result from Standar

12、d MaterialD6708 Practice for Statistical Assessment and Improvementof Expected Agreement Between Two Test Methods thatPurport to Measure the Same Property of a MaterialD6792 Practice for Quality Management Systems in Petro-leum Products,Liquid Fuels,and Lubricants TestingLaboratoriesD7372 Guide for

13、Analysis and Interpretation of ProficiencyTest Program ResultsD7915 Practice for Application of Generalized ExtremeStudentized Deviate(GESD)Technique to Simultane-ously Identify Multiple Outliers in a Data SetE177 Practice for Use of the Terms Precision and Bias in1This practice is under the jurisdi

14、ction of ASTM Committee D02 on PetroleumProducts,Liquid Fuels,and Lubricants and is the direct responsibility of Subcom-mittee D02.94 on Coordinating Subcommittee on Quality Assurance and Statistics.Current edition approved May 1,2022.Published May 2022.Originallyapproved in 1998.Last previous editi

15、on approved in 2021 as D6299 21.DOI:10.1520/D6299-22E01.2For referenced ASTM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm.org.For Annual Book of ASTMStandards volume information,refer to the standards Document Summary page onthe ASTM website.*A Summary

16、 of Changes section appears at the end of this standardCopyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United StatesThis international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade(TBT)Committee.1ASTM Test MethodsE178

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