1、MEXTOCyAAPCTBEHHbM COBET No CTAHAAPTN3ALN,METPONOrN CEPT中KALN(Mrc)INTERSTATE COUNCIL FOR STANDARDIZATION,METROLOGY AND CERTIFICATION(ISC)FOCTMEKTOCyAAPCTBEHH bICTAHAAPT323342013MACJIA CMA3O4HbIEOnpegeneHne notepb oT cnapeHg HaTepMorpaBnMeTpn4ecKoM aHann3aTope(TGA)MeTogOM HoaKM3aHne onuanbHoeMocKBaCT
2、aHAapTHOPM2014FOCT 32334-2013npeAncnoBneLen,ocHoBHble npHynbi n nopAok npoBegeHnA paoT no MexrocyAapcTBeHHo cTaHAapTn3a-MM ycTaHoBneHbi OCT 1.0-92 MexrocyAapcTBeHHa ccTeMa cTaHAapTn3aynn.OcHOBHbIe nonoxe-HM OCT 1.2-2009 MexrocyAapcTBeHHa cncTeMa cTaHAapTn3ayn.CTaHAapTbi MexrocyAapcTBeH-Hble,npaBnna
3、n peKoMeHgaynn no mexrocyAapcTBeHHon cTaHAapTn3aynn.lpaBna pa3pa6oTkn,npnHa-T,nMeHeH,HOBneH OTMeHbCBegeH o cTaHapTe1 NOATOTOBJEH OTKpbITbIM aKyOHepHbIM 06eCTBoM BcepoccncKn Hay4HO-uccneoBaTenbcK HcTTyT no nepepa6oTke HeT(OAO BHM H)Ha OcHOBe co6CTBeHHoroayTeHT4Horo nepeBoga ha pyccKn A3bIK cTaHAapTa,
4、yka3aHHoro B nyHKTe 42 BHECEH 中egepanbHbIM areHTCTBoM no TexHn4eckomy perynnpoBaHnIo n MeTponornn3 PMHAT MexrocyAapcTBeHHbIM CoBeTom no cTaHgaptn3aynn,MeTponornn n ceprnonKaynn(npoToon N 60-oT 18 oKTa6pa 2013 r.)3a npHATe nporonocoBann:KpaTKoe HanMeHoBaHe cTpaHbI noKoA cTpaHbI noCokpaeHHoe HanMeHoBa
5、Hne HaoHanb-MK(MCO 3166)004-97MK(MCO 3166)004-97Horo opraHa no cTaHAapT3aApMeHAAMMH3KOHOMKn Pecny6nnKM ApMeHABenapycbBYFoccTaHAapT Pecny6nnkn BenapycbKnpr3AKGKbiprbi3cTaHAapTMongoBaMDMonAoBa-CTaHAapTPOCCARUPoccTaHAapTTaAKcTaHTJTaAKKcTaHAapTy36eKncTaHUZy3cTaHAapT4 HacTouni craHAapT nAeHTn4eH craHgapr
6、y ASTM D 6375-09 Test method for evaporation lossof lubricating oils by thermogravimetric analyzer(TGA)Noack method Merog onpegeneHnA noTepb oT uc-napeHA CMa304HbIX Macen Ha TepMorpaBnMeTp4ecKoM aHann3aTope(TGA)MeToAoM HoaK.CTaHAapt nogroToBneH KomTeToM ASTM D 02 HepTenpoAyKTb n CMa304Hble Matepnanb
7、 MHenocpeACTBeHHyO OTBeTCTBeHHOCTb 3a MeTOg HeceT nOAKOMMTeT D02.06 AHann3 cMa304HbIX MaTepna-nOB.epeBog c aHrnckoro 3bika(en).HanmeHoBaHne HacToA山ero MexrocyAapcTBeHHoro cTaHAapTa 3MeHeHO OTHOCTeNbHO HanMeHO-BaHnA yka3aHHoro cTaHgapta An npnBegeHn B cooTBeTcTBe c OCT 1.5-2001(nopa3gen 3.6).OnnanbHb
8、le 3K3emnnpbi cTaHAapTa ASTM,Ha ocHoBe KoToporo nogroToBneH HacToq Mex-rocyAapcTBeHHbi cTaHAapt,u cTaHgapToB ASTM,Ha KOTopble gaHbi CCbinkn,nMeoTCA B eAepanLHOMMHopMaLOHHOM OoHAe TexHnecKnX pernaMeHTOB cTaHAapToB.CBegehnA o cooTBeTCTBn MexrocyAapcTBeHHbiX cTaHAapTOB CCbino4HbiM cTaHAapTaM npnBeAeHbI
9、B AononHTenbHOM npnoeH.A.CTeneHb cooTBetctB-AeHT4Ha(IDT)5 门lpnka3om 中egepanLHoro areHTcTBa no TexHn4eckomy perynnpoBaHnio n MeTponornn oT 22HoA6pA 2013r.Ne 690-cT MexrocyAapcTBeHHbiM cTaHAapT OCT 32334-2013 BBeAeH B AecTBne BkayectBe HauoHanbHoro cTaHAapta PoccncKon Pegepaunn c 01 HBapa 2015 r.6 BBE
10、AEH BNEPBbIEFOCT32334-2013MHpopMayuA 06 u3MeHeHuAx K HacmogeMy cmaHdapmy ny6nukyemcA e exe2odHoMuHpopMaquOHHOM yKa3amene HayuoHanLHbie cmaHdapmb,a mekcm u3MeHeHu u nonpaeok-eexeMecA4HOM uHopMayuoHHoM yka3amene HaquoHanLHbIe cmaHdapmbI.B cny4ae nepecMompa(3aMeHbi)unu omMeHbI HacmoRuwe2o cmaHdapma coo
11、meemcmeyiouwee yeedomneHue 6ydemony6nukoeaHo e exeMecA4HOM uHpopMayuOHHOM yka3amene HauuoHanLHbie cmaHapmbi.Coomeemcmeyiouwas uHpopMayu,yeedoMneHue u mekcmbi pa3meaomcs makke e uHopMayuOHHocucmeMe o6we2o nonL3oaHuR-Ha opuuanLHoM calume PedepanbHo2o a2eHmcmea no mexHu4eckoMypezynupoeaHuo u Memponozuu
12、 e cemu HmepHemCTaHAapTHopM,2014B Poccnckon Pegepaun HacToAu cTaHgapT He MOeT ObITb NONHOCTbo Mn yacTM4HOBOcnpoM3BegeH,TpapoBaH n pacnpocTpaHeH B Ka4ecTBe oManbHoro 3AaHnA e3 pa3peweHA中egepanbHoro areHTcTBa no TexHeckoMy perynpoBaHIo n MeTponornnFOCT 32334-2013ME KTOC YA APC TBEHHbIMC TAHAAPTMACJIA
13、CMA3O4HbIEOnpegeneHne noTepL oT ncnapeHnA Ha TepMorpaBnMeTpn4eckoM aHann3aTope(TGA)MeTogoM HoaKLubricating oils.Determination of evaporation loss of by thermogravimetric analyzer(TGA)Noack methodAaTa BBeAeH-2015-01-011 06nacTb npuMeHeH1.1 HacTo cTaHAapt ycTaHaBnnBaet MeTog onpegeneHnA notepL oT ncna
14、peHA MeTogom Ho-aK c ncnonb3oBaHeM TepMorpaBnMeTp4eckoro aHann3aTopa(TGA)n pacnpocTpaHAeTcA Ha a3oBble nToBapHble CMa304Hble Macna,nMeloune Anana3oH noTepb oT ncnapeHnA no Hoak oT 0%macc go 30%Macc.OnpegeneHue no AaHHomy meTogy tpe6yet He6onbworo o6bema o6pa3ya u npn nocneAoBatent-HOM aHanM3e HecKon
15、bKnX 06pa3yoB CnbITaHMe BbinonHgeTcA 6bicTpee n 6e3onacHee cTaHAapTHoro MeTo-Aa Hoak c ncnonb3oBaHneM cnnaBa Bya.1.2 loTepu or ucnapeHn,onpeAengembie no HacToqueMy cTaHgapTy,cooTBeTcTByoT noTepAM,onpegengeMbim no cTaHAapTHbim MeTogam CnbitaHni no MeTogy Hoak.1.3 3Ha4eHnA B cncTeMe eAnHny C paccMaTpB
16、aoT KaK cTaHAapTHble.1.4 B HacToLem cTaHAapte He npeAycMoTpeHO paccMoTpeHne Bcex BonpocoB o6ecne4eHnA Ge3-onacHOCTM,CB3aHHbiX c ero npMeHeHMeM.门oNb3oBaTenb HacToguero cTaHgapTa HeceT OTBeTcTBeH-HOCTb 3a ycTaHoBneHe cooTBeTcTByounx npaBnn no TexHKe be3onacHOcTn n oxpaHe 3gopoBbA,a Takkeonpegenget yen
17、ecoo6pa3HocTb npMeHeHnA 3aKoHoAaTenbHbix orpaHn4eHn nepe ero ncnonb3oBaHeM.2 HopMaTBHble ccbInKMAng npMeHeHnA HacTouero cTaHAapTa HeooxoAnMbi cneAyioue ccbino4Hble goKyMeHTbi.AnHeAaTpoBaHHbix ccbinoK npnmeHAioT nocneqHee n3AaHne ccbino4Horo gokyMeHTa(Bknio4a Bce ero n3-MeHeHn)1):ASTM D 5800 Test met
18、hod for evaporation loss of lubricating oils by the Noack method(MeroAonpegeneHn notepb oT ucnapeHA cMa304HbIx Macen no MeTogy Hoak)ASTM D 6299 Practice for applying statistical quality assurance and control charting techniques toevaluate analytical measurement system performance(lpakTka npMMeHeHMA
19、MeTOAOB cTaTCTMeckoroKoHTpong Ka4ecTBa KoHTponbHbix Kapt An oyeHKn xapaKTepcTnK aHanTecKon CCTeMbI 3MepeHA)ASTM D 6792 Practice for quality system in petroleum products and lubricants testing laboratories(门paKTuKa cncTeMbi KayecTBa cbiITaHn HeTenpogyKToB n cMa304HbIX MaTepnanoB B na6opaTopnx)ASTM E
20、1582 Practice for calibration of temperature scale for thermogravimetry(pakrnka kanw6-poBKn TeMnepaTypHo wKanbi An TepMorpaBnMeTpn)门p n M e 4 a H ne-门pn nonb3oBaHnn HacTOA(MM cTaHAapToM yenecoo6pa3Ho npoBepNTb AecTBne ccbi-no4HbIX cTaHAapToB B HPopMaLMOHHon ccTeMe oowero nonb3oBaHA-Ha opnynanbHoM ca
21、nte OepepanbHoroareHTcTBa no TexHMueckoMy perynnpoBaHno n MeTponorM B ceT VHTepHeT nM no exeroAHoMy HOOpMaOHHOMyya3aTenio HaoHanbHble cTaHgapTbi,KoTopbin onyonnKoBaH no cocToAHHo Ha 1 HBap tekyuwero roga,n no Bbi-nyckam exeMecq4Horo HpopMaynoHHoro yKa3aTeng HayMoHanbHble cTaHAapTbi 3a Tekywn rog.Ecn
22、n ccbIno4HbicTaHAapT 3aMeHeH(M3MeHeH),To np nonb3oBaHM HacTOALLMM CTaHAapTOM cneAyeT pyKOBOACTBOBaTbCA 3aMeHHO-MM(3MeHeHHbIM)cTaHAapToM.Ecnn ccbino4HbIN cTaHAapT OTMeHeH 6e3 3aMeHbi,To nonoxeHne,B KOTopoM AaHaccbinka Ha Hero,npMeHgeTcA B act,He 3aTparnBaowen 3Ty ccbinky.CcInKn Ha cTaHAapT ASTM MoxHo
23、 yTo4HNTb Ha caite ASTM website,www.astm.org nnn B cnyx6e noepxknknneHToB ASTM serviceastm.org,a Takke B nHpopMayoHHOM ToMe ekerogHoro copHnKa cTaHAapToB ASTM(Website standards Document Summary).M3aHne ouanbHoeOCT 32334-20133 TepMHbI onpeeneHgB HacToAeM cTaHgapTe npMeHeHbi cneAylouMe TepMMHbI C COOT
24、BeTCTByHOMMonpegeneHAM:3.1 3TanoHHoe Macno Ang cnbITaH MeTogoM Hoak(ganee-aTanoHHoe Macno)(Noack ref-erence oil):Macno,nocraBngemoe npon3BoguTenMn o6opygoBaHMA An MeToga Hoak,ucnonb3yeMoeAn npoBepkn pa6oTocnoco6HocTn aHann3aTopa noTepL oT cnapeHnA.3.2 cTaHapTHoe BpeMA cnbITaHA MeTogoM HoaK(ganee-cTa
25、HAapTHoe BpeM)(Noack ref-erence time):BpeMa,B MnHyTax,Heo6xogumoe Ang goctxeHA 3TanoHHbIM MacnOM n3BeCTHOTO 3Ha4eHnAnoTepb oT cnapeHng B ycnoBnx HacToguwero MeToga ncnbiTaH.3.3 neTy4ectb p cnbITaHnn MeTogoM HoaK c ncnoNb3oBaHMeM TepMorpaBnMeTpnecKoroaHann3aTopa(TGA Noack volatility):loTepn oT ncnape
26、HnA cMa3o4Horo matepnana,B npoueHTax no mac-ce,onpegeneHHble no HacToueMy cTaHAapTy.4 CyHOCTb MeToa4.1 O6pa3ey cma3o4Horo macna nomewaioT B TnrenL TepMorpaBnMeTpn4eckoro aHann3aTopa.Tn-renb ycTaHaBnMBaoT Ha gepkaten Turng TepMorpaBnMeTpueckoro aHan3aTopa n ObicTpo HarpeBaoT Bnotoke Bo3gyxa go Temnep
27、atypbi oT 247 C go 249 C,3aTem BbiAepxnBaioT B Te4eHMe 3aAaHHoro BpeMe-Hn np ycTaHoBneHHoM TeMnepaType.p HarpeBaH TepMorpaBnMeTpecK aHann3aTop KOHTponpy-et n perncTppyet noTepn maccbi o6pa3ya or ncnapeHA.3aTem no TepmorpaBnMerpn4ecKo KpnBoonpegengioT noTepn Maccbi o6pa3ya(%)OT BPeMeH.5 Ha3Ha4eHne n
28、cnonb3oBaHne5.1 Hacoqu meog onpegeneHn aBngeTca e3onacHo n 6bictpo antepHaTnBHo meToAn-Kon onpegeneHnA notepb oT cnapeHA CMa3o4HbIX MaTepnanoB MeToAOM HoaK.5.2 3HayeHne noTepb oT cnapeHnA gBngeTcA BaxHbim napameTpoM cMa3o4Horo Matepnana,nc-nonb3yemoro B ropg4nx 30Hax o6opyAoBaHMA,B KoTopbix ncnapeHn
29、e cMa3o4Horo MaTepnana MokeT np-BeCT K yBenneHHo ero pacxoga.5.3 B cneynnKaynAx Ha cMa304Hble MaTepnanbi ycTaHaBnnBaioT 3Ha4eHne MaKcManbHO gony-CTMbIX noTepb OT cnapeHA.6 Annaparypa6.1 TepMorpaBnMeTpnueckn aHann3aTop c nporpaMMHLIM ecne4eHneM,cOOTBeTCTByIO山 Tpe-6oBaHAM HacTowero cTaHAapTa.6.2 AnoMH
30、eBbi Trenb An 06pa3uaAnoMnHneBbi yunnHApnyeckn tureNt c oThOweHNeM BHyTpeHHero Anametpa k BbicoTe He onee0,45,BMeCTuMOCTbo(503)cm3.Ecn turnn,nocTaBngemble npon3BoAnTenAMn TepMorpaBnmeTpn4ecknxaHann3aTopoB,He cooTBeTcTByot 3tm napaMeTpaM,MOHO cnonb3oBaTb n agantpoBatb Ana ycTaHoB-kn B Aepxatent TepmorpaBnmeTpneckoro aHann3aTopa Apyre Turnn.pnMepbi anTepHaTnBHbiX TnrneMnpnBeeHbl Ha pncyHke 1.1231-npoBono4haa nogBecka;2-anbtephatBhble turnn An o6pa3yoB;3-ctaHgapthble turnn An o6pa3yoB,no-cTaBnAeMble B KoMnnekTe c TepMorpaBMeTpecKM aHann3aTopOMPcyHOK 1-pMepbi anbTepHaTBHbIx Turne An 06pa3ya2
