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2、CHOBHble npNHunnbl N nopanok npoBeneHna pa6oT no MexkrocynapcTBeHHoN CTaHnapTn3aunnycTaHoBneHbl OCT 1.0-92 MexkrocynapcTBeHHa CncTeMa CTaHAapTn3aunn.OCHOBHble nonoxkeHWOCT 1.2-2009 MexkrocynapcTBeHHas cncTeMa cTaHAapTn3auwn.CTaHAapTbl MexkrocyAapcTBeHHble,npa-Bnna n peKoMeHnaunn no MexkrocyAapcTBeHH
3、on cTaHnapTn3aunn.npaBnna pa3pa6oTKn,npnHaTn,npnMe-HeHNA,O6HOBneHNA M OTMeHbICBeneHNa o cTaHAapTe1 nOFOTOBNEH OTKPbITbIM akuNoHepHbIM 06weCTBOM BcepoccnncKNN Hay4Ho-wccnenoBa-TenbCKnN MHCTNTyT no nepepa6oTKe HedTn(OAO BHMM Hn)Ha oCHOBe co6CTBeHHoro ayTeHTM4HoronepeBoAa Ha pyccKnn 93blK cTaHnapTa,yKa
4、3aHHoro B nyHKTe 42 BHECEH enepanbHbIM areHTCTBOM no TexHNyeCKoMy perynnpoBaHnlo n MeTponornn3 nPMHAT MexkrocynapcTBeHHbIM coBeTOM no cTaHnapTn3aunn,MeTponornn n cepTnonkaunn(npoTokon oT 14 Ho96pa 2013r.Ne 44)3a npNHATne nporonocoBanw:KpaTkoe HawMeHOBaHwe CTpaHblKon cTpaHblCokpaweHHoe HanMeHoBaHne H
5、aunoHanbHoro opraHan0MK(MC03166)004-97noMK(MC03166)004-97no CTaHnapT3aunApMeHNAAMMWH3KOHOMNKN Pecny6nNKn ApMeHN9Knpr319KGKblprbl3CTaHgapTPoccMaRUPoccTaHnapTTanxnKnCTaHTJTanknKcTaHnapTy36ekncTaHUZy3cTaHnapT4 HacToaunn cTaHnapT waeHTwueH cTaHnapTy ASTM D 4530-11 Standard test method fordetermination o
6、f carbon residue(micro method)CTaHnapTHbIN MeToA onpeneneHna KoKcoBoro ocTaTka(MWK-pomeTo).CTaHnapT pa3pa6oTaH KoMNTeTOM ASTM D02 no HedTenpoayKTaM n cMa3o4HbIM MaTepnanaM,wHenocpeACTBeHHyIo OTBeTCTBeHHOCTb 3a MeToA HeceT noAKoMMTeT D02.06 AHanM3 CMa304HbIX MaTe-pwanoB.nepeBon c aHrnwnckoro 93blka(e
7、n).HanMeHoBaHne HacTogwero cTaHnapta N3MeHeHo OTHOCNTenbHO HanMeHoBaHNA yKa3aHHoro cTaHnap-Ta ana npuBeneHna B cooTBeTCTBMe crOCT 1.5-2001(noApa3nen 3.6).OdnunanbHble 3K3eMnnapbl cTaHnapTa ASTM,Ha ocHoBe KoToporo nonroToBneH HacToAwNN Mexkrocy-apcTBeHHbIN cTaHnapT,ncTaHnapToB ASTM,Ha KoTopble naHbl
8、ccbinkn,WMelOTCA B enepanbHOM NHdopMa-LNOHHOM OHne TexHNyeCKnx pernameHToB M CTaHnapToB.CBeneHNA O COOTBeTCTBNN MexkrocynapcTBeHHbIX cTaHnapToB cCblnoyHbIM CTaHnapTaM npnBeneHbl BnononHNTenbHoM npnnoxkeHWN A.CTeneHb COoTBeTCTBNA-MAeHTNYHa(IDT)5 npnka3oM enepanbHoro areHTCTBa no TexHMuecKoMy perynnpo
9、BaHnio n MeTponornn OT 22 Ho96pa2013r.Ne 689-CT MexrocynapcTBeHHbin cTaHnapTrOCT 32392-2013 BBeAeH B nencTBne B KayecTBe Hauno-HanbHoro cTaHAapTa Poccnnckon enepaunn c 1 AHBapa 2015r.6 BBENEH BNEPBbIE0CT32392-2013MHobopMauua o6 u3MeHeHuax K HacmoaweMy cmaHoapmy nyonukyemca e exe200HOM UHobopMauuoH-H
10、OM yka3amene HauuoHanbHble cmaHdapmbl,a mekcm u3MeHeHuu unonpaBok-BexkeMecAYHOM UHobop-MauuoHHOM yka3amene HauuoHanbHble cmaHdapmbI.B cnyyae nepecMompa(3aMeHbI)unu omMeHblHacmoswe2o cmaHdapma coomeemcmeylowee yeedomneHue 6ydem ony6nukoeaHo 6 exemecayHoMuHc中opMauuOHHOM yKa3 ameneHauuoHanbHb/e cmaHdap
11、mb/.Coomeemcmeylowaa uHg中opMauus,yBe-doMneHue umekcmbl pa3Mewalomca makke 6 uHobopMauuoHHou cucmeMe oowe2o nonb3o6aHua-Ha ocbu-uuanbHOM caume edepanbHo2o a2eHmcmea no mexHuyeckoMy peaynupoeaHulo u Memponoauu e cemuMHmepHemCTaHAapTMH中opM,2014B Poccnnckon enepaunn HacToaun cTaHnapT He MoxeT 6bITb nonH
12、OCTblo wnn yacTNHO Bocnpon3Be-neH,ThpaxknpoBaH n pacnpocTpaHeH B kayecTBe odnunanbHoro M3naHna 6e3 pa3peweHna enepanbHoroareHTCTBa no TexHNyeckoMy perynnpoBaHnio N MeTponornWFOCT 32392-2013CoAepaHne1 06nacTb npMeHeHg.2 HopMaTBHble ccbInK.3 TepMHb n onpegeneH4 CyHOCTb MeToAa.5 Ha3HaeHe cnonb3oBaHne6
13、Annaparypa.7 OT6op npo6.8 poBegeHe ncnbiTaHg.9 OnpegeneHne KokcoBoro octatka B 10%-HoM(no 06LeMy)octatke ot pa3roH10 BbI4cneHe.。.-.11 OopMneHe pe3ynbTaToB.12 门peLN3MOHHOCTb N CMeeHne.7pnnoxeHn X(cnpaBo4Hble).9X1 VHpopMayuA o6 nccnegoBaHnn koppengyun pe3ynbtatoB cnbitaHnA.9X2 PeKoMeHgaynn Ang aHanntn
14、ka.10pnnoxeHne AA(cpaBo4Hoe)CBeAeHnA o cOoTBeTcTBnn MexrocyAapcTBeHHbIX cTaHAapToBCCbIN04HbIM CTaHAapTaM.11IV0CT32392-2013M E X rO C yA P C T B E HH bIC T A HA P THETEnPOnyKTbIOnpeneneHne KokcoBoro ocTaTka MWkpoMeToDOMPetroleum products.Determination of carbon residue by micro methodAaTa BBeneHna-20
15、15-01-011 06nacTb npnMeHeHnA1.1 HacTogwnn CTaHnapT ycTaHaBnnBaeT MeTon onpeneneHna conepxaHn KoKcoBoro ocTaTka(MWK-poMeTo),o6pa3oBaBweroca nocne BbinapnBaHna N nwponv3a HedTenponyKToB npn ycTaHoBneHHbIX ycno-BNAX,wnpe Ha3HayeH nn onpeneneHnA CKnOHHOCTN TaKnx nponyKToB Ko6pa3oBaHnlo KoKca(npnMeyaHne
16、1).1.2 Pe3ynbTaTbl ncnblTaHwa no HacTogweMy CTaHAapTy 3KBMBaneHTHbl pe3ynbTaTaM NcnblTaHNA Cncnonb3oBaHneM MeTona KoHpancoHa no ASTM D 189n p n M e 4 a H M e 1-MeTog npencTaBnaeT co6on Mognonkauwio nepBoHauanbHoro TepMorpaBnMeTpnueckoroMeTopa M annapara a onpepeneHn KOKCoBoro ocTaTka B HedTenpopyKTa
17、x).na nonyueHn 3KBMBaneHTHblx pe3ynbTa-TOB npn Ncnonb3oBaHNn TepMorpaBnMeTpnueckoro MeTona ycnoBna NcnbITaHnA nonxkeH onpenenATb aHanNTNK.1.3 HacToawnn MeTon ncnblTaHa MOXHo ncnonb3oBaTb n ncnblTaHna HedTenpoAyKTOB,KoTopbleHacTNYHo pa3naraloTca npn neperoHke npn aTMocoepHoM naBneHwn N KOTopbIX 3Haye
18、HNA KOKCOBOrOOCTaTKa HaxoAaTca BAMana3oHe oT0,10%Macc.Ao 30%Macc.O6pa3ubl,Ana KoTopblx npennonaraeMoe 3Ha-eHNe KoKcoBoro ocTaTka MeHee 0,10%Macc.,npenBapNTenbHoneperoHAOT nA OTroHa 90%06beMa npo6bl(CM.pa3nen 9).3aTeM 10%-HbIn oCTaToK B Kon6e aHanv3npyloT ana onpeneneHna KoKcoBoro OcTaTka noHacToAweM
19、y MeTony WcnbITaHNA.1.4 3ona,onpeneneHHa no ASTM D 482,n TpyAHo ncnaparowneca npncankn MoryT 6bITb BKnoyeHbl Bobwee conepxkaHve KokcoBoro ocTaTka.1.5 n An3enbHoro TonnnBa,conepkawero anknnHnTpaTbl(aMnnHNTpaT,reKcnnHNTpaT wnn oKTMn-HNTpaT),3HayeHN KOKcoBoro ocTaTKa 6onbwe,yeM y TonnnBa 6e3 npncanKn,4
20、To MoXKeT npnBecTn K own604-HOMy 3aknioyeHNIO o CKnOHHOCTN TonnNBa K o6pa3oBaHniO KoKca.ConepxaHne anknnHNTpaToB B TonnNBeonpenenaioT no ASTM D 4046.1.6 3HayeHNa B CNCTeMe ennHny CM paccMaTpnBaloT Kak cTaHAapTHble.1.6.1 VcknioyeHne-B 6.4 n6.5 ncnonb3yioT eAHnubl n3MepeHna AioNMbl-yHTbl.1.7 npenynpex
21、neHne-ycTaHoBneHo,YTo pTyTb ABngeTca onacHbIM BewecTBOM,KoTopoe MoxeTBbl3BaTb nopaxkeHne ueHTpanbHon HepBHoN CNCTeMbl,noyek w neyeHn.PTyTb wnn ee napbl onacHbln 30-poBba n oKa3blBaHOT arpeccNBHoe Bo3neNcTBNe Ha Matepvanbl.npn obpaweHnn c pTyTblo nponyKTaMn,conepxkawlMN pTyTb,npWHWMalOT COOTBeTCTByHO
22、wNe Mepbl npenocTopoKHOCTN.nonpo6Hble yka3aHna naHblB nacnopTax 6e3onacHOCTN COOTBeTCTByOwNx MaTepnanoB(MSDS).nonb3oBaTenn nonxKHbl yyNTbIBaTb,4TOnponaxka pTyTn w/wnn nponyKToB,conepxkawx pTyTb,MoxkeT 6bITb 3anpewleHa 3aKoHonaTenbCTBOM.1)CM.&TonnMBa,TOM 63,mionb 1984 r.,C.931-934.DenapTaMeHT HayHblx nccnegoBaHnn,Esso PetroleumCanada,PO Box 3022,CapHn,OHTapno,N7T 7M1,KaHana.AocTynHo B MHTepHeTe c 12 aBrycra 2003 r.M3 naHne o中unanbHoe
