1、 D4483-18 ,STANDARD PRACTICE FOR EVALUATING PRECISION FOR TEST METHOD STANDARDS IN THE RUBBER AND CARBON BLACK MANUFACTURING INDUSTRIES 2019 ():08.04.2019:3644-19/ASTM Web:www.interstandart.ru -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM Internati
2、onal)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM Int
3、ernational)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the spec
4、ified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D4483-18 1 D4483-18 ,1 D4483;,.().,ASTM ,E691.,.,E691 ,.1 ASTM D11 ,D11.16 .1 2018.2018.1985.2014.D4483-14.DOI:10.1520/D4483
5、-18.ASTM D4483-18 2 D4483,D11,1985.D4483 ,E691.D4483,(ITP).-,:.,.(),.-,2:(1),(2).(1),.ASTM E11 .-,(2)(ITP ).,.,ASTM D4483-18 3 ,.1.1.1 (ITP).,.E691.,.1.2 ,.,.1.3 (),.-,.-,.h k ASTM D4483-18 4 .(-).1.4 :1 2 3 4 5 (ITP)6 :1 8 8.1 8.2 5%-8.3 h k R1 8.4 1 2 :2 9 R1 9.1 2%-9.1 h k R2 9.1.2 1 2 :3 10 R2 1
6、0.1 11 12 13 ,A1 A2 h k A3 ,A4 ,A5 A6 1.5 6,.A1 A2 ASTM D4483-18 5,.A3-A5 .,.A6 .,.1.6 ,.,.1.7 -,().2.2.1 ASTM:2 D1646 ,()2 STM,ASTM www.astm.org STM serviceastm.org.STM.Document Summary ASTM.ASTM D4483-18 6 D6600 E691 2.2 ISO:3 ISO 289 3.3.1 .3.1.1 ,.,.3.1.2 A1 .:(1),(2),.3.2,:3.2.1 3 (ISO),1,ch.de
7、 la Voie-Creuse,Case postale 56,CH-1211,Geneva 20,Switzerland,http:/www.iso.ch.ASTM D4483-18 7 .,.3.2.2 ,.(.),()().3.2.2.1 :,.3.2.3 (),.3.2.3.1 ,.3.2.4 ,.3.2.4.1 ,.(,).3.2.5 .(,),(,),.3.2.5.1 ,(,ASTM D4483-18 8).,.3.2.5.2 ,.3.3 :3.3.1 (),-.3.3.1.1 ,.,.3.3.2 .,.3.3.2.1 ().().(A1).,.3.3.3 ;(,).3.3.3.1
8、 ASTM D4483-18 9 .,.().,.5.1.4.1.3.3.4 (),(n=1,2,3 .).,()().3.3.5 (),.3.3.5.1 ,.3.3.3,.5.1.4.1.-ITP,(,).().3.3.4.3.3.6 ()-,.3.3.6.1 ().3.3.7 (),.ASTM D4483-18 10 3.3.7.1 :,(ISO).3.4 ,:3.4.1 (),n ;n,().3.4.1.1 ().n 1 10.,()+Bi,=,Bi=.,.A1.2.5 A1.2.6.A2.3.4.2 ,.3.4.3 (),.3.4.3.1 ,.,.ASTM D4483-18 11 3.
9、4.4 ,;.3.4.4.1 ().,.3.4.5 ,.3.4.5.1 ,-(.A1).,.3.5:.(),.:,.3.5.1 ,(),.ASTM D4483-18 12 3.5.1.1 ,.,.,.,.,.;().D6600.3.5.2 (r),();(95%-)(),.3.5.3 ,(R),(),;(95%-)(),.3.5.4,r ,n (),;ASTM D4483-18 13 (95%-),.3.5.4.1 ,.,.,().,.3.5.4.2 ,3.5.4,.,()N ITP.,.()(),-ITP.-,.,-.3.5.5,R ,N (n ),;ASTM D4483-18 14 (95
10、%-),.3.5.5.1 n ().N ().,.().,().3.5.5.2 ,.,.,%(,%,%.),.3.6 ,5.1.,.ASTM D4483-18 15 4.4.1 ,.,().4.2 :(1),(2),.,.ITP (,),ITP.4.3,.(1-4)4 ,ITP .().ITP,7.4,-.ASTM D4483-18 16 4.4 .,.5.:5.1 :.11.,4 .ITP .ITP h k ,A3.5.1.1 ,.,.1 .2 .ITP ().,(),.,ASTM D4483-18 17 ,ITP.A3 A5.5.1.2 :(),(,pH .),(,).,()().-,.,
11、8-10.5.1.3 (),.(,).:(1),(2),(3)()ASTM D4483-18 18 ,(4)(),(5)()(),.5.1.4 ,.,.(),.,.5.1.4.1 (),.,().5.1.5 :5.1.5.1 1 ,.,.5.1.5.1.1 ,ASTM D4483-18 19 .5.1.5.2 2 ,;,.,.5.1.6 .:-(SBR),.1 ,-.,.,1.5.2 ,.ITP 4,.,ITP.,.11.ASTM D4483-18 20 6.6.1 ITP,:6.1.1 ,.,().ITP ,.6.1.2 ITP ,.ITP .,5.1.5.1.,2.6.1.3 .,-.,.
12、ASTM D4483-18 21 6.1.3.1 11.6.1.4 ,.(),.n,.ITP n=2.3 4,.6.1.5 ,.()1 7.(,).(,).e .6.1.6 ,.,.,ASTM D4483-18 22 5.1.6.1.7 ,.,.,-(),.2 -,.6.1.8 ()ITP 6,.12 18.,(),.6.1.9 ,-ITP,.().ASTM D4483-18 23 .6.1.10 ITP ,.,.(,),.ITP ,ITP.6.1.11 ITP ITP.,.(),(),().(,),-,.ITP.ASTM D4483-18 24 7.7.1 ITP.().().,1.,2 3
13、 ,.A4 .r R,.1.1 (),.7.1.1 -ITP.(,).()(,).(.8.1.3).ASTM D4483-18 25 A6.1-ITP 7.1.2 1 ()ASTM D4483-18 26 h k.A3.A4 ,h k .h k h k 5%-.-.,.,.-,2.1.A (j)=(i)1 2 3 4.q 1 2 Yijk 3 4 5 .P A ITP .:,p,L(i)=1,2,3,.p ,q,m(j)=1,2,3,.,q,n ;=L(i),m(j);n=2 Yijk-;k=1,2,.n(ij);,(23)(i,j),n ,.7.1.3 2 -5%-,(1)(1),(2)(2
14、)A3,A5 5.1.1.,R1(Revision 1),ASTM D4483-18 27 .h k,h k 2%-.,.R1 .,3.7.1.4 3 -h k h k 2%-,(1)(1),(2)(2).,R2 .1 ,ASTM E11 .STM.(5).ASTM .8.1 A4.7.1.5 ,r,R,(r)(R)()ITP .-,ITP :ASTM D4483-18 28 -.-,ITP ,.,ITP ,.,-.7.2 A2 ,.A2.5 .,.7.2.1 SL2 A2.5.1.,.SL2 ;,SL2 .,.(.,),SL2 ,().7.3 ASTM D4483-18 29 -.,.,.,
15、().,.,.,(),.7.4 :(1)(,20 .1),(2).,20 .,.,.7.5 1 ,.,ITP .,.ASTM D4483-18 30 ,0,5%(p=0,005).-,ITP .E691.,.7.6 2 ,.:5%-.p=0,05,.95%-().,.7.6.1 ,.()-.,.ASTM D4483-18 31 7.7 5%-5%-.,h k ().-(h k),(h k).7.7.1 5%-R1(Revision 1)()h,k,.,ITP.:R1 h k,h k.7.7.2 ITP,.().,.2%-.ITP,6,.7.8 (12 )ASTM D4483-18 32 (),
16、3 (h/k).,h k(),.h k h k,5%-2 2%-.(2004.),2 ,.,(),.8.:1 8.1 1,.;.1 .p q ().pq.(ASTM D4483-18 33-)n.Yijk.2,.n=2.2.A (j)=(i)1 2 3 4.q 1 2 Yijk 3 4 5 .p A ITP .:,p,L(i)=1,2,3,.p ,q,m(j)=1,2,3,.,q,n ;L(i),m(j);n=2 Yijk-(ij)n .8.1.1 ,.2 n .,8.1.3.1 8.3 8.4.A3.8.1.2 .3 ,n .,w .,.1 ASTM D4483-18 34 8.3 8.4.A3.3.(j)=(i)1 2 3 4 q 1 2 Yijk 3 4 5 p A ITP .:,p,L(i)=1,2,3,.p ,q,m(j)=1,2,3,.,q,n ;L(i),m(j);n=2 Yijk-(ij)n .8.1.3 ,.,.,.(1 N),.ASTM D4483-18 35 8.1.3.1 ()(),.(,),.(AOT).8.1.3.2 ITP ,.,.().A5.8.2 .A