1、:D 4045-15 STANDARD TEST METHOD FOR SULFUR IN PETROLEUM PRODUCTS BY HYDROGENOLYSIS AND RATEOMETRIC COLORIMETRY ():2742-15/ASTM :19.10.2015 2015 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken
2、,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Consho
3、hocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for
4、 ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 4045-15 1 :D 4045-15 1 D 4045;,.().1.*1.1 0,02/10,00/.1.2 .1.3 ,30 371 (86 F 700 F).,-1 ASTM D02 ,D02.03 .1 2015.2015.1987.2010.D4045-04(2010).DOI:10.1520/D4045-15.
5、ASTM D 4045-15 2,.1.4,.1.4.1 (5.5).1.5 ,.,.2.2.1 ASTM:2 D 1193 D 6299 3.3.1 ,.1300 ,(H2S).H2S .2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 4045-15 3 ,.4.4.1 .4.2 .5.3,4 5.1 ,900 1400 5 .,550,.(.1).;1250.5.2 H2S H2S .H2S 3,5.1 5.4.,Analytical Systems Keco,9215 Solo
6、n Rd.,Suite A4,Houston,TX 77064.Drushel,H.V.,Trace Sulfur determination Petroleum Fractions,Analytical Chemistry,Vol.50,1978,p.76 4 ,Analytical Systems Keco.,-ASTM International.1,.ASTM D 4045-15 4 ,.,0,1/(.2).1 .1 .2 H2S ASTM D 4045-15 5 5.3 ,550.100-3/25-.(,.)5.4 .,.6/0,06/6.5.5 10 10000 ,0,2 1/(0
7、,5 3/).,.5.6 ,500 1400,250 .,316,1/16 (1/6).6 6.1 .,(ACS),ASTM D 4045-15 6 .5 ,.6.2 ,II,D 1193.6.3 ,.().6.4 ,.5%,0 ,.(.,.,).6.5:6.5.1 2,2,4-()(.)5 Reagent Chemicals,American Chemical Society Specifications,Am.Chemical Soc.,Washington,DC.,.Annual Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dors
8、et,U.K.,and the United States Pharmacopeia,and National Formulary,U.S.Pharmacopeial Convention,Inc.,(USPC),Rockville,MD.ASTM D 4045-15 7 6.5.1.1 ASTM6 .,.1 ,.6.6 1 19 (.6.2).().6.7-(3222)2S).,.6.8 ,.(.)7.7.1 ,.3 1300,.900,.,.7.2 ,6 Phillips Petroleum Co.,P.O.Drawer O.Borger,TX 79071.ASTM D 4045-15 8
9、 ,5%.,.(,.,.,.)200/.(.)1315 15.,.550 (.7.6).(,250-,.,.)7.3 .,.,.,15/,.7.4 H2S.7.5 .7.6 ,ASTM D 4045-15 9 550 .550 ,550 .,6/,200/.,.(500/15/;.)8.8.1 ,.-.8.2 ,-.,:)/(106aedcbz :(1)/(106zedcba(2):-,/,z,b-:32,06,-,d-,ASTM D 4045-15 10 -,z-,.:,0,5013 98%-,1000/.a=1000/b=32,06 c=146,29-(CH3CH2CH2CH2)2S d=
10、0,5013 e=0,98 z=10001098,05013,029,146/06,326107,66 107,66 .,/,.8.3 1000/,125-,100-20-.2,2,4-().(.).90 100-.0,5 -50.100.125-,z 100.,.ASTM D 4045-15 11 .1/.,.9.9.1 200/,.,5%.,Rb 11.1.,.9.2 .4 90%.Rstd 10.1.10.10.1 .Rs 11.1.10.2 .2 ,.10.3 1/,6/,/.1/.ASTM D 4045-15 12 ,.11.11.1 :S,/=Cstd (Rs Rb)/(Rstd
11、Rb)(3):Cstd-,/,Rb-(),Rs-,Rstd-.11.2 :S,=(/)/()=/(4).12./(QA/QC)12.1 (QC).12.1.1 QA/QC ,.12.1.2 ,1 QA/QC.12.2 ,-1 .ASTM D 4045-15 13 13.13.1 ,:13.1.1 ,(.1).=0,16X(5)-,/.1.,/(),/,/.0,02 0,10 0,50 1,00 2,50 10,00 0,02 0,05 0,11 0,16 0,25 0,50 0,04 0,08 0,18 0,26 0,41 0,82 13.1.2 ,(.1).=0,26X(6)ASTM D 4
12、045-15 14 2 (0,2 ),95%-.-ASTM.7 13.2 ,.14.16.1 ;()1.D02 1.1 (QC).1.2 ,QC(.D 6299 MNL78).1.3 QC ,(.D 6299 MNL78).,7 -ASTM International RR:D02-1405.8 ASTM MNL 7,Mannual of Presentation of Data Control Chart Analysis,6th ed.,Section 3:Control Charts of individuals,ASTM International,W.Conshohocken,PA.
13、ASTM D 4045-15 15,().,.1.4 ,QC ,.QC .QC ,.,QC .QC ASTM,.1.5,QC,.QC ,.1.6.D 6299 MNL78 QC .D02.03 (D 4045-04(2010),.(1 2015.)(1)3 4.ASTM D 4045-15 16 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.
