1、:D3401-97(2017.)STANDARD TEST METHODS FOR WATER IN HALOGENATED ORGANIC SOLVENTS AND THEIR ADMIXTURES 2019 ():16.07.2019:3718-19/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM
2、 International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,US
3、A.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM Internationa
4、l or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 3401-97(2017)1 :D3401-97(2017.)1 D3401;,.().1.1.1 (KF)2 1000.:1.1.1 A,KF-(10 H2O),1 ASTM D26 ,D26.04 .1 2017.2017.1975.2012.D3401-97(2012).DOI:10.1520/D3401-97R17.ASTM D 3401-97(2017
5、)2 50,.,.1.1.2 B,KF-.KF-,.1.2 (15 500),.1.3 KF-.1.4 ,.,.11 15.1.5 -,(TT).ASTM D 3401-97(2017)3 2.2.1 ASTM:2 E203 3.3.1 ,:H2O+I2+SO2+CH3OH+3RN (RNH)SO4CH3+2(RNH)I(1)RN .3.2 ,KF-,.,.3.3 ,.3.4 ,.2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 3401-97(2017)4 4.4.1 .4.1.1
6、,.4.1.2 .4.1.3 ,.5.5.1 ,.5.2 ,KF-,.5.3 ,KF-,203 .3,4 6.6.1 5(),.3 Mitchell J.,Smith D.M.,III ,2-.,J.Wiley and Sons,Inc.,-,NY,1977.4 ,4-.,Riedel-deHaen Aktiengesellschaft(Cresent Chemical Co.,Inc.).5 .ASTM D 3401-97(2017)5 6.2 5(B),.6.3,2,5,10 20.6.4,5.6.5 .6.6 ,.6.7.6.8 ,0,01.7.7.1 ,(),.7.2 ,(),.7.3
7、 (),.7.4 ,4(B),().1,00,2,00 5,00 H2O/.7.5 ,4(B),.1 ,ASTM D 3401-97(2017)6 .,.8.8.1 ,.8.2 ,.8.3 110 C .8.4 .,1 .8.5 KF-,.8.6 .ASTM D 3401-97(2017)7 A KF-9.9.1 ,.,.9.2 ,.,.9.3 ,.,.,.ASTM D 3401-97(2017)8 10.10.1 ,.,.10.2 3,0 5.3000 (3,0)H2O.10%;.10.3 ,.,.11.11.1 ,100 200 .11.2 ASTM D 3401-97(2017)9 .1
8、1.3 ,.11.4 KF-.,50%.,KF-,.11.5 ,.12.12.1 .12.2 ,/.,.12.3 ,.1 .12.4 ,.ASTM D 3401-97(2017)10 1.,1000 0,5 500 0,5 100 1,0 50 2,0 10 5,0 1 10 12.5 ,.12.6 .12.7 0,01.12.8 .,.,.12.9 .,.12.10 ,.,start titration()run()ASTM D 3401-97(2017)11 .12.11 (),.(%),.13.13.1 :H2O=H2O()/()(2)B KF-14.14.1 ,.(),.,.15.15
9、.1 ,ASTM D 3401-97(2017)12.15.2 KF-.,100%.,KF-.15.3 ,.,.15.4 .15.5 ,.16.16.1 ,.16.2 ,.16.3 5,3,0 ,.:3,0 H2O/=/H2O (3)16.4 ,ASTM D 3401-97(2017)13 .17.17.1 .17.2 ,.17.3 ,.17.4 .17.5 ,.2 .2 1 2 H2O/.2.,5 H2O/,2 H2O/,1 H2O/,1000 2,5 10 1 10 0,5 5 500 5 20 2 20 1 10 100 20 10 20 5 20 50.20 10 20 10.20 2
10、0 ASTM D 3401-97(2017)14 17.6 ,.17.7 ,.17.8 .17.9 0,01.17.10 .,.,.17.11 .,.17.12 ,.,start titration()run().17.13 (),.(%),.ASTM D 3401-97(2017)15 18.18.1 :H2O=H2O()/()(4)19.6 19.1 ():19.1.1 200 ,()2.1000 15.19.2 ():19.2.1 200 ,()3.1000 10.19.3 -.,.20.20.1 ;.6 -ASTM RR:D26-1004 RR:D26-1009.ASTM D 3401-97(2017)16 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.
