1、:D 3227-16:342/00 ,()STANDARD TEST METHOD FOR(THIOL MERCAPTAN)SULFUR IN GASOLINE,KEROSINE,AVIATION TURBINE,AND DISTILLATE FUELS(POTENTIOMETRIC METHOD)():3051-16/ASTM :15.12.2016 2016 (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM
2、International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and
3、does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly fo
4、rbidden according to the USA legislation and international copyright.-,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/ASTM D 3227-16 :D 3227-16 :342/00 ,()1 D 3227;,.().1.*1.1 ,0,0003%0,01%.,.0,0005%.,9.2,.1 ASTM D02 ,D02.03 .1 2016.2016.1973.2013.D3
5、227-13.DOI:10.1520/D3227-16.*1ASTM D 3227-16 1.2,.1.2.1 .1.3 ,.,.6,8,9 1.2.2.1 ASTM:2 D 1193 D 1250 D 1298 ,API D 4052 ,API()D 4057 D 4177 D 6299 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.2ASTM D 3227-16 3.3.1,/.,.4.4.1 ,.5.5.1 5.2 5.5;,5.3,9 ,11.1 ,14.5.2 ,9 10-12 2 1
6、.,.3 5.3,.3 .3ASTM D 3227-16 ,.2 (0,08),.5.4,10,0,05 ,120 (5).5.5 ,.6.6.1 .,(ACS),.4 ,.6.1.1 ,.6.1.2 ,.4“Reagent Chemicals,American Chemical Society Specifications”,Am.Chemical Soc.,Washington,DC.,.”Analar Standards for Laboratory U.K.,Chemicals,”BDH Ltd.,Poole,Dorcet,and the United States Pharmacop
7、eia,and National Formulary,U.S.Pharmacopeial Convention,Inc.,(USPC),Rockville,MD.4ASTM D 3227-16 6.2 ,I,D 1193.6.3 ,(150/)150 (3CdSO48H2O).(.().)10 H2SO4(.)1.6.4 ,(0,1/)17 KI(0,01)100 1-1.6.5-2-(.,-2-.-2-.,).6.6 ,(0,1/)17 AgNO3 100 1-1 -2-(99%)(.1).,0,0005 .1 -2-,;,.,.6.6.1 6 HNO3(.1,42)(.)100 5ASTM
8、 D 3227-16(,200-,250-300-).5.5 0,1/KI AgNO3,.6.7 ,(0,010/)0,1 .100 0,1/1-2-.6.8 (10/)10 Na2S 1.2 ,.(Na2S9H2O)30,6/.6.9 ,.5 1 (.1,84).(:.,.),10 .6.10 ,.,.6ASTM D 3227-16 6.10.1 2,7 -(NaC2H3O23H2O)1,6 (NaC2H3O2)25 ,975 -2-(99%)(.1).,10 ;.,.6.10.2 2,7 NaC2H3O23H2O 1,6 NaC2H3O2 20 ,975 -2-(99%)(.1)4,6 .
9、,10 ;.,.6.11 ,6 20.7.7.1 D 4057 D 4177.7.2 ()6,2,.,()7ASTM D 3227-16,4,.7.3 (100/),85C,.3 0,010%,120.,.0,01%.8.8.1 .()(.,)(10).,.8.2 /(QC)(.12),:8.2.1 ,.8ASTM D 3227-16 8.2.2 100 ,8 Na2S.8.2.3 (,)10 0,1/AgNO3 10 15.8.2.4 ,.8.2.5 5 100 ,0,5 0,1/AgNO3.9.9.1 ,D 1298 D 4052 ,(D 1250).9.2 (H2S)5 5 CdSO4.
10、,9.3.,H2S :(3-4 ,),CdSO4 .,.CdSO4.25-30 ,.9ASTM D 3227-16 ,CdSO4,.,9.3.,CdSO4,H2S .(,H2S .,.,H2S().9.2.1 /(QA/QC),.,X1.9.2.2 ,H2S ,H2S .,.,.9.2.3 9.2.9.3 ()20 50 10ASTM D 3227-16 (,200,250 300 ),100 .,9.3.1 9.3.3.,.0,01/AgNO3 ,25 (1).9.3.1 .-250 -350.0,01/-AgNO3 .,6/.4 ,.5 20 50 .,20-50 .20 .11ASTM
11、D 3227-16 6 .9.3.2 AgNO3,0,5 .6/0,1,0,05 0,01/AgNO3.5 10.,.,.9.3.3 ,0,01 0,01 AgNO3 .,6/.,.,.(),8.1 8.2.5.9.4 ,()9.3 9.3.3 .10.10.1 :12ASTM D 3227-16 ,%=(DM(A1 A0)3,206/W(1),%=(DM(A1 A0)3,206)/(d V)(2)D=(W+I)/W(3)D=(V+J)/V(4):1-AgNO3,+300 (.1),0-AgNO3,+300 (.1),.(,.)d-,/,D-(.5),I-,J-,-AgNO3,W-,3,206
12、-100 .S ,V-.11.11.1 0,01 AgNO3 .,.1.,.13ASTM D 3227-16 11.1.1 ,.1,-250,6/,/.1 11.1.2 ,(Ag2S).11.1.3 ,Ag2S 550 350,14ASTM D 3227-16 +300.1.Ag2S ,.11.1.4 ,Ag2S (+300),.11.1.5 ,()(),4,9.2 9.4.12./(QA/QC)12.1 (QC).12.1.1 QA/QC ,.12.1.2 QA/QC ,2 QA/QC.12.2 ,-2 .13.13.1 0,0001%()1/.15ASTM D 3227-16 14.14.
13、1 ,:.2 ,14.1.1 ,:0,00007+0,027(.7):16ASTM D 3227-16 -%.7 .2.14.1.2 ,:0,00031+0,042(.7):-%.14.2 .15.15.1;.()1.1.1 1.1.1 (.().)(.).17ASTM D 3227-16 1.1.2 ,(.,),.1.1.3 ,QA/QC,.1.2 1.2.1 .1.2.2 ,.1.3 1.3.1 6.1 .1.3.2 ,6.1 .1.3.3 ,5%()(CH3COO)2Pb3H2O .1.3.4 ,18ASTM D 3227-16.(,.)1.3.5 ,50 1 (NaHCO3),1 .1
14、.3.6 ,.(,).1.4,1.4.1 .,.1.4.2 ,:1.4.2.1 ,3-4 .1.4.2.2 ,.(,.)1.4.2.3 .1.4.2.4 ,.1.4.2.5 ,.19ASTM D 3227-16(,.(),.)1.4.2.6 ,().2.D02 2.1 QC.2.2 ,QC(.D 6299 MNL75).2.3 QC (.D 6299 MNL75).().,.2.4 ,QC ,.QC ,5 ASTM MNL7,Manual of Presentation of Data Control Chart Analysis,6th ed.,Section 3:Control Chart
15、 for Individuals,ASTM International,W.Conshohocken,PA.20ASTM D 3227-16 .QC ,.,QC .QC ASTM,.2.5,QC,.QC ,.2.6.D 6299 MNL75 QC .D02.03 (D 3227-13),.(1 2016.)(1)8.2.3.21ASTM D 3227-16 22ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.
