1、:D 3606-101 STANDARD TEST METHOD FOR DETERMINATION OF BENZENE AND TOLUENE IN FINISHED MOTOR AND AVIATION GASOLINE BY GAS CHROMATOGRAPHY ():3061-16/ASTM :29.12.2016 2016 (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International
2、,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confi
3、rm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden accord
4、ing to the USA legislation and international copyright.-,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/ASTM D 3606-101 :D 3606-101 1 D 3606;,.().1 1.3 .7 2016.1.*1.1 .1.2 0,1 5%,2 20%.1.3 ,1 ASTM D02 ,D02.04.0L .1 2010.2010.1977.2007.D3606-07.DOI:10
5、.1520/D3606-1001.*1ASTM D 3606-101 (-,-,-).1.4 .X1 ,.1.5,.1.6 ,.,.2.2.1 ASTM:2 D 4057 E 694 E 969 E 1044 E 1293 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.2ASTM D 3606-101 3.3.1 (),.,(8.1.1),.,1,2,3-(2-)-(8.1.2),.,.4.4.1 ,.5.5.1 ,.1.:.1 ,.2 .3ASTM D 3606-101 5.2:5.2.1 A
6、 ,0,8 (2,5)3,2 (1/8)10%-(,OV-101)Chromosorb W,60 80.5.2.2 ,4,6 (15)3,2 20%-Chromosorb P,80 100.5.3 .,0,1%/.,0 1,2 0,3%.4 2 ,0,1%.5.4 5.5.5 ,A 0,5,1,5,10,15,20 (.E 694 E 969).5.6 1 2,0,01;5 0,1 ,(.E 1044 E 1293)(.11.1).1 5.5 5.6 -,4ASTM D 3606-101 .5.7 ,25 100.5.8 .5.9-.5.10 ,.5.11 ,24/40 ,500.(5.10)
7、.5.12 .5.13 ,25.1.:(),(A)0,8;()4,6 ,3,2 (A),10%(),20%(A)Chromosorb W,60-80 ()Chromosorb,80-100 .:,C 200,C 200,C 145-:,/6 ,3/30 ,200(30),0 1 ,/1 ,2 ,8 ,0,75A .5ASTM D 3606-101 6.6.1-,99,99%.(.)6.2 ,60 80 80 100.6.3 1,2,3-(2-)().3 6.4:6.4.1 .(.).6.4.2 .(.).6.4.3 .(.).6.4.4 .(.).6.5 :6.5.1 (),99,5%.(.)
8、.6.6 :6.6.1 99+.%.(.).3 OV 101 .6ASTM D 3606-101 6.6.2 (2,2,4-)99+.%.(.).6.6.3 (.).6.6.4-99+.%.(.).7.7.1 (.).,D 4057.8.8.1 (,10%Chromosorb W;20%Chromosorb P):8.1.1 45 Chromosorb W 60 80 500 (5.11).5 50 .(.).-,Chromosorb W.(5.10)-.7ASTM D 3606-101 A.1.2.1.8ASTM D 3606-101.AB6CarleInstrumentsCo.8034(F
9、ullerton,Ca).1.2.2.9ASTM D 3606-101 8.1.2 1,2,3-(2-)()80 Chromosorb P 80 100 500 (5.11).20 200 ,Chromosorb P.(5.10)-.(180).9.9.1 :.50 (.).50 .(.).9.2 A B .0,8 (A)(8.1.1)4,6 (B)(8.1.2),:10ASTM D 3606-101 -,.-.-.6 (1/4).10.10.1 A B(5.1).1 2.,.40 3/.,C ,1/2 50 1/2 100 150 1 170 3 10.2 B .1,.10.3 :10.3.
10、1 (.1):10.3.1.1 A B C;,(.1)205 11ASTM D 3606-101(30 .).GC .10.3.1.2 A B C.GA .,.10.3.1.3 B.,GC 3,5 7 (0,5 1 .)10.3.1.1.10.3.1.4 B ,GA 14 28 (2 4 .).10.3.1.5 A C (.1 B1).10.3.1.6 A B.(.)(.1).10.3.2 (.2):10.3.2.1 (.2 B1)A (.1).10.3.2.2 (.2 B2),.,.(1 3/).10.3.2.3 .12ASTM D 3606-101 ,.,.().10.4 .5%-.,11
11、.4,(10.3),1 .-.,-.-.30-60.,-.,-.,.11.11.1 0 5%0 20%13ASTM D 3606-101 :100,(2,2,4-),.%,%,5 5,0 20 20,0 2,5 2,5 15 15,0 1,25 1,25 10 10,0 0,67 0,67 5 5,0 0,33 0,33 2,5 2,50 0,12 0,12 1 1,0 0,06 0,06 0,5 0,50 11.2 1,0 25 (11.1).2 ,().11.3 10.4,:11.4 :11.4.1 .,11.4.2,.11.4.2 5 ,3 .(!),2,0,14ASTM D 3606-
12、101 ,1 2 .,.11.5 ,12.4.3.,.,.3 ,11.5.4 ,.,15,.12.12.1 1,0 25.12.2 ,10.4,11.4.15ASTM D 3606-101 ,10.4 ,B.,%.3.()12.3 ,.5 :,.4 .,%/5,0 7508 6258 1,200 2,5 3874 6457 0,600 1.25 1991 6401 0,311 0,67 1052 6537 0,161 0,33 516 6532 0,079 0,12 183 6324 0,029 0,06 93 6166 0,015 16ASTM D 3606-101 1.2.3.(.);4.
13、().4.12.4 .6 15 ,-.13.13.1 .,.13.2%,:(1),%=(V/D)0,8844:V-%,D-15,6/15,6C(60/60F).17ASTM D 3606-101(2),%=(V/D)0,8719:VT-%,D-15,6/15,6C(60/60F).14.14.1 0,01%.15.15.1 (95%-):,.15.1.1 ,.2,20:15.1.2 ,.3,20:7 1994.,(-,-18ASTM D 3606-101 ,-,).0,1 1,5%1,7 9%.-ASTM International.4 2.1 X=%.%.0,1-1,5 0,03(X)+0,
14、01.7 1,5 0,03.8 1,7-9 0.03(X)+0,02.7 9 0,62.8 3.1 X=%.%.:0,1-1,5 0,13(X)+0,05.7 1,5 0,28(X).8 1,7-9 0,12(X)+0,07.7 9 1,15.8 8 ,.1,5%9%.-ASTM International.4 15.2 -,.4 -ASTM International RR:D02-1042.19ASTM D 3606-101 16.16.1 ;.X1.X1.1 X1.1.1 D3606 ,.,EPA Q&A.X1.2 X1.2.1 ,:X1.2.1.1 1 5 1/8,Chromosorb
15、(10%OV 101 Chromosorb PAW 80/100).X1.2.1.2(-).X1.2.1.3 2 5 1/8,Chromosorb(20%Chromosorb PAW 80/100).X1.2.1.4 3 15 1/8,Carbowax 1540(15%)Chromosorb W 60/80).X1.2.1.5(-).X1.2.2 5.15 20ASTM D 3606-101 20,20 .20-,15,(Carbowax ).,.1.1.X1.2.3 2-()2-(SBA).X1.2.4 :135C 65 .26,6 3/X1.2.5 ,.X1.2.X1.2.6 ,0,02%
16、.X1.3 B X1.3.1 ,21ASTM D 3606-101 5.(R)3,00 X1.3.3 .5 .-(N2)(.X1.3).23.X1.1.,5 2,Restek,Inc.,110 Benner Circle,Bellefonte,PA 16823.,-ASTM International.,/11OV1012TCEP3CarboWax 22ASTM D 3606-101 .X1.2.X1.3.2 (.X1.4):X1.3.2.1 1 6,2 1/8 (10%Rtx 1 100/120 Silcoport)-.10%,(.).X1.3.X1.3.2.2 .X1.3.2.3 2 15,5 (4,76),23ASTM D 3606-101 2 1/8 (BenzoSep).5 X1.3.2.4 .X1.1 1 MXT(Restek)(),PDMS-,.,.(S)10%-1 2,8 ,(.X1.3),.,10%,10%-.A,B,.S=B/A.X1.3.3 21 (6,57).X1.5.X1.3.4 2-()2-(SBA).X1.3.5 :135C 65/.20 3/X1.3.6