1、 D197716 ()/-STANDARD TEST METHOD FOR NICKEL AND VANADIUM IN FCC EQUILIBRIUM CATALYSTS BY HYDROFLUORIC/SULFURIC ACID DECOMPOSITION AND ATOMIC SPECTROSCOPIC ANALYSIS 2017 ():05.10.2017:3288-17/ASTM -,.9,-49,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM I
2、nternational)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(
3、ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of
4、the specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D1977-16 1 D197716 ()/-1 D1977;,.()1.1.1 ,50 25/,.1.2,.1.3 ,.1 ASTM D32 D32.03 .1 2016.2016.1991.2008.D1977-03(2008)
5、.DOI:10.1520/D1977-16.ASTM D1977-16 2 ,.2.2.1 ASTM:2 D1193 D3766,E105 E177 ASTM E288 E456,E691 2.2 :3 NNN-P-395C A 3.3.1 .D3766.4.4.1 ()2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 DLA(DLA Document Services):Building 4/D,700 Robbins Ave.,Philadelphia,PA 19111-5094,http:
6、/quicksearch.dla.mil.ASTM D1977-16 3 .,-,-.5.5.1 .6.6.1 .Al2O3(7800 (ppm),.6.2 ,;,.7.7.1 ,0,1.ASTM D1977-16 4 7.2 ,250 10C.7.3 ,250 .7.4 ,50,100,250,500 1000,E288.7.5 ,5,10 25,NNN-P-395C.7.6 ,100 1000.8.8.1 .,.4 ,.8.2 ,IV ,D1193.8.3 :8.3.1 (HF),48%.8.3.2 ,(H2SO4),98%.8.3.3 ,49%,4 ,DC.,.,BDH Ltd.,Inc
7、.(USPC),.ASTM D1977-16 5,H2SO4(98%),.8.3.4 ,38%.8.3.5 ,19%,HCl(38%),.8.3.6 (HNO3),70%.8.3.7 1000/(.1).1 ,0,1%.8.3.8 1000/(.1).8.3.9 ,AlCl36H2O 8.3.10 39000/Al2O3,184,5 AlCl36H2O ,1 .8.3.11 3-%.9.9.1 .,.,E105.10.10.1 ,0;5,0;ASTM D1977-16 6 20,0 50,0/Ni 7800/Al2O3 10-%,0,5,0,20,0 50,0 1000/1000-,200 A
8、l2O3 39000/100 .10.2 ,0;10,0;25,0;50,0 100,0/V 7800/Al2O3 10-%,0,10,0,25,0,50,0 100,0 1000/1000-,200 Al2O3 39000/100 .11.11.1 ,2,0,0,1 250-.11.2 10 48-%,10 10 .11.3 (250C ).11.4 .11.5 20 19-%30 3-%,.11.6 ,.ASTM D1977-16 7 11.7 ,.11.8 ,100-().11.9 (),-()-().,.,12.12.1 :/=SDC(1):-,/,D-,;.11.8,D=100.,D
9、=100 x V2/V1,V1 11.8 V2 ,S-.ASTM D1977-16 8 13.13.1 ,.E691,.13.2 ,2,772 S,2,772 S 95%,S .E456 E177,.Ni()95%()95%()208/8/(3,9%)14/(6,7%)152/5/(3,3%)24/(15,8%)437/9/(2,1%)31/(7,1%)V()95%()95%()1191/43/(3,6%)201/(16,9%)1898/72/(3,8%)303/(16,0%)3346/82/(2,4%)531/(15,9%)13.3 ,.14.14.1 ;.ASTM D1977-16 9 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.
