1、:D 1364-02(2012.)()STANDARD TEST METHOD FOR WATER IN VOLATILE SOLVENTS(KARL FISCHER REAGENT TITRATION METHOD)2012.():1813-12/ASTM :12.11.2012 -,.9,-49,-1,119991.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ruhttp:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA
2、 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohoc
3、ken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for AS
4、TM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 1364-02(2012)1:D 1364-02(2012.)()1 D 1364;,.(),.1.*1.1 ,.1.2 ,.1.3 ,1 ASTM D01 ,D01.35 ,.1 2012.2012.1955.2007.D 1364-02(2007).DOI:10.1520/D1364-02R12.ASTM D 1364-02(2
5、012)2 ,E 29.1.4,.1.5 ,.,.1.6 .2.2.1 ASTM:2D 1500 ASTM(ASTM)E 29 3.3.1 :3.1.1 ,.2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 1364-02(2012)3,20-50,0,05 (6 H20 1),10 20,30.1 ,.3.1.2 ,.,;-.-30,.2 ,D 1500.4.4.1 .,:H2O+I2+SO2+3C5H5N 2C5H5N HI+C5H5N SO3(1)C5H5N SO3+ROH C5
6、H5NHSO4R 4.2 (,1+10+3),2-,-(1+4),.ASTM D 1364-02(2012)4-,.5.5.1 ,.6.6.1 100 250-,;250-,(.1)3,.300 ;,.6.2 26 5.3 8 ,25 3 ,Rankin Glass Blowing Co.,3920 Franklin Canyon Road,Martinez,CA.,ASTM.,1 .ASTM D 1364-02(2012)5 .1 .1 6.3 ,5000 20 50 10 20 .4 6.4 ,25 50-,();5 .-,4 ,Fisher Scientific Co.().,ASTM.
7、,1 .5 ,No.J-821 ,Scientific glass Apparatus Co.,Bloomfield NJ.,ASTM.,1 .250-.3-4 ASTM D 1364-02(2012)6 ,.,.6.5 ,.7.7.1 .,.6 ,.7.1.1 (6 H2O 1)7 133 1 I2 425 2 (0,1%H2O).425 2 (0,1%H2O)2-.-4C SO2,H2SO4(1,84);SO2 SO2(102 1)(70 1).,70 (SO2).6 -,.,Analar Standards for Laboratory Chemicals,BDH Ltd.,Poole,
8、Dorset,U.K.United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.7 .,.,ASTM.,1 .ASTM D 1364-02(2012)7 7.1.2 1 (0,1%H2O)4 (0,1%H2O).3 ,2-,0,1%,.4 ,5%95%.1 19 -,5%,95%.8.8.1 ,.-,.,.,.9.9.1 (3),.9.1.1 25 -10.,ASTM D 1364-02(2012)8 ,0,15-0,18 ,0,1.10.9.1.
9、2 W :W=A/V (2):W-,A-,V-,.10.10.1 10 25 (-,1+4),.,.10.2 ,.(.3.1)(.3.2).,-.10.3 .1.,.ASTM D 1364-02(2012)9 .,.5 (a),.(b).6 ,.7 ,.,.-.1 ,%2,5-10,0,15-0,18 H2O 0,5-2,5 10 0,5 25 11.11.1 :,%=(V W)/(10 S)(3):V-,W-,ASTM D 1364-02(2012)10 S-,.8 ,S=,.12.12.1 0,5%0,001%.,0,008%,(95%).13.13.1 0,100-0,500%,0,11
10、8 0,406%,-,0,050 0,176%,0,5%,95%,:9 ASTM.13.1.1 ,0,015%.13.1.2 ,0,027%.ASTM D 1364-02(2012)11 13.2 0,010-0,100%8 ,0,015,0,034,0,052,0,071,0,098%.,.,.13.2.1 ,0,030%,x .13.2.2 ,0,060 x%,x .13.3 ,.,.,8.1 .5,6 7.14.14.1 ;8 -ASTM International RR:D01-1049.ASTM D 1364-02(2012)12 D01.35 (D 1364-95(1999),.(1)E 29 1.3 .(2)E 29 .ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).ASTM(www.astm.org/COPYRIGHT/).
