1、 D708504(2010)1 -()STANDARD GUIDE FOR DETERMINATION OF CHEMICAL ELEMENTS IN FLUID CATALYTIC CRACKING CATALYSTS BY X-RAY FLUORESCENCE SPECTROMETRY(XRF)2017 ():13.12.2017:3335-17/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr
2、 Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)
3、100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified trans
4、lations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D7085-04(2010)1 1 D708504(2010)1 -()1 D7085;,.()1 2010.,.1.1.1 (29)-()().1.2 ,1 ASTM D32 D32.03 .1 2010.2010.2004.2004.D7085-041.DOI:10
5、.1520/D7085-04R10E01.ASTM D7085-04(2010)1 2 -.1.3 .1.3.1 X2.3 X2.5 (ppm/).,.1.4 ,.,.2.2.1 ASTM:2 C982 ()(2008.)3 C1118 ()(2011.)3 D1977 -()/-E1172 E1361 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 www.astm.org.ASTM D7085-04(2010)1 3 E1621 E1622 (2006.)3 3.3.1 .:(,8-15)
6、(B,16-23).,.,.,(,).,.,ASTM D7085-04(2010)1 4 ,.,.4.4.1 .().4.2 .5.5.1 ,.-C982,C1118 E1172.5.2 ,600C.5.3 ,200C.5.4 ,50-.5.5 ,60C.,.ASTM D7085-04(2010)1 5 5.6 ,.5.7 :5.7.1 ,1100C.5.7.2 -,5%,.5.8 :5.8.1 ,(,)(,).5.8.2-,.5.8.3 ,-.5.8.4 ,25000 .,.-.-25 40.6.6.1 :6.1.1,.6.1.2 ,ASTM D7085-04(2010)1 6 ,.,.6.
7、2 :6.2.1 ,.6.2.2 ,.-.6.3-,.P-10:10%90%.6.4 2-,ACS().6.5 ,.6.6 ,10000/10000/.7.7.1 ,.7.2 ,.ASTM D7085-04(2010)1 7 7.2.1 ,.100 29,.7.2.2 ,.7.3 ,X1,29 .A 8.8.1 ,.8.2 .9.9.1 ,.,-,.ASTM D7085-04(2010)1 8 10.10.1 .10.2 .10.3.10.4 .11.11.1 .0,1%.,().11.2 E1621,E1361 E1622.11.3 ,.,.()X1.ASTM D7085-04(2010)1
8、 9 1.%-12.12.1 :12.1.1 ,.,.12.1.2 13,.12.1.3 ,.12.1.2,D1977.,%2 (.95%)%ASTM D7085-04(2010)1 10 12.2 ,.13.13.1 50 600C 25 1,3,.13.2 20-30 30.,.13.3 ,.,:1 3-5 ,.1 ,1,5 (0,01)6,5 (0,01).13.4 10,.13.5 .13.6 ,2-,-,.ASTM D7085-04(2010)1 11 13.7 25000-60000 ./.,30000 .10 (2)40-.13.8 .,.13.9 .14.14.1 ,.12.2
9、.15.15.1 1 ,16.(),%,:%=(/)100 16.16.1 c ASTM D7085-04(2010)1 12 ,.17.17.1 ,.,-,.18.18.1 .18.2 .18.3.18.4 .19.19.1 .0,1%.,.19.2 E1621,E1361 E1622.19.3 ,.ASTM D7085-04(2010)1 13 ,.()X1.20.20.1 ,.,.,.20.2 :20.2.1 50 600C 25 2.20.2.2 1000 10000/1000 10000/.2 ,NIST(),-.20.2.3 1,00 0,01 5,00 0,01 ;.3 Pt/5
10、%.,5:2 10:1.:49,75%,49,75%ASTM D7085-04(2010)1 14 0,50%.20.2.4 .20.2.3.20.2.5 ,.,0,05%Ni .20.2.6 .20.2.7 ,1000/,0,500 .20.2.8 250C 30.().20.2.9 .500 ,1,00 .0,05%.20.2.10 ,0,500 10000/.5000 1,00 ,0,5%.20.2.11 .,.20.2.12 1100 100C 8-10,.4 .20.2.13 ,ASTM D7085-04(2010)1 15 ,-.20.2.14 ,-,.20.3 ,.,.20.3.
11、1 ,1,0%.,.20.3.2 .2,5 .20.3.3 0,06363 (78,584%).,.20.3.4 2,5 .,.20.3.5 1100 100C 8-10,.20.3.6 .20.3.7 ,5.20.3.8 :=25,0600 =20,0000 =0,06363 ASTM D7085-04(2010)1 16%=100 (0,06363 0,78584)/(25,0600 20,0000)=5,0003/5,0600 =0,9882%Ni 20.3.9 .,.20.4 .20.2.3-20.2.14.,.20.2.2,.20.3.9.,.20.3.9.,.20.3.9,.20.
12、5 ,.,.20.3.9,.20.6 ,.21.21.1 3-8 600C 1,3,.21.2 .:1 3 ,1 10 ,.,ASTM D7085-04(2010)1 17 -.21.3 ,.21.4 -.21.5 1100 100C(1250C).,.21.6 -.-,25 40.2,.,.,.5 .2.,%2 (.95%)%ASTM D7085-04(2010)1 18 22.22.1 ,.20.6.23.23.1 2 ,11.,15.(),%,:%=(/)100 24.24.1;-();().ASTM D7085-04(2010)1 19 ()X1.X1.1 X1.1.1 60 66 4
13、-.X1.1.2 .X1.1.3 .X1.1.4 ,-.X1.1.5 K-.X1.1.6 LiF200.X1.1.7 48,6450.X1.1.8 300.X1.1.9 20.X1.2 X1.2.1 47 85 4-.X1.2.2 .X1.2.3 .X1.2.4 ,-.X1.2.5 K-.X1.2.6 LiF200.X1.2.7 76,9636.X1.2.8 78,1040.X1.2.9 300.X1.2.10 20.ASTM D7085-04(2010)1 20 X2.X2.1 X2.1 X2.5 ,.X2.1.():7 ():0 :():30:5:Rh:1 ASTM D7085-04(20
14、10)1 21 X2.2 1 2 PHS1 UL PHS1 UL Al KA PE002 150 32 125 144,9250 22 78 Ba LA LiF200 300 37 108 87,1818 1,3322 29 71 Bi LA LiF200 300 60 66 32,9700-1,6000 1,6000 19 78 Ca KA LiF200 300 32 125 113,1304-0,9158 28 71 Ce LA LiF200 300 47 85 79,0450 30 70 Co KA LiF200 300 60 66 52,7922-0,5000 0,6000 19 67
15、 Cu KA LiF200 300 60 66 45,0020 0,7606 20 70 Fe KA LiF200 150 57 70 57,5136 15 70 KA LiF200 300 32 125 136,6930-1,3512 27 74 La LA LiF200 300 42 95 82,9362 30 70 Mg KA PX1 700 32 125 22,2722-0,8000 0,8910 23 85 Mn KA LiF200 300 57 70 62,9750-0,9390 15 72 Mo KA LiF200 150 60 66 20,2866-0,5000 0,5000
16、25 75 Na KA PX1 700 32 125 26,9218-2,1684 1,9352 21 78 Nd LB1 LiF200 300 57 70 65,1298 0,6124 15 70 Ni KA LiF200 300 60 66 48,6450 19 69 P KA Ge111 300 32 125 140,9576-1,2698 2,6310 22 78 Pb LA LiF200 300 60 66 33,9024 0,7630 18 72 Pr LB1 LiF200 300 57 70 105,0006 0,8612 12 69 S KA Ge111 300 32 125 110,6618 1,9098 11 78 Sb1 KA LiF200 300 60 66 13,4078-0,5000 29 75 Si KA PE002 150 32 125 109,1046 24 78 Sm LB1 LiF200 300 57 70 59,5042 0,5296 15 76 Sn1 LA LiF200 300 32 125 126,8242-1,5000 29 70 Sr
