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ASTM_D_6349_-_13_rus.pdf

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1、 542372022 -542372022II1 ()2 1793-52022.741-4 634913-,-(ASTMD634913Standardtestmethodfordeterminationofmajorandminorelementsincoal,cokeandsolidresiduesfromcombustionofcoalandcokebyinductivelycoupledplasmaatomicemissionspectrometry,NEQ)5 542372010 26 29 2015.162-.-(1 ),.().,-(www.rst.gov.ru).,2022,-5

2、42372022III1.12 .13.34.35 .36,.47 .58.79.810.1011.1212.1313.13.151 202301011 ,(,)-.11,-,.-,59592.,55661,-.2 :1770(104283,478880).,.6563.9147.9656.10157.10929.11125.11303.11304.11305.11306.14261.17070.542372022 -Solidmineralfuel.Determinationofchemicalcompositionofashbymethodofatomicemissionspectrome

3、trywithinductivelycoupledplasma 542372022219908,-.23083,.25336.,27313.-27589(ISO687:2010).29169(64877).29227(835-181).1.33503(ISO11722:2013,ISO5068-2:2007).-336542022,.33756.33814.ISO13909-2.2.ISO13909-3.3.OIMLR76-1.-.1.51568(3310-190).-52501(3696:1987).54332.55661(1171:2010).59248,.-59252,.59253,.-

4、59254.59257,.59592.5725-62002()-.6.13909-5.5.13909-6.6.18283.,1 ,.,.,().,.,.54237202233 17070.4 (81510),.,.,-(ICP-AES).1-,.1ICP-AES,212,412;288,16;251,611396,152;256,80;308,215;309,271259,940;271,44;238,204317,93;315,887;364,44;422,67279,553;279,08;285,21;277,983337,280;350,50;334,941178,287;214,900

5、766,491;769,896588,995;589,592182,04257,610;294,92;293,31;293,93455,403;493,41;233,53421,555 5.1 2-52501.5.2(HCI)14261.5.3(HF)1.5.4(HNO3)11125.5.5(H3BO3)9656.5.6(H2O2)10929,30%.5.7,10157.5.8(Li2B4O7)2,.5.9 2-()(LiBO22H2O)3.5423720224 (5.8)(5.8)(5.9)1:4.5.10(LiI)4.5.11()-,(7.2.5).1-,.,ICP-AES.2,99,99

6、9%.3,-,-.(,),.5.12()(,),-,.-.-.110/3.-.,-,-.,99,999%,.5.13.-,(-1),7460-98.1-,.2 5.6 ,6.1 IOIML R 76-10,0001.6.2 ,350,100130.6.3 1250,(815 10)10001200.6.4-.6.5,(6.6),100130.6.6,2503.,1003.5423720225,.6.7-19908,91476563.6.8 901003 6563.,.6.9 6.10().6.11 212,2007551568.6.12 1()1770-.6.13,1770.6.14 2-29

7、169.6.15 2-29227.6.16,1()25336.6.17 25336.6.18 33756,.6.19.,5.,.7 7.1 ,-,235.1.(6.7)(6.3)80023,57(6.17).(6.8)(6.7),(5.1)900950.7.2 5.1.7.2.1 5%-10003(6.16)3004003-(6.12)503(5.4).-10003.(6.18).7.2.2 (5.8,5.9)(4,000,05),0,0001,(6.16)10003,-5423720226(6.10).5003(7.2.1),(6.9).,.30.(6.13)10003,.(6.18).7.

8、2.3 1,5%-10003(6.16)15(5.5)5003,.10003.(6.18).7.2.4 7:3 (5.2)(5.3).(6.18).7.2.5 -(5.11).V,3,C VCV,=(1),/3;V,3;,/3.(6.14,6.15)(6.13)1003.10153,23(5.4)V,3,(1).(6.18).7.2.6 1 400/3,100,-(7.2.5).Vo,3,C VCV,=(2),/3;V ,3;,/3.1003(6.13)10153(7.2.2)(6.14,6.15)(7.2.5),(2).5423720227(5.12),(.7.3),.100310153(7

9、.2.3),(2).(5.12),53HCIHF(7.2.4)23(5.4).(7.2.3).-.,-.7.2.7 ,.,1003,(7.2.2),(5.12).100310153(7.2.3),(5.12),53 HCIHF(7.2.4)23(5.4).-(7.2.3).7.3 -(6.4).,(5.12).8 11303,11304,23083,33814,ISO 13909-2,ISO 13909-3,54332,59248,59252,59253,59254,59257,13909-5,13909-6,182836.212.,200.,.-,-,-.1,.11305,275893350

10、31130655661.5423720228-,(6.2)105110.-.-/,.9 9.1 ,:-;-,.,.-,-.-.(5.13)-.13.2.9.2 7.1/(6.7)-,/./-.(6.1)0,0001.-0,1.-./(6.3),2(81510)/2./,(6.17)./0,0001,1-(81510),/,.-/,0,001,.18.,.5566111306.(6.19)75(6.11).9.3 (0,1000,001),9.2,0,0001(6.8).(0,4000,005)(5.8,5.9).0,1(5.10).5423720229(6.3)10001200.7-.(6.1

11、0)503 (7.2.1).(6.9).,30.-.-,.,.1003(6.13),-(5.1).(5.12).9.4 (0,1000,001),9.1,(6.6)-(6.1)0,0001.,.(6.12),53HCIHF(7.2.4)2 3(5.4),.100130(6.5)(6.2),2.,13 H2O2(5.6).,.,(5.12)1003(7.2.3).,100 130,1.9.5 9.39.4,.9.6 9.6.1 ,(7.2.7)(7.2.6),.-2,:-;54237202210-,-;-,.2 ,/3,/3102030151,518023040020020 :(/3)-(5.1

12、2).,.,.9.6.2 -1520(9.3,9.4)(9.5).-.,-5%.-,.,.,-,.9.7 ICP-.,9.3,9.49.5,.,D,.6.13 6.146.15.,13.100.10 10.1 ,%,54237202211()AC CV D m610100,-=.(3),/3;.,/3;V ,3;D ;m ,.10.2-,%,AA aa,100=(4)-,9.2,%,mmmmA a3121,100-=(5)m3/,;m1/,;m2/,.,3.3,2SiSiO0,4674=2NaNa O0,7419=23AlAl O0,5293=2KK O0,8301=23FeFe O0,699

13、4=2MnMnO0,6319=CaCaO0,7147=3SSO0,4005=MgMgO0,6032=BaBaO0,8956=2TiTiO0,5995=SrSrO0,8456=25PP O0,4365=54237202212,-,27313.,r,-.5725-62002(5.2).11 .11.1 ,r,4.11.2 ,R,4.4=95%r RSiO22,04%73,73%0,13+0,09x2,00+0,10yAl2O31,04%29,54%0,17+0,06x0,86+0,07yFe2O30,39%47,94%0,13x0,23yMgO0,40%7,29%0,02+0,08x0,11+0,

14、11yCaO1,04%44,03%0,11x0,25yTiO20,06%1,47%0,02+0,07x0,05+0,12yK2O0,09%2,53%0,06+0,11x0,14+0,30yP2O50,10%1,34%0,01+0,18x0,11+0,31yNa2O0,17%7,44%0,06+0,09x0,10+0,17yMnO2198 834/0,16x0,42yBaO266 950/0,07x190yBaO0,13%3,00%0,17x0,30ySrO285 10460/33+0,076x73+0,164ySO30,14%10,0%0,03+0,060,08+0,06 1 x,y,.2 S

15、O3,-,.5423720221312 :);),;););,;),;),-,;),;),-;);),;)(),().13 13.1 :-13.2;-13.3.13.2 -(5.13).,-.,-9,-10.CCDo0,5,9-(6)r R CD220,95,2-=(7),%/;(),%/;D0,95=0,95,%/;R r ,4,%/.,.().5423720221413.3 ,.-7,5725-6336542022().336542022().-.5423720221512612-028-69886968-20142726-09-04-253-86()36-09-4756-792-()46-09-3551-79,1-,-512.13.1-03.-()6.14-2008.7762014 .54237202216.08.08.2022.23.08.2022.6084.2,12.-.2,32.,117418,-,.31,.2.www.gostinfo.ru infogostinfo.ru662.6:543.812:006.35475.160.10:,-

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