1、:D5865/D5865M-19 STANDARD TEST METHOD FOR GROSS CALORIFIC VALUE OF COAL AND COKE 2020 ():16.01.2020:3813-20/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM
2、 International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International
3、 does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM International or FBU“CIC“Interst
4、andard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D5865/D5865M-19 1 :D5865/D5865M-19 1 D5865/D5865M;,.().1.*1.1 .1.2,-,.,;,.1.3 ,.1 ASTM D05 ,D05.21 .1 2019.2019.1995.2013.D5865-13.DOI:10.1520/D5865_D5865M-19.*ASTM D5865/D5865M-19 2 ,.8.1.4 -,().2.2.1 AS
5、TM:2 D121,D346 D388 D1193 D2013 D3173 D3177 (2012.)3 D3180 D4239 2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 .www.astm.org.ASTM D5865/D5865M-19 3 D7582 E144 E178 E691 E882 E2251 ASTM 3.3.1 ,.D121.3.2:3.2.1 ,.3.2.2 ,.3.2.3 ,lbm .3.2.3.1 ASTM D5865/D5865M-19 4 (I.T.)1956
6、.,:1 I.T.=4,1868.,:1 I.T./=1,8 I.T./,1 I.T./=2,326/.3.2.4 ,.3.2.5 ,.3.2.6 (,),Qv(),.3.2.7 ,1 .3.2.8 ,.,.3.2.9 (,),Qp()ASTM D5865/D5865M-19 5 ,0,1 1,.3.3 ,:3.3.1 ,.3.3.2 ,.3.3.2.1 .4.4.1 .,.4.2 .,.(.2.1.)5.5.1 ,ASTM D5865/D5865M-19 6 ,.5.2 ,.5.3 .5.4 D388.6.6.1 ,.6.2 ,.,.20 3000 .,.6.3 ,0,0001.ASTM D
7、5865/D5865M-19 7 6.4 .,.,.,.10 0,01C,.,.,.6.5 ,0,1C(),0,1C,().,10 .6.6:6.6.1 0,0001C.,.ASTM D5865/D5865M-19 8 .0,1C .6.6.2 ,10.9,.,.6.6.3 ,S56C,S116C S117C E2251.6.6.3.1 ,.6.7 ,.4 500C.,0,0001.6.8 -100 16 34 B&S -(C),.0,10 38 B&S .(),ASTM D5865/D5865M-19 9 .6.9 6 30 ,.6.10 ,;.6.11 ,.4 7.7.1 ,II D119
8、3 .7.2 ,.5 4 -ASTM International RR:D05-1025.ASTM Customer Service serviceastm.org.5 ,D.C.,.,BDH Ltd.,Poole,Dorset,U.S.Pharmaceutical Convention,Inc.(USPC),Rockville,MD.ASTM D5865/D5865M-19 10 7.3 C6H5COOH (NIST),NIST.,.7.4 ,99,5%.,500C.7.5 ,.,.7.6 (Na2CO3).3,706 ,24 105C 1.(0,0699 N)HNO3 ,-59,7/-14
9、,3/(.X1.1).4,2 1,0.,1,0 0,1000 N 6,0 1,4 .,1 (/N)59,7 14,3.ASTM D5865/D5865M-19 11 8.8.1 .144.,.8.1.1 ,.8.1.2 .8.1.3 ,.,.3 4 300 500-.,.8.1.4 .8.1.5 ,.ASTM D5865/D5865M-19 12 8.1.6 .8.1.7 .9.9.1 ,250 60,D346 D2013 .10.10.1 0,8 1,2 .0,0001.10.2 :10.2.1 ,.1,0 .10.2.2 .10.2.3 .2 3 20 30.,.,.ASTM D5865/
10、D5865M-19 13 10.3 :10.3.1 ,2C ,.,.10.3.2 ,M 0,5,M .,.10.3.3 ,.10.4 :10.4.1 30 .0,001C,0,001C/.10.4.2 ,.,0,002C.10.4.3 ,30 ,10.4.1.ASTM D5865/D5865M-19 14 10.5 ,:10.5.1 ASTM S56C 0,002C.ASTM S116C S117C 0,001C,25 0,0001.,.10.5.2 5.0,01C 3.10.5.3 .a ta.10.5.4 .0,01C .1 ,0,001C.tc,c.,0,001C .ASTM D5865
11、/D5865M-19 15 tc,c.10.5.5 ,80%.,.6 ,1 .,.10.5.5.1 (-.),.(1000-.)16,03 .()(-.),16.03.().,.16 100%.,20 6 -ASTM International RR:D05-1028,.ASTM Customer Service serviceastm.org.ASTM D5865/D5865M-19 16 80%-(16,03 100/20=80%).10.5.6 ,.,.10.6 (.X1):10.6.1 (.X1.1)(10.6.1.1),(10.6.1.2).10.6.1.1 ,(.7.5),(.7.
12、6),.,()59,7 14,3 e1.10.6.1.2 ,.,.1 ASTM D5865/D5865M-19 17 340.340,.10.6.1.1.(e1),.,(e2),1%.(NAF),.e1=(NAF)*,(1):,340 41,9 10,0,1 26,45 6318.1,58 1000 1,58 1000.,:e1=1,58*,()(2),(e1),ASTM D5865/D5865M-19 18 .7 e1=(1,58/1000)*E*t(3),2%.10.6.2 (.X1.3):10.6.2.1 4:e2=Kl l(4):e2-,l-,Kl-0,96/0,23/34 B&S,K
13、l-1,13/0,27/34 B&S,Kl-0,00/,;10.6.2.2 (m),7 -ASTM International RR:D05-1028,.ASTM Customer Service serviceastm.org.ASTM D5865/D5865M-19 19 .e2=Km m(5):e2-,m-,Km-5,9/1,4/34 B&S,Km-7,5/1,8/34 B&S,Km-0,00/.J,.10.7 ,t,:t=tc ta+Ce+Cr(6):t-,C;ta-;tc-;Ce-,(.A1.6 A1.8);Cr-(.A1.1 A1.2).10.7.1 .10.8 (E):ASTM
14、D5865/D5865M-19 20 E=(Hc m)+e1+e2/t(7):E-,/C;Hc-,/;m-,;e1-10.6.1,(10.6.1.1),(10.6.1.2),;e2-10.6.2,;t-10.7,C.10.8.1 ,10.1 10.8,.10.8.2 (RSD),0,17%.,178,.1 .,.10.9 :10.9.1 .,.ASTM D5865/D5865M-19 21 ,.1.A J/C 1 10 258 20 2 10 249 20 3 10 270 272 4 10 254 0 5 10 245 72 6 10 249 20 7 10 241 156 8 10 266
15、 156 9 10 258 20 10 10 245 72 102 535 811 10 254 A/10 (s2)90 B/9 (s)9 ()(RSD)0,09%(/)100 10.9.2 25%,.10.9.3 .0,7 1,3 ,-,56/24/.ASTM D5865/D5865M-19 22 10.9.4 ,.11.11.1 .,-.,-,.11.1.1 .,.,.;,;.,.11.1.2 ASTM D5865/D5865M-19 23 ,10%,.5%,.,.,.11.1.3 :.11.2 :11.2.1 ,.().,(),.,.,.ASTM D5865/D5865M-19 24 1
16、1.2.2 .(.).LWL UWL(),95%,LCL UCL(),(99,7%),.,5%(.1 20),.11.2.3 ,.,.11.2.4 882 (1)8.(,),10 .:UCL +3/(N)UWL +2 /(N)X(),10 LWL -2 /(N)LCL -3 /(N)8,.ASTM D5865/D5865M-19 25 N ,-.-()N=1.()0,10%10 ,0,10%,.2 ,.2.1 26 454/()0,10%RSD 99%-(3)/UCL (/)UCL RSD 1.79,4 2 97,5 0,2606 56,1 3 115,3 0,2276 45,8 4 124,3 0,2088 39,7 5 130,1 0,1964 35,5 6 134,3 0,1874 32,4 7 137,6 0,1806 30,0 8 140,4 0,1751 28,1 9 142,7 0,1707 26,5 10 144,7 0,1669 25,1 15 151,8 0,1554 20,5 20 156,7 0,1470 17,7 25 160,2 0,1420 15,9 11
