1、 D5016-16 STANDARD TEST METHOD FOR TOTAL SULFUR IN COAL AND COKE COMBUSTION RESIDUES USING A HIGH-TEMPERATURE TUBE FURNACE COMBUSTION METHOD WITH INFRARED ABSORPTION 2018 ():26.11.2018:3581-18/ASTM -,.9,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM Inte
2、rnational)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(AST
3、M International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the
4、 specified translations by any Party,except for ASTM International or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D5016-16 1 D5016-16 1 D5016;,.().1.1.1 ,-,.1.2,.1.3 1 ASTM D05 ,D05.29 .1 2016.2016.1989.2008.D5016-081.DOI:10.1520/D50
5、16-16.ASTM D5016-16 2,.,.2.2.1 ASTM:2 D121,D3174 D3682 D3683 D4326 D4621 ,(2010.)3 D5142 (2010.)3 D6349 ,-2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.3 www.astm.org.ASTM D5016-16 3 D6357 ,-,-3.3.1 ,D121.3.2 .4.4.1 1450C .,.,.,-.-.,;,.-.,.,.ASTM D5016-16 4 4.2 ,4.1 (RM).5
6、.5.1 ,.,.6.6.1 ,.,-.,.:(1),(2)(3).,.,.ASTM D5016-16 5 7.7.1 ,(.7.2)150 165 1350C.7.2 ,23,3 450,-.7.3 ,.7.4 ,.8.8.1 ,.,.4,5 ,.8.2 (Mg(ClO4)2):.4 -ASTM.,.5 ,.American Chemical Society,Washington,DC.,.:,BDH Ltd.,Poole,Dorset,U.K.,U.S.Pharmaceutical Convention,Inc.(USPC),Rockville,MD.ASTM D5016-16 6 8.3
7、 COM-CAT.1 COM-CAT ,.8.4 99,5%,.:.,.9.9.1 ,.10.10.1 RM .,.RM (CRM),(NIST)(SABS),(ERM),CRM ,(IRM),CRM ERM,CRM.10.2 D3682,D4326 D6349.ASTM D5016-16 7 10.3 D3683 D6357.10.4 D3174 D5142 .2 ,.,.3 300 D3174,D3682,D4326,D5142 D6349;,.1.1450C 0,3 10 120 300 11.11.1/COM-CAT ,.1.,(.4).11.2 -,.1.ASTM D5016-16
8、8 (RM).RM .,.D4621.4 (6.1).RM .RM ,RM.11.2.1 .RM .,D3174,D5142,RM.RM .RM ,.RM ,.2.2.,RM 1 3 2 4 3 5 ASTM D5016-16 9 11.2.2 RM,.,RM.11.2.3 ,.RM,(.5).,.D4621,11.2.1,.5 RM,.-.11.3 :11.3.1 (.11.2).11.3.2 250 0,1 (,).1,0 COM-CAT.,.11.3.3 .,.6 (,1350C).ASTM D5016-16 10 A2 /,.12.12.1 (SO3):SO3 ,%=2,5 ST(1)
9、:ST ,%.12.2 :B=A (100 S)/100(2)A ,%,D3174 D5142;,%,;S ,%,12.1 13.13.1 .3.(Sr,r)(SR,R).A1.1 A1.3.%(r)A (R)A 0,7 3,8 0,06X+0,06 0,2X+0,2 A X .13.1.1 (r),ASTM D5016-16 11 ,95%.13.1.2 (R),95%.4.NIST SRM 1633b CRM RR,%CRM,%,%(95%)SRM 1633b 0,1907 0,2075 8,10 13.2 ,NIST SRM 1633b.NIST ,.4.7 ,.,(RM).,RM ,A
10、STM D5016-16 12 ,RM.,RM8.13.3 ,E691,2003.,-ASTM.6 14.14.1 ;6 -ASTM International RR:D05-1033.ASTM D5016-16 13 A1.A1.1 ,(Sr,r)(SR,R),.A1.1.A1.1.(Sr,r)(SR,R),.Sr SR r R SRM 1633b 0,19067 0,00921 0,01569 0,0258 0,04394 APBA 0,06919 0,00582 0,0144 0,01629 0,04032 BD 0,30605 0,01171 0,03036 0,03279 0,085
11、 BHA 1,74675 0,04919 0,15276 0,13773 0,42773 ESP5 3,14143 0,14028 0,32076 0,39278 0,89811 LP1 1,4066 0,02739 0,06569 0,07668 0,18393 LP2 3,8102 0,07168 0,21425 0,2007 0,59989 SDA 2,3825 0,09103 0,15721 0,25488 0,4402 SFA 1,74825 0,0652 0,12927 0,18255 0,36195 2009.A2.1.CA-18 COM-CAT .,C T-Max,.1-1,.
12、1-2,.2-1,.2-2,.1-1,.1-2,.2-1,.2-2.S,%.1450 1350 1350 300 300 480 223 300 378 300 300 438 241 300 441 300 300 401 2,43 1,97 2,47 2,39 2,04 2,44 2,48 2,15 2,36 2,43 2,11 2,40 2,43 2,07 2,42 A2.A2.1 ,ASTM D5016-16 14 1450C.(,1350C)(T-Max)SO2.60-,.CA-18 T-Max 480.A2.2 D5016(11)SO2 ,.A2.1.CA-18 ,1,57%.CA
13、-18 1350C.T-Max(300),.CA-18 ,1350C T-Max(480)(2,42%).A3.A3.1 COM-CAT ,(V2O5).,.V2O5 ,.A3.2 WAL-1 1450C.,.A3.1.WAL-1 ASTM D5016-16 15 1450C,.A3.1.WAL-1 1450C (C)1 2 3 3 .().().().().COM 1450 181 1,76 139 1,60 156 1,71 159 1,69-CCAT V2O5 1450 139 1,78 138 1,60 161 1,72 146 1,70 A3.3 CA-18 1350C.A3.2.A
14、3.2,COM-CAT .,COM-CAT T-Max.,V2O5 ,.,V2O5 ,1350C.A3.2.CA-18 1350C 1 2 3 3 .().().().().COM-CCAT 300 2,11 244 2,27 300 2,38 281 2,25 V2O5 184 2,46 169 2,3 263 2,43 225 2,40 ASTM D5016-16 16 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,West Conshohocken,PA 19428.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.
