1、 D 2384-83(2014.)-STANDARD TEST METHODS FOR TRACES OF VOLATILE CHLORIDES IN BUTANE-BUTENE MIXTURES 2017 ():27.04.2017:3143-17/ASTM -,.9,-49,119049.:(499)236-54-49:(499)230-13-72 E-mail:interstgost.ru http:/www.interstandart.ru/(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.AS
2、TM International ,ASTM International.-,ASTM International ,.This translation is executed by FBU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,
3、USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as the original version.Reproduction of the specified translations by any Party,except for ASTM Internatio
4、nal or FBU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.ASTM D 2384-83(2014)1 D 2384-83(2014.)-1 D 2384.,.().1.1.1 10 100 -.,-.,25 .1.2 .1 ASTM D02 ,D02.D0.04 C4.1 2014.2014.1965.2009.D2384-83(2009).DOI:10.1520/D2384-83R14.ASTM D 2384-83(2014)
5、2 1.3,.1.4 ,.,.5,8,11,14,19 Al.2.2.1 ASTM:2 D 329 D 1266 ()3.3.1 -.1 .-,.3.1.1 ;.3.1.2-2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM.ASTM D 2384-83(2014)3 ,.3.2 -.3.2.1 -.;.3.2.2 -,-Fe+.460 -.4.4.1 -.,;,.5.5.1 .,ASTM D 2384-83(2014)4 ,.3 ,.1.-5.2 ,.5.3(,.,.,3 ,DC.,.Analar
6、Standards for Laboratory Chemicals,BDH Ltd.,Poole,Dorset,United States Pharmacopeia and National Formulary,U.S.Pharmacopeial Convention,Inc.(USPC),Rockville,MD.-ASTM D 2384-83(2014)5 ,.,.)6.6.1 10 25,450 .(3100).6.2 20 .(137,5 ),.6.3 ,.7.7.1 ASTM ,D 1266,.8.8.1 ,8.3,D 1266.8.2 ()ASTM D 2384-83(2014)
7、6 .A1.1.)8.3,(2/)2,0 (Na2CO3)1.9.9.1 7 D 1266 ,35 Na2CO3.9.2 0,1.,.(.1)(.2).,(.D 1266,A3,.5).2 .,40 60,.:60-80C.9.3 ;,.CO2-O2 ,35 -;ASTM D 2384-83(2014)7 .,.9.4 ,.,0,1.,.,.9.5 16 21.-10.10.1-4 -.2.:,.4 ,Atlas Instrument Co.,8902 E.11th St.,Tulsa,OK,Greiner Glass Blowing Laboratories,3604 E.Medford S
8、t.,Los Angeles,CA 90034.,-ASTM International.1,.ASTM D 2384-83(2014)8 ,.10.2 1200/,.1 4 2 5 3 6 .2.-11.11.1 ().A1.1.)11.2 (.A1.2.)11.3 ,(2/).8.3.-O2 2 ASTM D 2384-83(2014)9 12.12.1 .50 Na2CO3.(.1)().A1.1.).,.)12.2 ,.12.3 16 21.12.4 ,50 Na2CO3.,.,.,.12.3.13.13.1 -,3 1%,0,005 0,008/.;ASTM D 2384-83(20
9、14)10 0,05 0,08 0,10 0,16 A/.3.13.2 ,.3,(600/),10-.13.3 ,.3.13.4 ,.:10 ASTM D 2384-83(2014)11 0,03 05 (0,76 1,3)0,75 1,0 (19,1 25,4)6,.90.(,).13.5 -10,.14.14.1 (99,5%)(.A1.3.),D 329.14.2 2 100 (80 100C),20 (KNO3).14.3 0,10 100 ,1 .,1.3 ,.HNO3(3+97).14.4,(10 Cl/)1+10 ,10 Cl/.ASTM D 2384-83(2014)12 14
10、.5 (10/)1 100 1 .,1.14.6 ,1 (H2O2,30%).14.7-(,Hg2Cl2),10 50 ,.(:.,.A1.4.)14.8 (.1,42)(HNO3).,.14.9 (1+28)1 (HNO3,.1,42)28 .14.10,.(.,.A1.5.)14.11 (100/)100 (KNO3)1.14.12 ,KNO3 .14.13 ,(KC1).14.14 ,(0,1)ASTM D 2384-83(2014)13 0,1 (AgNO3).14.15 ,(0,01)100 0,1 AgNO3 1.14.16 ,(0,001)10,0 0,1 AgNO3 1.14.
11、17 (2/)2 (Na2CO3)1.15.15.1 HNO3(.1,42).,.15.2 .5-,20 .(,).15.3 1-(305-)6;.,ASTM D 2384-83(2014)14 .,.,;KNO3.4 ,KNO3.1.15 15 ,10 25,20 25 HNO3,1 2 (10/),0,3 0,5 ,A/0,05-0,08 0,10-0,16 AgNO3 0,001 0,01 ,0,25 0,05-0,10 16.16.1 ,-,200 10,15 ,25,15 (.1).16.2 .1 ,HNO3 .16.3 ASTM D 2384-83(2014)15 ,.1.,-0,
12、23 0,02.1/;,.16.4 AgNO3(.1),30 40 .,.AgNO3 (.1);.,.,-.17.17.1 AgNO3 .,AgNO3.AgNO3,.5 (.4).,-;ASTM D 2384-83(2014)16 .-.4.17.2 ,:,=(A B)N 35 455/W(1):A-AgNO3,-AgNO3,N-AgNO3,W-,35 455-106().,ASTM D 2384-83(2014)17 18.18.1 (-),5 460 10 0,010 .19.19.1 ,(10 Cl/)14.4.19.2 2 (Fe(C104)36H20)1 (Hg(SCN)2).8,8
13、.19.3 14,0 (HNO3,1+2).120 (HClO4)HClO4.30.,100 5 10,.1.(HC1O4 ,.)19.4 (Hg(SCN)2).,Hg(SCN)2.19.5 (70%)(HClO4).ASTM D 2384-83(2014)18 20.20.1 0,0,1,0,2,0,3,0,4,0 5,0-(10 Cl/)25-.0,6 HC1O4,3,00 .,5-460.1,.,.21.21.1 ,-,200-10 .25-.21.2 20 ()25-.0,6 HC1O4,3,00 .,5-20.ASTM D 2384-83(2014)19 22.22.1 ,:,=(C
14、 B)/FW(2):-,-,(,),F-,W-.23.23.1 ,:23.1.1 (.6),:,15-70 11 6 ,.23.1.2 (.7),ASTM D 2384-83(2014)20,:,15-70 13 23.2 ,.7 ,.24.24.1;()A1.A1.1 ().,.,.ASTM D 2384-83(2014)21 .,.A1.2 .,.,./.,-.,.,.ASTM D 2384-83(2014)22.G-4 G-4.15 .A1.3 .,.,.A1.4 :.,.5 :1725 Jefferson Davis Hwy.,Arlington,VA 22202-4102.ASTM
15、D 2384-83(2014)23 .A1.5 .,.,.,.ASTM D 2384-83(2014)24 ASTM International -,.,.,.-ASTM International.,.,.ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959,United States.610-832-9585,610-832-9555 E-mail:serviceastm.org ASTM:(www.astm.org).,222 Rosewood Drive,Danvers,MA 01923,Tel:(978)646-2600;http:/.