1、 :D 6299101 STANDARD PRACTICE FOR APPLYING STATISTICAL QUALITY ASSURANCE AND CONTROL CHARTING TECHNIQUES TO EVALUATE ANALYTICAL MEASUREMENT SYSTEM PERFORMANCE 2011.():1552-11/ASTM :14.11.2011 Copyright ASTM International -,.9,-49,-1,119991.:(499)236-54-49,236-43-83:(499)230-13-72 E-mail:interstgost.
2、ru Web:www.interstandart.ru (ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International ,ASTM International.-,ASTM International ,.This translation is executed by FGU“CIC“Interstandard”of Federal Agency on Technical Regulating and Metrology under the license of American
3、 Society for Testing and Materials(ASTM International)100 rr Harbor Drive,West Conshohocken,PA 19428,USA.ASTM International does not approve and does not confirm these translations and in any cases only the English version published with a sign of ASTM International copyright can be considered as th
4、e original version.Reproduction of the specified translations by any Party,except for ASTM International or FGU“CIC“Interstandard”,is strictly forbidden according to the USA legislation and international copyright.Copyright ASTM International ASTM D 6299-101 1 :D 6299101 1 D 6299;,.().1 2011.1.1.1 ,
5、().1 ,.,1 ASTM D02 D02.94 .1 2010.2010.1998.2009.D 6299-09.DOI:10.1520/D6299-10.Copyright ASTM International ASTM D 6299-101 2:(1),(2),(3),(4),(5),.1.2 ,.1.3 .1.4 .1.5 ,D6708 .2 .D 3764.3 1.5 .1.6 ,(),.4 .Copyright ASTM International ASTM D 6299-101 32.2.1 ASTM:2 D 3764 D 5191 (-)D 6708 ,D 6792 D 73
6、72 E 177 ASTM E 178 E 456,E 691 3.3.1:3.1.1 ,.,(1),(2),Copyright ASTM International ASTM D 6299-101 4 ,(NIST),(3),.177,456 3.1.2,.177,456 3.1.3 ,.,.456 3.1.4 ,.,.177,456 3.1.5 ,.,.456 3.1.6,.,.456 3.1.7,.,.456 3.1.8 ,.,.2 ASTM,ASTM www.astm.org ASTM serviceastm.org.ASTM.Document Summary ASTM Copyrig
7、ht ASTM International ASTM D 6299-101 53.1.9 ,.,.3.2 ,:3.2.1 ,.,.3.2.1.1 (,ASTM,ISO).3.2.1.2 ,.3.2.2 ,.().3.2.3 ,.,.3.2.3.1 ,.Copyright ASTM International ASTM D 6299-101 6 ,.,.3.2.4 (,),.,.3.2.5 ,.(),.3.2.6 ,.,.3.2.7 ,.3.2.7.1 ASTM D02 ,.3.2.8 (),.,Copyright ASTM International ASTM D 6299-101 7,.3.
8、2.9 (SEV),.,.3.2.9.1 SEV ;,SEV,.3.2.10 (R),.,0,95(95%),.3.2.11 ,.,15.3.2.11.1 Copyright ASTM International ASTM D 6299-101 8 ,.,.24-,.3.2.12 ,.,.3.2.13 ,.(),.3.3:3.3.1 ARV .3.3.2 EWMA .3.3.3 I (I-).3.3.4 MR .3.3.5 MR .3.3.6 QC ().3.3.7 R .3.3.8 SEV .3.3.9 R .3.3.10 VA .3.3.11 2 -.3.3.12 .4 Copyright
9、 ASTM International ASTM D 6299-101 94.1 .,.4.2 .4.3 ,.5 5.1 ,.5.2,.5.3 ,.Copyright ASTM International ASTM D 6299-101 106.6.1 .6.1.1 ,.5 ,.6.1.2 ,(1),(,)(2).6.1.3 .6.1.4 .6.1.5 ,.6.1.6 ,.,6.1.3,Copyright ASTM International ASTM D 6299-101 11 .(,.,.,.,.)6.2 .6.2.1 ,.6 .6.2.2 ,.(ARV).3 6.2.2.1 ,.,Cop
10、yright ASTM International ASTM D 6299-101 12 .F .7 (ARV).,16 ARV ARV 4 .,ARV .16,.8 ,ASTM D02.CS92 ILCP;ASTM D02.01 N.E.G;ASTM D02.01.A;,Alberta Research Council.6.2.3 ,.,2,2-D 5191.,.6.3 (VA),3 ,.RR:D02-1007,E178 E691,ASTM ,ASTM International,1997.Copyright ASTM International ASTM D 6299-101 13 ,.7
11、.(QA)7.1 (1)4 (QA):(1),(2),(3),(4),(5)(VA),.(QA),(.7.1.1).7.1.1 ,.,.9 ,.D 6792.10 (PT),.D 7372.7.2 Copyright ASTM International ASTM D 6299-101 14 ,.7.3 :7.3.1 .7.3.2 ,NIST,JIS,BSI,.,(),.7.4/:7.4.1 .11 ,4 .Copyright ASTM International ASTM D 6299-101 15,.,.7.4.2 ,.,(1),(2),(3),(4),(5),.12 .,(.7.2),(
12、.7.3).,.(.7.3),(.7.2).7.4.3 .7.4.4 ,.7.4.5 ,.7.4.6 ,.13 ,Copyright ASTM International ASTM D 6299-101 16 .7.5 :7.5.1 ,.7.5.2 ,.7.6 :7.6.1 ,(ASTM),.,.7.6.2 (),.Copyright ASTM International ASTM D 6299-101 177.7 (VA).,VA,(QA).14 ,(),.,(QA)(VA).7.7.1 (VA),.7.7.1.1 ,.7.7.1.2 ,.,.7.7.1.3 .,Copyright ASTM
13、 International ASTM D 6299-101 18(ARV).,.8.,8.1 ,.,:8.1.1 ().8.1.2 ,(,).8.1.3,.8.1.4 .15 ,9,.8.2 ,.8.2.1 Copyright ASTM International ASTM D 6299-101 19 ,.8.2.2 ,.8.2.2.1 1 (1),(ARV),(2),(ARV):=(ARV)()(1)8.2.2.2 2 ,(ARV),=ARV /(ARV)2+(ARV)2 (2)ARV ,ARV,;ARV ARV.,ARV ,Copyright ASTM International AST
14、M D 6299-101 20,ARV .(.16.)8.2.2.3 (ARV),ARV .16 ARV .8.2.3 (VA),8.2.1 8.2.2.8.3 (1,2)(I),(MR),1(),2(EWMA)(.A1)(),(b)(3),.I ,.1()2(EWMA).MR .17 ,.,.8.3.1 :Copyright ASTM International ASTM D 6299-101 21 1 (),.2 (),1;,1,.1 8.4 ,(.19).20 .,(1.4).18 ,.19 1,8.7.2.3 8.7.3(Q-),.8.4.1 ,.,Copyright ASTM Int
15、ernational ASTM D 6299-101 22,.15,.8.4.2 ,.(.1.3).,.8.4.3 ,.-(Anderson-Darling)(.1.4).(.A1.4),.20 ,Copyright ASTM International ASTM D 6299-101 23.8.4.4 ,.8.4.4.1 MR .MR ,MR MR.8.4.4.2 I I.8.4.4.3 (EWMA)EWMA I.EWMA I.2 8.4.5 .8.5 :8.5.1 (.1.5),().8.5.2 ,.21 ,Copyright ASTM International ASTM D 6299-
16、101 24 ,.8.6 1 :8.6.1 1 (1),;(2).8.6.2 20 F-(.1.8),.F-,100 ,.8.6.3 F-,100 ,.8.6.4 F-,.,.8.7 2 :8.7.1 2 ,Copyright ASTM International ASTM D 6299-101 25 ,.I ,.8.7.2 1,:8.7.2.1 ,20.8.7.2.2 .,.8.7.2.3 ,MR .,I ,MR .MR,.Copyright ASTM International ASTM D 6299-101 268.7.2.4 20 ,F-,.F-,100 ,.8.7.2.5 F-,100 ,.8.7.2.6 F-,.,.8.7.2.7 I MR (EWMA 2),8,MR.8.7.2.8 I MR .8.7.3 2,Q-(.1.9)(6):8.7.3.1 .,Copyright ASTM International ASTM D 6299-101 27 .22 ,50 .8.7.3.2 Q-(),MR,(QA).8.7.3.3 Q-I,20 (Q-),8.7.2,20 ,Q-M
