1、Designation:D288719a2Designation:406Standard Test Method forBoiling Range Distribution of Petroleum Fractions by GasChromatography1,2This standard is issued under the fixed designation D2887;the number immediately following the designation indicates the year oforiginal adoption or,in the case of rev
2、ision,the year of last revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon()indicates an editorial change since the last revision or reapproval.This standard has been approved for use by agencies of the U.S.Department of Defense.1NOTEEditorially corrected Tabl
3、e 3 in March 2020.2NOTEEditorially corrected Table X6.1 in October 2020.1.Scope*1.1 This test method covers the determination of the boilingrange distribution of petroleum products.The test method isapplicable to petroleum products and fractions having a finalboiling point of 538 C(1000 F)or lower a
4、t atmosphericpressure as measured by this test method.This test method islimited to samples having a boiling range greater than 55.5 C(100 F),and having a vapor pressure sufficiently low to permitsampling at ambient temperature.NOTE1Since a boiling range is the difference between twotemperatures,onl
5、y the constant of 1.8 F C is used in the conversion ofthe temperature range from one system of units to another.1.1.1 Procedure A(Sections 6 14)Allows a largerselection of columns and analysis conditions such as packedand capillary columns as well as a Thermal ConductivityDetector in addition to the
6、 Flame Ionization Detector.Analysistimes range from 14 min to 60 min.1.1.2 Procedure B(Sections 15 23)Is restricted to only3 capillary columns and requires no sample dilution.Inaddition,Procedure B is used not only for the sample typesdescribed in Procedure A but also for the analysis of samplescont
7、aining biodiesel mixtures B5,B10,and B20.The analysistime,when using Procedure B(Accelerated D2887),is reducedto about 8 min.1.2 This test method is not to be used for the analysis ofgasoline samples or gasoline components.These types ofsamples must be analyzed by Test Method D7096.1.3 The values st
8、ated in SI units are to be regarded asstandard.The values given in parentheses after SI units areprovided for information only and are not considered standard.1.4 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is theresponsibility of the user of
9、 this standard to establish appro-priate safety,health,and environmental practices and deter-mine the applicability of regulatory limitations prior to use.1.5 This international standard was developed in accor-dance with internationally recognized principles on standard-ization established in the De
10、cision on Principles for theDevelopment of International Standards,Guides and Recom-mendations issued by the World Trade Organization TechnicalBarriers to Trade(TBT)Committee.2.Referenced Documents2.1 ASTM Standards:3D86 Test Method for Distillation of Petroleum Products andLiquid Fuels at Atmospher
11、ic PressureD1160 Test Method for Distillation of Petroleum Products atReduced PressureD2892 Test Method for Distillation of Crude Petroleum(15-Theoretical Plate Column)D4057 Practice for Manual Sampling of Petroleum andPetroleum ProductsD4626 Practice for Calculation of Gas ChromatographicResponse F
12、actorsD6300 Practice for Determination of Precision and BiasData for Use in Test Methods for Petroleum Products,1This test method is under the jurisdiction of ASTM Committee D02 onPetroleum Products,Liquid Fuels,and Lubricants and is the direct responsibility ofSubcommittee D02.04.0H on Chromatograp
13、hic Distribution Methods.Current edition approved Dec.1,2019.Published January 2020.Originallyapproved in 1973.Last previous edition approved in 2019 as D2887 191.DOI:10.1520/D2887-19AE02.2This standard has been developed through the cooperative effort betweenASTM International and the Energy Instit
14、ute,London.The EI and ASTMInternational logos imply that the ASTM International and EI standards aretechnically equivalent,but does not imply that both standards are editoriallyidentical.3For referenced ASTM standards,visit the ASTM website,www.astm.org,orcontact ASTM Customer Service at serviceastm
15、.org.For Annual Book of ASTMStandards volume information,refer to the standards Document Summary page onthe ASTM website.*A Summary of Changes section appears at the end of this standardCopyright ASTM International,100 Barr Harbor Drive,PO Box C700,West Conshohocken,PA 19428-2959.United StatesThis i
16、nternational standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for theDevelopment of International Standards,Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade(TBT)Committee.1Liquid Fuels,and LubricantsD6708 Practice for Statistical Assessment and Improvementof Expected Agreement Between Two Test Methods thatPurport to Measure the Same Property of a MaterialD7096