1、Designation:D 1967 86(Reapproved 1995)e1Standard Test Method forMeasuring Color After Heating of Drying Oils1This standard is issued under the fixed designation D 1967;the number immediately following the designation indicates the year oforiginal adoption or,in the case of revision,the year of last
2、revision.A number in parentheses indicates the year of last reapproval.Asuperscript epsilon(e)indicates an editorial change since the last revision or reapproval.e1NOTEUnit of measurement statement and Keywords were added editorially in May 1995.1.Scope1.1 This test method covers the measurement of
3、the color ofdrying oils after heating under specified conditions.1.2 The values stated in SI units are to be regarded as thestandard.The values given in parentheses are for informationonly.1.3 This standard does not purport to address all of thesafety concerns,if any,associated with its use.It is th
4、eresponsibility of whoever uses this standard to consult andestablish appropriate safety and health practices and deter-mine the applicability of regulatory limitations prior to use.2.Referenced Documents2.1 ASTM Standards:D 1544 Test Method for Color of Transparent Liquids(Gardner Color Scale)2E 1
5、Specification for ASTM Thermometers33.Significance and Use3.1 When oil is heated to polymerization temperature,somedarkening may occur rendering the oil unsuitable for use wherelight color is essential.Excessive darkening may be an indica-tion of residual soap content from the alkali refining proces
6、srendering the oil unsuitable for use where light color isessential.3.2 Some oils that are low in soap content may actuallybleach when heated to polymerization temperature,which isbeneficial.3.3 This test method is indicative of the color developedwhen the oil is heated to polymerization temperature
7、s.4.Apparatus4.1 Heater4A high-temperature gas burner or other suit-able gas burner.4.2 ThermometerAnASTM Partial Immersion Thermom-eter having a range from 5 to+400C(20 to 760F)andconforming to the requirements for Thermometer 3F(3C)asprescribed in Specification E 1.4.3 Color StandardsAset of perma
8、nent color standards asdescribed in Test Method D 1544.5.Procedure5.1 Place 100 mL of the oil sample in a 250-mL heat-resistant Griffin low-form beaker on a ring stand with anasbestos wire pad.Immerse the thermometer in the center ofthe oil so that the end of the bulb is from14to516in.(6 to 8mm)from
9、 the bottom of the beaker.Heat to 550F(288C)in5 to 10 min,and hold at this temperature 65F(63C)for 5min.Remove the beaker from the stand and allow to cool toroom temperature.Determine the color of the sample inaccordance with Test Method D 1544.6.Precision and Bias6.1 PrecisionThe following criteria
10、 should be used forjudging the acceptability of results at the 95%confidencelevel.6.1.1 RepeatabilityDuplicate results by the same operatorshould be considered suspect if they differ by more thanone-third color unit.6.1.2 ReproducibilityTwo results obtained in differentlaboratories should be conside
11、red suspect if they differ by morethan two-thirds color unit.NOTE1These precision statements are based on results obtained in acollaborative study involving six laboratories with two operators in eachlaboratory and four samples of drying oils.6.2 BiasBias has not been determined.7.Keywords7.1 color
12、after heating;drying oil color1This test method is under the jurisdiction of ASTM Committee D-1 on Paintand Related Coatings,Materials,and Applications and is the direct responsibility ofSubcommittee D01.32 on Drying Oils.Current edition approved March 27,1986.Published May 1986.Originallypublished
13、as D 1967 66 T.Last previous edition D 1967 85.2Annual Book of ASTM Standards,Vol 06.01.3Annual Book of ASTM Standards,Vol 14.03.4The Fisher heater has been found satisfactory for this purpose.1AMERICAN SOCIETY FOR TESTING AND MATERIALS100 Barr Harbor Dr.,West Conshohocken,PA 19428Reprinted from the
14、 Annual Book of ASTM Standards.Copyright ASTMThe American Society for Testing and Materials takes no position respecting the validity of any patent rights asserted in connectionwith any item mentioned in this standard.Users of this standard are expressly advised that determination of the validity of
15、 any suchpatent rights,and the risk of infringement of such rights,are entirely their own responsibility.This standard is subject to revision at any time by the responsible technical committee and must be reviewed every five years andif not revised,either reapproved or withdrawn.Your comments are in
16、vited either for revision of this standard or for additional standardsand should be addressed to ASTM Headquarters.Your comments will receive careful consideration at a meeting of the responsibletechnical committee,which you may attend.If you feel that your comments have not received a fair hearing you should make yourviews known to the ASTM Committee on Standards,100 Barr Harbor Drive,West Conshohocken,PA 19428.D 19672
